Thermoplastic vulcanizates obtained by reaction-induced phase separation: Interplay between phase separation dynamics,final morphology and mechanical properties

Reaction-induced phase separation (RIPS) of miscible blends of poly(?-caprolactone) (PCL) and an epoxy resin based on poly(propylene oxide) (PPO) was used to prepare thermoplastic vulcanizates (TPVs) with fine rubber dispersions. Scanning electron microscopy (SEM) confirmed the formation of cross-linked rubber particles dispersed in the thermoplastic matrix at PCL contents ≥20 wt%. The morphology development during phase separation was studied by optical microscopy (OM) and time-resolved small-angle light scattering (SALS). It was shown that higher curing temperatures lead to a decrease in rubber particle size, but at the same time lead to an increase in the extent of particle connectivity. In some cases, gelation of the PPO-rich phase limits full structure development, which leads to extensive connectivity between the dispersed rubber particles and a strong deterioration in tensile properties.     

Effects and properties of poly(arylene ether benzonitrile)s of various molecular weights blended with sulfonated poly(ether ether ketone)

Poly(arylene ether benzonitrile) (PAEBN) was synthesized with 2,6‐dichlorobenzonitrile and biphenol. PAEBNs with various molecular weights (MWs), 1,640,000 and 185,000 g/mol, were synthesized by control of the stoichiometry of the monomers and were blended with sulfonated poly(ether ether ketone) (SPEEK). The effects of MW on the water uptake, swelling, methanol permeability, and proton conductivity of the SPEEK/PAEBN blend membranes were investigated. The molecular mobility of the SPEEK/PAEBN blends was also examined in this study. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

支持专业知识获取的中间件的研究

 分析了如何利用中间件技术支持专业知识获取的问题．提出了基于XML，SOAP，UDDI和WSDL的web服务技术的专业知识获取的中间件应用模式，它可以有效解决消息传送、服务功能的抽象描述以及服务在网络上的发布与发现等问题。以固定瓦推力滑动轴承的性能参数计算Web服务为实例，指出web服务是分布式设计知识获取和知识资源集成的有效途径．     

2197铝锂合金的组织和性能

通过力学性能测试和显微组织观察研究了2197合金组织和性能之间的关系。结果表明,2197合金具有中等强度,小的各向异性,强的热稳定性。该合金在T8状态下能获得最佳的强度和塑性配合,在T6峰时效状态以析出少量δ′相、θ′相和T_1相联合强化为主。在2197合金的相组成中,T_1相析出数量不占主导地位,Al_6Mn弥散质点的析出有利于减小各向异性。2197合金中Li含量较低,使其呈现较强的热稳定性。     

一种跟踪电网频率的新方法

基于正交变换,提出了一种新的电网频率跟踪方法.针对两种模型进行仿真,表明该方法能够较为精确与快速地跟踪电网频率,尤其针对突变频率的信号,具有较好的跟踪效果;同时算法克服了同步采样条件的限制,通过迭代,在不同初始频率下均具有较好的收敛性.     

无键联接传动的特点及锥面弹性衬套设计和应用

无键联接在特殊行业和工况中是键联接传递动力和运动的有力补充,介绍了工程上应用的圆弧三边形型面联接、弹性环无键联接、圆柱面过盈联接等几种无键联接传动方式及其工作原理,并分析了各自的性能特点和应用情况。针对无键联接传动的特点、特殊行业和工况的应用实际,设计了锥面弹性衬套无键联接传动结构并介绍了其在工程中的实际应用。     

联邦卡尔曼滤波在INS＼GPS组合导航中的应用

介绍了INS＼GPS组合导航系统的优点;根据联邦卡尔曼滤波原理,设计了INS＼GPS组合导航系统的滤波算法;对该组合系统的联邦卡尔曼滤波算法进行了仿真;仿真结果表明,在INS＼GPS组合导航系统中采用联邦卡尔曼滤波,不仅提高了定位精度,而且保证了滤波的快速性.     

ARM嵌入式处理器在智能仪器中的应用

介绍了一种基于ARM嵌入式处理器系统的智能仪器的硬件和软件设计方案,并结合uc/os-II嵌入式实时操作系统,给出了一套完整的任务调度和管理的方法,最后给出实例说明.     

CO毒化AB5型合金分形特征研究

研究了三种贮氢合金 L a Ni5、L a Ni4 .7Al0 .3、Ml Ni4 .5Al0 .5被 10 0× 10 - 6 CO毒化后的分形特征 ,求出这三种合金在含 10 0× 10 - 6 CO的氢中循环 ,分维分别为 0 .2 5 4 7、0 .170 9、0 .0 72 5。可以较好的解释合金被毒化的宏观现象。     

童亭矿锚杆支护安全可靠性控制

简要介绍了煤巷锚杆支护技术在童亭煤矿的应用推广情况 ,重点介绍了童亭煤矿在安全可靠性控制方面强化管理、优化设计、提高工艺水平和质量保证体系建设的一些经验和做法 ,并对今后发展煤巷锚杆支护技术提出了看法。