New natural 2-acetoxy fatty acids using chemical ionization and electron impact mass spectrometry

The phospholipids of the spongePolymastia gleneni contain saturated long chain (C_22–30)-acetoxy fatty acids. Their structures were assigned based on chromatographic and spectrometric data as well as comparison with a synthetic sample. The use of capillary gas chromatography combined with chemical ionization and electron impact mass spectrometry was instrumental in the eludication of structures, since only a very small amount of crude lipids was available. Part 10 of “Phospholipids in Marine Organisms.” For Part 9 in this series, see reference 12.     

A broad line n.m.r. study of oriented poly(vinylidene fluoride)

Broadline nuclear magnetic resonance measurements have been carried out for the proton resonance in oriented poly(vinylidene fluoride). The spectra in general show two component lines with distinctly different line widths. The broad component shows a high degree of molecular orientation and can be satisfactorily assigned to the crystalline regions of the polymer. The narrow component corresponds to an oriented non crystalline phase which is sufficiently constrained to allow motion about the chain axis only. An appreciable decrease in the value of the rigid mass fraction was observed in both of the samples over the temperature range examined. Our calculations indicate that this could play an important role in the temperature dependence of the pyroelectric response of this material.     

Laboratory accreditation in the UK

Two complementary national laboratory accreditation schemes are run by the National Physical Laboratory (NPL) to provide official recognition of competent British laboratories and an assurance of quality to their customers. The first of these, the British Calibration Service (BCS), was set up in 1966 to accredit laboratories to calibrate instruments, gauges and reference materials. In 1981 the National Testing Laboratory Accreditation Scheme (NATLAS) was formed to extend the service to all kinds of testing. Both BCS and NATLAS form an integral part of the UK national measurement system and were combined to form the National Measurement Accreditation Service on 1 October 1985.     

Combining multiple knowledge bases

Combining knowledge present in multiple knowledge base systems into a single knowledge base is discussed. A knowledge based system can be considered an extension of a deductive database in that it permits function symbols as part of the theory. Alternative knowledge bases that deal with the same subject matter are considered. The authors define the concept of combining knowledge present in a set of knowledge bases and present algorithms to maximally combine them so that the combination is consistent with respect to the integrity constraints associated with the knowledge bases. For this, the authors define the concept of maximality and prove that the algorithms presented combine the knowledge bases to generate a maximal theory. The authors also discuss the relationships between combining multiple knowledge bases and the view update problem     

A mixed finite element model for the elastic contact problem

The static elastic contact problem is approached using Lagrange multipliers, leading to a mixed finite element problem. A non-linear friction law is introduced explicitly and the non-local character of the friction phenomena is implicitly assumed. In order to avoid stress oscillations near singular points, a perturbed Lagrangian functional is considered. The algorithms herein proposed do not impose nodal dependencies over the contact surfaces, allowing for the independent discretization of both bodies. The method is able to model simultaneous contact over different regions of any geometrical shape. Computer code, examples and results presented here are restricted to axisymmetrical and bidimensional cases.     

Dosimetric characteristic of VVR-M reactor with respect to tritium

Translated from Atomnaya Énergiya, Vol. 67, No. 2, pp. 111–113, August, 1989.     

测定钠中杂质的手动阻塞计的研究

文章介绍了测定钠中杂质浓度的手动阻塞计的原理、装置和实验结果。为了减少测量误差,我们研究了影响准确测定阻塞温度的因素,并且找到了减少测量误差的办法。在同样的杂质饱和温度下,该阻塞计测得的高、低阻塞温度所对应的杂质浓度差是很接近的。对氧其差值为1.03ppm;对氢为0.0763ppm。