Lipase‐catalyzed dynamic kinetic resolution of (R,S)‐fenoprofen thioester in isooctane

A lipase‐catalyzed enantioselective hydrolysis process under in situ racemization of the remaining (R)‐thioetser substrate with trioctylamine as the catalyst was developed for the production of (S)‐fenoprofen from (R,S)‐fenoprofen 2,2,2‐trifluoroethyl thioester in isooctane. Detailed investigations of trioctylamine concentration on the enzyme activation and the kinetic behavior of the thioester in racemization and enzymatic reactions were conducted, in which good agreement between the experimental data and theoretical results was observed. © 2002 Society of Chemical Industry     

Prolongation and enhancement of postischemic c-fos expression after fasting

BACKGROUND AND PURPOSE: A rapid but transient expression of c-fos after cerebral ischemia has been extensively documented. However, the mechanism of this induction and whether induction of c-fos is neuroprotective or detrimental to the brain after ischemia is presently not clear. Fasting before transient cerebral ischemia has been shown to reduce delayed neuronal necrosis and infarct volume. The purpose of the present study was to examine the effect of preischemic fasting for 24 hours on the expression of c-fos after transient focal cerebral ischemia. METHODS: Focal cerebral ischemia was induced by temporary occlusion of the right middle cerebral artery and both common carotid arteries for 60 minutes. Male Long-Evans rats weighting 250 to 300 g were randomly divided into two groups: fed (control group) and food deprived for 24 hours (fasted group) before ischemic surgery. Infarct volumes were measured on the basis of triphenyltetrazolium chloride-delineated infarct areas, and plasma glucose levels were determined by the glucose oxidase method. Temporal and spatial expression of c-fos was assessed by Northern blot analysis, in situ hybridization, and immunohistochemistry. RESULTS: Fasting for 24 hours before 60 minutes of ischemia resulted in a 26.6% decrease in preischemic plasma glucose levels and a 74.5% reduction in infarct volumes in the fasted group compared with the control group. A rapid but transient induction of c-fos mRNA was observed in the ischemic cortex in control animals after 60 minutes of ischemia. Fasting not only prolonged but also enhanced the intensity of c-fos expression in the ischemic cortex. Regional c-fos expression was also different between these two groups. CONCLUSIONS: The results support the contention that c-fos expression may be compatible with its purported neuroprotective role in selected experimental paradigms. The signaling mechanisms underlying the effect of fasting and subsequent lowering of plasma glucose levels on postischemic c-fos expression remain to be explored.     

应用线性相关分析方法探讨国土卫片几何畸变纠正的精度

我国卫星影像具有空间分辫率高，比例尺适中的特点。由于国土片是全.景成像比例尺变化大，用它来编绘专业地图，给精度衡蚤带来很大困难，需要对国土片进行几何校正。本文试图用线性相关分析方法，分析经过AR月尧卜n图像处理系统刘正的国土片几何精度。以便为分析专题图精度提供依据，同时也为分析遥感影像几何精度介绍一种方法。     

Ion implantation doping of OMCVD grown GaN

Doping by ion implantation using Si, O, Mg, and Ca has been studied in single crystal semi-insulating and n-type GaN grown on a-sapphire substrates. The n-and p-type dopants used in this study are Si and O; Mg and Ca, respectively. Room temperature activation of Si and O donors has been achieved after 1150°C annealing for 120 s. The activation of Mg and Ca acceptors is too low to measure at both room temperature and 300°C. Using higher doses to achieve a measurable p-type conduction increases the amount of damage created by the implantation. Rutherford back scattering measurements on this material indicate that the damage is still present even after the maximum possible heat treatment. Secondary ion mass spectrometry measurements have indicated a redistribution in the measured profiles of Mg due to annealing.     

Fast‐scale bifurcation in power‐factor‐correction buck‐boost converters and effects of incompatible periodicities

In this paper, we derive the discrete‐time model for the power‐factor‐correction (PFC) buck‐boost converter in terms of a stroboscopic switching map. Fast‐scale instability is analysed through a fold diagram, which exposes the periodicity of the operation as well as the locations of the critical phase angles of the line voltage at which instability begins to occur along a half‐line cycle. The asymmetrical locations of the critical phase angles along a half‐line cycle is explained in terms of ‘under‐developed’ bifurcation. Border collision bifurcations are observed and analysed in detail. Copyright © 2006 John Wiley & Sons, Ltd.     

Structure and Magnetic Properties of LaCo_(13-X)M_X Intermetallic Compounds

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短毫米波和亚毫米波接收机的发展现状

本文概述了短毫米和亚毫米波接收机的发展现状，介绍了接收机的重要组成部件：混频器、振荡器和放大器的发展水平以及毫米波单片集成电路的现状，给出了接收机的最新性能指标。     

CALCULATION ON TWO-PHASE FLOW TRANSIENTS AND THEIR EXPERIMENTAL RESEARCH

From basic equations of gas-liquid, solid-liquid, solid-gas two-phase flow, the calculating method on flow transients of two-phase flow is developed by means of characteristic method. As one example, a gas-liquid flow transient is calculated and it agrees well with the experimental result. It is shown that the method is satisfactory for engineering demand.     

新型处理药剂（EP-110）处理各种重金属离子的实验研究

各行各业生产过程中会产生大量废水,重金属离子污染物是其中的重要控制指标,传统的处理方法不能完全解 决这类污染。本文通过大量的实验数据,对新型的处理药剂(EP-110)处理各种重金属离子的性能做了全面的测试、分析,并 提出了使用方法。     

一种可调节电流的电流型PWM直流转换器

介绍一种用于驱动发光二极管(LED)的可调节电流的电流型PWM直流转换器.该直流转换器由于接有一个外接电阻,可以通过调节外接电阻的大小来调节输出电流.输出电流调节范围在5～40mA之间.主要分析了电路的输出电流调节功能,和这种输出电流可变的电流型PWM直流转换器的电流和电压反馈环的反馈实现原理.并简要介绍了这种带电流调节功能的PWM直流转换器的工作原理,最后给出了电路在输出不同电流时使用HSPICE软件对反馈参考电压,PWM锁存器输出波形的仿真结果.