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991.
在建设部令第136号《城市地下管线工程档案管理办法》颁布前后,珠海馆从思想着手,从立法、宣传、教育、调研协调、具体措施等方面,将工作落到实处,为珠海市科学管理城市地下管线奠定了基础。 相似文献
992.
风管摩擦阻力的直接计算方法 总被引:2,自引:1,他引:1
提出用高精度的反映密度、黏度和温度关系的经验公式和Colebrook公式计算风管摩擦阻力系数的方法。分析和算例表明,用该方法计算,计算结果比采用常用工程设计方法更为准确,为应用计算机进行风道设计提供了直接、简便的方法。 相似文献
993.
Junwei Fu Zhengbiao Zhang Zhenping Cheng Jian Zhu Wei Zhang Xiulin Zhu 《Polymer Bulletin》2008,61(3):287-297
A novel reversible addition-fragmentation chain transfer (RAFT) reagent bearing triphenylamine (TPA)
group, 4-diphenylamino-dithiobenzoic acid benzyl ester (DDABE), was designed and synthesized. It was used
in the RAFT polymerizations of styrene (St) and methyl acrylate (MA) to prepare end-functionalized polymers.
The results of the polymerization showed that the RAFT polymerizations could be well controlled using DDABE
as the RAFT agent. Number-average molecular weight (Mn,GPC) increased linearly
with monomer conversion, and molecular weight distributions were relatively narrow (PDI<
1.50). The results of chain-extension reaction, 1H NMR spectra and UV/Vis
spectra confirmed that most of the polymers chains were end-capped by the functional triphenylamine
(TPA) groups. The effect of feed molar ratios of St/DDABE/AIBN on polymerization was investigated. 相似文献
994.
光栅谐振子检测地震波的理论和方法研究 总被引:2,自引:0,他引:2
提出了一种新的检波理论和方法 ,它是一种实现检测地震波信号的地震勘探技术。采用光栅谐振子为敏感元件 ,将大地震动的机械信号转换成光调制信号—莫尔条纹 ,再用光电接收器件将其转换成数字化电信号输出。光栅谐振子检测地震波的装置能够直接将大地震动的机械信号转化为脉冲数字信号输出 ;并以记数的形式采样 ,避免了器件的精度不同对传感器输出的数据质量的影响 ,从而简化了组装工艺。文中阐述了该方法的工作原理、参数计算、测试方法和实验结果 相似文献
995.
The cellulose solvent dimethyl sulfoxide (DMSO)/tetrabutylammonium fluoride trihydrate (TBAF) was
successfully applied as reaction medium for the synthesis of allyl cellulose by conversion of the polymer
with allyl chloride in the presence of solid NaOH. Samples with degree of substitution from 0.50 to 2.98
were accessible by varying the molar ratio anhydroglucose unit:allyl chloride:NaOH and reaction time. DMSO/TBAF
was found to be an efficient reaction medium for the preparation of highly functionalized samples from spruce
sulfite pulp with degree of polymerization of about 500 even in a scale of 50 g. The allyl cellulose samples
were characterized by means of FTIR- and NMR spectroscopy. Size exclusion chromatography revealed negligible
polymer degradation during synthesis and purification of the samples. 相似文献
996.
Vanesa Rodríguez-Amor Juan P. Fernández-Blázquez Antonio Bello Ernesto Pérez María L. Cerrada 《Polymer Bulletin》2008,60(1):89-96
Summary The effect of molecular weight on the uniaxial orientation process has been analyzed in two samples of thermotropic poly(diethylene
glycol p,p′-bibenzoate), evaluating the influence of that parameter on the type of orientation obtained. Several strain rates and deformation
temperatures have been tested in order to map out the conditions for obtaining the two different kinds of orientation. The
results show that in the lower molecular weight PDEB sample (Mw=31200) it is rather easy to get exclusively perpendicular “anomalous” orientation, with the molecular axes aligned transversely
to the stretching direction. However, it is extremely difficult to obtain 100% parallel “normal” orientation. On the contrary,
either type of orientation or a mixture of them can be easily developed for the higher molecular weight PDEB sample (Mw=102900). 相似文献
997.
