Graded evolution of anisotropic microstructure during sintering from crystal-oriented powder compact

Anisotropic sintering, including shrinkage and grain growth, was examined for c-axis-oriented (Sr,Ca)₂NaNb₅O₁₅ (SCNN) ceramics, which were prepared by colloidal processing under a magnetic field. In the c-axis-oriented SCNN powder compact, shrinkage and grain growth along the c-axis were higher than those along the a-axis. The anisotropic microstructural development was clearly associated with anisotropic sintering shrinkage. X-ray diffraction, scanning electron microscopy, and energy back scattering diffraction showed that the grain growth of oriented particles by including random grains contribute to the development of the oriented microstructure. Finally, the highly crystal-oriented SCNN ceramics with a densified microstructure were obtained through anisotropic sintering. These results clearly showed the potential to develop a well-defined anisotropic microstructure during sintering by designing and controlling the particle packing structure in a powder compact.     

刘家山排土场滑坡治理措施

刘家山排土场为民采排弃形成，已经出现大规模滑坡。为了保证上下游生产生活设施的安全，依据现场实际情况，结合现场调查，提出了削坡处理的方案。经过治理后，刘家山排土场平稳地渡过了雨季，目前处于稳定状态，达到了治理目的。     

随钻扩眼工具及技术研究

基于随钻扩眼技术优势的分析，研究了机械式、液压式和偏心式随钻扩眼工具执行机构和扩眼总成的机构原理，并介绍了国内所开展的相关研究。文章提出应加强现有工具的适应性和匹配性研究，发掘各类工具的优势。优化执行机构、扩眼总成和水力机构、重视底部钻具组合力学特性的分析是今后发展和完善随钻扩眼工具及技术的几个重要内容。实践表明，随钻扩眼技术在处理井下复杂情况、降低钻井综合成本、提高钻井速度、提高建井质量和安全性等方面具有显著的优势，随钻扩眼工具也正逐渐成为一种重要的石油钻井配套工具。     

Robust nonlinear feedback–feedforward control of a coupled kinetic Monte Carlo–finite difference simulation

Robust nonlinear feedforward–feedback controllers are designed for a multiscale system that dynamically couples kinetic Monte Carlo (KMC) and finite difference (FD) simulation codes. The coupled codes simulate the copper electrodeposition process for manufacturing on-chip copper interconnects in electronic devices. The control objective is to regulate the current density subject to the condition that the steady-state fluctuation of the overpotential remains bounded within ±0.01 V. The controller designs incorporate a low-order stochastic model that captures the input–output behavior of the coupled KMC–FD code. The controllers achieve the objectives and the closed-loop responses implemented on the low-order model and the coupled KMC–FD code match well within stochastic variations. The nonlinear feedforward control reduces the rise time of the controller response while the feedback control ensures robustness in the presence of model uncertainty.     

焉耆盆地原油物理化学特征及油源对比研究

在焉耆盆地侏罗系三工河组和八道湾组均发现原油,目前关于侏罗系产层原油的油源问题存在不同的认识。对研究区原油的物理、化学性质进行系统的研究,认为侏罗系三工河组和八道湾组原油不仅在物理性质上有一定的差别,而且在地球化学组成及生物标记化合物上也有一定的差异,应具有不同的来源。侏罗系三工河组原油属于典型腐殖型干酪根成因,而侏罗系八道湾组原油除了具有腐殖型干酪根成因的某些特征外,还具有湖相泥岩生烃的特点。通过原油与各类源岩生物标志物进一步对比分析发现,侏罗系三工河组原油与西山窑、三工河组烃源岩及石炭系、三叠系烃源岩地球化学特征均存在明显差异,与侏罗系八道湾组烃源岩对比性较好。侏罗系八道湾组原油与八道湾组、三叠系源岩有一定相似性,因此认为八道湾组源岩为其主要源岩,三叠系源岩也有一定的贡献。目前勘探生产主要以八道湾组烃源岩为目标,下一步应加强对三叠系烃源岩贡献区带的勘探部署。      

大牛地气田气井无阻流量的确定方法研究

大牛地气田气井试井大多采用一点法，由于气层渗透性差，测试时间短，流压很难达到稳定，计算的无阻流量往往偏高，且无法获得正确的产能方程。通过气田多口井修正等时试井数据进行统计分析，获得了一点法试井在不同生产时间下计算无阻流量的经验公式；利用气田修正等时试井的二项式方程系数曰，计算惯性阻力系数并经过曲线回归处理获得了经验关系式，很好地解决了一点法试井计算产能方程的问题。     

施工过程中腐蚀隐患的控制

通过分析石化装置施工过程中常见的现象,分析产生由这些现象加重腐蚀的原因和机理, 指出应加强施工过程中的控制,而达到预期的防腐蚀效果,消除腐蚀隐患。     

茂金属线型低密度聚乙烯的加工性能

采用齐聚-共聚复合催化剂合成出了相对分子质量分布指数大于4的原位共聚线型低密度茂金属聚乙烯(mLLDPE)。流变实验结果表明,mLLDPE具有切敏性和非温敏性。改性实验结果表明,向100质量份mLLDPE中加入5质量份氟母粒,或10质量份LDPE,或2质量份氟母粒和5质量份LDPE,可使mLLDPE的加工流动性能获得改善,聚合物的机械性能不会发生明显降低,可用常规加工设备加工。加工成型实验结果表明,使用65型管材挤出机和TDL-12L中空成型机,以氟母粒-LDPE复合改性mLLDPE为原料,可生产出内、外表面均光滑的32管材和10L中空容器,挤出过程稳定。