大港油田关家堡地区不同含油层系气测解释方法探讨

大港油田关家堡地区油气藏特征复杂，不同含油层系油气显示特征不同，气测录井解释符合率相对较低。针对这一情况，通过分析关家堡地区明化镇组、馆陶组和沙河街组的地质和气测显示特征，结合试油结论，提出不同含油层系相应的气测录井解释方法——TR与Wh（湿度比）气测解释法和三角形图板法，归纳总结了全烃及组分在不同层系的变化规律。应用实例表明，效果较好，对于复杂油气藏多层系油气层的解释评价具有一定的借鉴作用。     

液体静力称量法液体密度测量及其不确定度评定

介绍了液体静力称量法测量液体密度的原理并给出液体密度的计算公式,对影响测量结果的各种因素作了详细的分析,并对各个分量所引入的不确定度进行了数值计算,得出液体密度最终测量结果的合成标准不确定度.     

由碳五馏分合成甲基叔戊基醚工艺的研究

以催化裂化C_5馏分与工业甲醇为原料,D005型大孔强酸型阳离子交换树脂为催化剂,采用筒式膨胀床双反应器,考察了甲基叔戊基醚的合成工艺条件。一阶反应器的操作条件为：循环比为2：1,醇烯比为1.2：1,入口温度为70℃,空速为6 h~(-1),平均转化率为53.63%；二阶反应器的操作条件为：入口温度为50℃,空速为1.2h~(-1),平均转化率为71.32%,全调合方案可以使催化裂化汽油的辛烷值平均提高0.55个单位。     

Organic Electroluminescent Thin Film Using 8—hydroxyquinoline Zinc as Emitting Layer

Organic electroluminescent thin film using Znq2(Znq2) as the emitting layer material with structure of glass/ITO/Znq2/Al(cell) was fabricated.The V-I curve ,V-B curve and electroluminescent spectra of the cell were measured.Meanwhile the fluorescent spectra, excited spectra and absorption spectra of Znq2 with power and film states were also measured.     

激光结晶a-Si:H SOI离子注入和快速退火

本文对激光结晶a-Si∶H SOI结构砷注入和快速退火行为作了研究.a-Si∶H激光结晶有Lp-LCR,OD,FCR-2,FCR-1四个结晶区.用剖面电镜观察了结晶区的结构.扩展电阻测量表明Lp-LCR区中有两种扩散机制,即杂质在晶粒体内扩散和沿缺陷扩散.OD区中有三种扩散形式,除有上述两种以外,还有沿缺陷的扩散.首次比较了沿晶界和缺陷的扩散速度.     

致密低渗砂岩气藏压裂效果综合评价

依据川西洛带蓬莱镇组气藏地质、压裂及试井资料，通过定性及灰关联分析，结果表明压裂层段岩性、孔隙度及地应力特征是影响压裂效果的主要因素。根据试井解释理论，综合运用压前压后试井资料分析试井曲线形态特征及地层参数变化，动态认识压裂层段储渗特征，深入剖析评价气藏压裂效果，为气藏今后压裂选层、措施方案改进提供依据。研究方法对同类型气藏的科学管理开发具有一定的指导和借鉴意义。     

单晶钛酸铋纳米片的XPS和Raman特性

以Bi（NO3）3·5H2O和Ti（OC4H9）4为原料，NaOH为矿化剂，采用水热法制备了形貌规则的单晶Bi4Ti3O12纳米片。X射线衍射（XRD）结果表明，所合成的产物为正交相层状钙钛矿结构的Bi4Ti3O12。场发射扫描电子显微镜（FESEM）研究显示：样品是由大量边缘尺寸接近200nm，厚度约为15nm的片状结构组成。利用X射线光电子能谱（XPS）研究产物的化学组分和价态分布。室温拉曼光谱研究表明，Bi4Ti3O12纳米片的声子寿命和热稳定性低于相应的块体材料。     

Influence of phosphorus element on direct laser sintering of multicomponent Cu-based metal powder

This article presents a detailed investigation on the influence of the phosphorus element upon the laser sintering of a multicomponent Cu-based metal powder system consisting of Cu, Cu-10Sn, and Cu-8.4P. Powder systems containing 0, 10, 15, and 20 wt pct CuP were sintered in atmosphere at room temperature using the following optimal processing parameters: laser power of 350 W, scan speed of 0.04 m/s, scan line spacing of 0.15 mm, and layer thickness of 0.25 mm. It was found that the relative density of the sintered sample with 15 wt pct CuP increased by 24,4 pct as compared with the sample without phosphorus addition. A further increase in the CuP content (≥20 wt pct), however, resulted in a poor densification with a serious delamination. The exact metallurgical roles of the phosphorus element in the laser sintering process were addressed as follows. First, the phosphorus could prevent the sintering system from oxidation by forming CuPO₃, thereby improving the wetting characteristics and the sintering kinetics. Second, the phosphorus could decrease the surface tension of molten materials, leading to a successive transition from highly discontinuous sintered tracks to fairly coherent ones with increasing the phosphorus content. Third, the phosphorus could lower the melt viscosity, thereby improving the microstructural homogeneity of the laser-sintered samples.     

Pattern search algorithms for nonlinear inversion of high-frequency Rayleigh-wave dispersion curves

Inversion of Rayleigh wave dispersion curves is challenging for most local-search methods due to its high nonlinearity and to its multimodality. In this paper, we implemented and tested a Rayleigh wave dispersion curve inversion scheme based on GPS Positive Basis 2N, a commonly used pattern search algorithm. Incorporating complete poll and complete search strategies based on GPS Positive Basis 2N into the inverse procedure greatly enhances the performance of pattern search algorithms because the two steps can effectively locate the promising areas in the solution space containing the global minima and significantly reduce the computation cost, respectively.The proposed inverse procedure was applied to nonlinear inversion of fundamental-mode Rayleigh wave dispersion curves for a near-surface shear (S)-wave velocity profile. The calculation efficiency and stability of the inversion scheme are tested on three synthetic models and a real example from a roadbed survey in Henan, China. Effects of the number of data points, the reduction of the frequency range of the considered dispersion curve, errors in P-wave velocities and density, the initial S-wave velocity profile as well as the number of layers and their thicknesses on inversion results are also investigated in the present study to further evaluate the performance of the proposed approach.Results demonstrate that pattern search algorithms applied to nonlinear inversion of high-frequency surface wave data should be considered good not only in terms of accuracy but also in terms of the computation effort due to their global and deterministic search process.     

拉伸试验测量不确定度的研究

分析了拉伸试验中抗拉强度Rm的影响因素，对测量不确定度的主要分量进行量化，评定了Rm的相对测量不确定度，作为生产检验中评定测量不确定度的尝试，以便为用户提供钢材性能测量结果的不确定度。