Qingzhao Yao Yuming Zhou Yanqing Sun Xiaoyun Ye 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(4):477-484
TiO2 hybrid molecular imprinted polymer (MIP) for ethofumesate using methacrylic acid (MAA) as the functional monomer and silane
coupling agent 3-(trimethoxysilyl) propylmethacrylate (KH570) as organic–inorganic connective bridge was synthesized via photo-excitation
method. Hydrogen bond was proved to act between MAA and ethofumesate for pre- and post-polymerization binding properties as
testified by UV spectrometric method. KH570 modified TiO2 nanoparticles were prepared via sonochemical reaction, which can accelerate hydrolysis, increase collision chance for the
reactive system and improve the dispersion of the nanoparticles. Scanning electron microscope (SEM), transmission electron
microscope (TEM), binding and the adsorption kinetics experiments as well as thermogravimetric analysis (TGA) were employed
for characterization. The results indicated that the hybrid MIP revealed a larger surface area and more ordered imprinting
cavities with improved thermal stability compared to organic-only MIP. Furthermore, faster adsorption kinetics and enhancive
adsorption capacity were achieved, which made it promising in chemical sensor applications. 相似文献
998.
Muhammad Maqbool Hugh H. Richardson Martin E. Kordesch 《Journal of Materials Science》2007,42(14):5657-5660
Thin films of Praseodymium doped AlN are deposited on silicon (111) substrates at 77 K and 950 K by rf magnetron sputtering
method. About 500–1000 nm thick films are grown at 100–200 watts RF power and 5–8 mTorr nitrogen, using a metal target of
Al with Pr. X-rays diffraction results show that films deposited at 77 K are amorphous and those deposited at 950 K are crystalline.
Cathodoluminescence studies are performed at room temperature and luminescence peaks are observed in a wide range from ultraviolet
to infrared region. The most intense peak is obtained in green at 526 nm from amorphous films as a result from 3P1→3H5 transition. In crystalline films the intense peak was obtain in red at 648 nm as a result from 3P0→3F2 transition. Films are thermally activated at 1300 K for half an hour in a nitrogen atmosphere. Thermal activation enhances
the intensity of luminescence. Two peaks at 488 nm and 505 nm merged after thermal activation, giving rise to a single peak
at 495 nm. 相似文献
999.
影响碾压混凝土抗裂性能的因素很多,本文主要从水泥矿物成分、石粉含量、掺和料(氧化镁等)、骨料特性(弹性模量)及砂率等方面影响因素开展试验研究,分析各因素对碾压混凝土抗裂性能的影响效果。试验结果表明,砂率和石粉含量均存在碾压混凝土抗裂能力最大的最优含量;掺入适量的氧化镁掺和料和合理增加水泥熟料中的C,S和C4AF两种矿物成分含量,对提高碾压混凝土的抗裂能力非常有利;骨料的弹性模量是影响混凝土弹性模量的重要因素,使用低弹性模量骨料可以大大降低混凝土的弹性模量,增大极限拉伸值,提高混凝土的抗裂能力。 相似文献
1000.
在600mm的有机玻璃冷模塔中,用水-空气体系测定矩形垂直筛板的塔板压降、漏液和雾沫夹带等流体力学性能,确定了合理的塔板结构,使其具有较高的气液通量和较宽的操作范围,空塔动能因子最大可达3.0kg1/2(m1/2.s)-1,液流强度可达21.6m3/(m.h)。并对不同气液流量下塔板的流体力学实验数据进行关联和分析,得出了矩形垂直筛板的干板压降计算关联式以及漏液率随液流强度和空塔动能因子的变化关系,为矩形垂直筛板的设计提供了依据。与新垂直筛板相比,矩形垂直筛板具有更低的塔板压降。 相似文献