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61.
In order to improve the solubility of C60 fullerene in conventional solvents, grafting of hydrophilic poly(ethylene oxide) (PEO) by utilizing the radical-trapping nature of C60 fullerene was investigated. Macroazo initiators containing a poly(ethylene oxide) unit, known as Azo-PEO, were prepared at various molecular weights by the reaction of 4,4′-azobis(4-cyanopentanoyl chloride) with poly(ethylene glycol) methyl ether. PEO radicals formed by thermal decomposition of Azo-PEO were successfully trapped by C60 fullerene to give PEO-grafted C60 fullerene. Their structures were confirmed by FT-IR spectroscopy, size exclusion chromatography, UV-vis spectroscopy, and differential scanning calorimetry. When Azo-PEO with low-molecular weight was reacted with C60 fullerene, a bis-adduct, C60-(PEO)2, and a tetrakis-adduct, C60-(PEO)4, were formed. In contrast, in reactions with Azo-PEO of higher molecular weight, only the bis-adduct was formed, and no formation of the tetrakis-adduct was observed. The structure of bis-adduct was found to be 1,4-type. The solubility of C60 fullerene in water, THF, methanol, and other conventional organic solvents was remarkably improved by grafting of PEO. In addition, the thermal stability of PEO was dramatically increased by grafting onto C60 fullerene. 相似文献
62.
Prediction model of surface residual stress within a machined surface by combining two orthogonal plane models 总被引:2,自引:1,他引:2
Hiroyuki Sasahara Toshiyuki Obikawa Takahiro Shirakashi 《International Journal of Machine Tools and Manufacture》2004,44(7-8):815-822
The variation of surface residual stress within a machined surface layer caused by face turning was studied. The size of the tool’s corner radius and the feed rate affect residual stress. A process model using the finite element method is proposed and the mechanical effects of the corner radius and feed rate on a machined surface were discussed. When a tool with a small corner radius is used, surface residual stress perpendicular to the cutting direction becomes compression stress. As well, surface residual stress changes from tension to compression as the feed rate decreases. The process model consists of an orthogonal cutting simulation and an indentation-like simulation of a corner radius into a work piece surface. The simulated results show quantitative agreement with the residual stress measured experimentally. The integrity of the machined surface will be controlled more efficiently if the cutting conditions during finishing are determined with the proper consideration of the surface generating process. 相似文献
63.
HiroyukiHoshino HiromitsuMurakami HideoYokota SatoshiSuda HidekiTsuge KoichiTerasaka ToshiakiWakabayashi 《材料热处理学报》2004,25(5):475-479
In quenching, the cooling uniformity is most important to diminish distortion occurring on work pieces. As a trial to accomplish uniform cooling, therefore, there exist various mixing methods of a quenchant and the quenchant circulation with an external pump has so far been the well accepted mixing method. However, this study proposes an advanced oscillation mixing method that can improve more the cooling uniformity in quenching. The proposed method includes a stirrer in oscillating motion, so that the simultaneous oscillating and mixing movements of the stirrer are considered to provide efecfively the uniform cooling characteristics for the quenchant. In comparison with the case of the circulation pump mixing, the investigation using the oscillation mixing method has demonstrated the following two experimental facts:(1) the short vapor blanket stage caused by the quick breakage of the oil vapor blanket and (2) the reduced variation of the quenching distortion. 相似文献
64.
Sun-Chan Jeong Ichiro Katayama Hirokane Kawakami Yutaka Watanabe Hironobu Ishiyama Nobuaki Imai Yoshikazu Hirayama Hiroari Miyatake Masao Sataka Satoru Okayasu Hiroyuki Sugai Shin-Ichi Ichikawa Katsuhisa Nishio Shinichi Mitsuoka Takamitsu Nakanoya Masahito Yahagi Takanori Hashimoto Kazunori Takada Mamoru Watanabe Tomoko Ishikawa Akihiro Iwase 《Journal of Phase Equilibria and Diffusion》2005,26(5):472-476
For the effective use of short-lived radioactive beams, soon to be available at the Tokai Radioactive Ion Accelerator Complex, the authors have developed a radiotracer method for diffusion studies in solids. The experimental test was performed by the measurement of the diffusion coefficients of Li in a sample of the compound βLiAl using an α-emitting radiotracer of 8Li (T1/2=0.84 s). It was found that the time-dependent yields of the α particles from the diffusing 8Li that was initially implanted in the sample could be used as a measure of the diffusivity of the tracer in a nondestructive way. The method was applied to measure the self-diffusion coefficients of Li in βLiGa, and for investigating how the Li diffusion in the Li ionic conductors is affected by the concentration of atomic defects (i.e., the existence of the atomic vacancies of Li and the defects in Ga sites that are replaced by Li). 相似文献
65.
Hiroyuki Sato 《Soft Computing - A Fusion of Foundations, Methodologies and Applications》2016,20(10):3803-3820
MOEA/D is one of the promising evolutionary algorithms for multi- and many-objective optimization. To improve the search performance of MOEA/D, this work focuses on the solution update method in the conventional MOEA/D and proposes its alternative, the chain-reaction solution update. The proposed method is designed to maintain and improve the variable (genetic) diversity in the population by avoiding duplication of solutions in the population. In addition, the proposed method determines the order of existing solutions to be updated depending on the location of each offspring in the objective space. Furthermore, when an existing solution in the population is replaced by a new offspring, the proposed method tries to reutilize the existing solution for other search directions by recursively performing the proposed chain-reaction update procedure. This work uses discrete knapsack and continuous WFG4 problems with 2–8 objectives. Experimental results using knapsack problems show the proposed chain-reaction update contributes to improving the search performance of MOEA/D by enhancing the diversity of solutions in the objective space. In addition, experimental results using WFG4 problems show that the search performance of MOEA/D can be further improved using the proposed method. 相似文献
66.
67.
Hiroyuki Sato Hernán Aguirre Kiyoshi Tanaka 《Annals of Mathematics and Artificial Intelligence》2013,68(4):197-224
In this work, we analyze variable space diversity of Pareto optimal solutions (POS) and study the effectiveness of crossover and mutation operators in evolutionary many-objective optimization. First we examine the diversity of variables in the true POS on many-objective 0/1 knapsack problems with up to 20 items (bits), showing that variables in POS become noticeably diverse as we increase the number of objectives. We also verify the effectiveness of conventional two-point and uniform crossovers, Local Recombination that selects mating parents based on proximity in objective space, and two-point and uniform crossover operators which Controls the maximum number of Crossed Genes (CCG). We use NSGA-II, SPEA2, IBEA ??+? and MSOPS, which adopt different selection methods, and many-objective 0/1 knapsack problems with $n=\{100,250,500,750,\mbox{1,000}\}$ items (bits) and m?=?{2,4,6,8,10} objectives to verify the search performance of each crossover operator. Simulation results reveal that Local Recombination and CCG operators significantly improve search performance especially for NSGA-II and MSOPS, which have high diversity of genes in the population. Also, results show that CCG operators achieve higher search performance than Local Recombination for m?≥?4 objectives and that their effectiveness becomes larger as the number of objectives m increases. In addition, the contribution of CCG and mutation operators for the solutions search is analyzed and discussed. 相似文献
68.
Ken-ichi Kohichi Hiroyuki Shiro Satoshi Hitoshi Atsushi 《Sensors and actuators. B, Chemical》2008,130(2):707-712
Pt-loaded metal oxides [WO3/ZrO2, MOx/TiO2 (MOx = WO3, MoO3, V2O5), WO3 and TiO2] equipped with interdigital Au electrodes have been tested as a NOx (NO and NO2) gas sensor at 500 °C. The impedance value at 4 Hz was used as a sensing signal. Among the samples tested, Pt-WO3/TiO2 showed the highest sensor response magnitude to NO. The sensor was found to respond consistently and rapidly to change in concentration of NO and NO2 in the oxygen rich and moist gas mixture at 500 °C. The 90% response and 90% recovery times were as short as less than 5–10 s. The impedance at 4 Hz of the present device was found to vary almost linearly with the logarithm of NOx (NO or NO2) concentration from 10 to 570 ppm. Pt-WO3/TiO2 showed responses to NO and NO2 of the same algebraic sign and nearly the same magnitude, while Pt/WO3 and WO3/TiO2 showed higher response to NO than NO2. The impedance at 4 Hz in the presence of NO for Pt-WO3/TiO2 was almost equal at any O2 concentration examined (1–99%), while in the case of Pt/WO3 and WO3/TiO2 the impedance increased with the oxygen concentration. The features of Pt-WO3/TiO2 are favorable as a NOx sensor that can monitor and control the NOx concentration in automotive exhaust. The effect of WO3 loading of Pt-WO3/ZrO2-based sensor is studied to discuss the role of surface W-OH sites on the NOx sensing. 相似文献
69.
Artificial Life and Robotics - In recent years, unspecified messages posted on social media have significantly affected the price fluctuations of online-traded products, such as stocks and virtual... 相似文献
70.
Mayu Muramatsu Yoshihisa Harada Takayuki Suzuki Hiroyuki Niino 《Advanced Composite Materials》2016,25(2):143-158
In this study, the correlation between the stress–strain behavior of a carbon fiber-reinforced plastic (CFRP) and the temperature at which the heat-affected zone (HAZ) is generated is investigated. First, CFRP ([?45/45]2s laminate) specimens were heated at several temperatures to induce thermal damage, i.e. a HAZ. Subsequently, tensile tests were conducted on the specimens with thermal damage. Then, microscopy and X-ray measurements were carried out to discuss the stress–strain responses from a microscopic viewpoint. The results of strain measurement during thermal treatment indicated that the strain increases with increasing temperature. The tensile tests showed that the CFRP specimens subjected to thermal damage during heating at a high temperature fractured in the ductile mode, whereas the fracture mode of the CFRP specimens with low-temperature thermal damage was discontinuous. Microstructure observation using X-ray tomography showed that the debonding between the carbon fibers and the resin matrix induced by heating to above the glass transition temperature was responsible for the continuous fracture mode. 相似文献