用激光烧结法制备的SnO2薄膜的气敏性质

用溶胶-凝胶法制备SnO2前驱液,然后用提拉法分别在单晶Si和Al2O3基片表面制备出SnO2前驱膜,再用脉冲Nd:YAG激光烧结前驱膜使其转变为晶体SnO2薄膜.用XRD分析了单晶Si表面的SnO2薄膜,研究激光功率对SnO2薄膜相组成的影响.TEM观察表明,激光烧结后的薄膜SnO2颗粒均匀,直径约为10 nm.用激光烧结法制备的SnO2薄膜对浓度为1.80×10-4丙酮的最高灵敏度为30～40,明显高于用传统烧结法制备的SnO2薄膜的灵敏度.激光烧结能降低薄膜具有最高灵敏度的工作温度.     

Performance evaluation on a double‐layered satellite network

How to evaluate the performance of satellite networks is a prerequisite to the construction of satellite networks, and is also one of challenges in the researches on satellite networks. In this paper, generalized stochastic Petri net (GSPN) models are presented to carry out the performance analysis of a double‐layered satellite network. Firstly, the GSPN model of a double‐layered satellite network is simplified by proper analysis. Then, two sets of experiments are conducted to analyse the performance of the satellite networks, and show that the double‐layered satellite network outperforms single‐layered ones on the heavy traffic load. Finally, the feasibility and effectiveness of the proposed approach is verified by simulation experiments. Copyright © 2005 John Wiley & Sons, Ltd.     

饮用水中挥发性三卤甲烷(THM)_s测定方法的改进

本文使用吹扫捕集法来前处理水样,用带有电子捕获检测(ECD)的气相色谱仪来测定水中三卤甲烷(THM)_s。水样加标回收率在85%～115%之间,相对标准偏差在5%左右。实验结果表明,该法具有简单、快速、灵敏的特点。     

乙烯裂解炉辐射段炉顶密封结构优化设计

乙烯裂解炉的炉顶密封效果关系到装置的安全、稳定运行.针对现行的密封结构,进行了合理的技术改造和优化设计,并经实际投入使用,效果良好,也可进一步推广到类似的炉型上.     

胨冻样芽孢杆菌(Bacillus mucilaginosus)对烟草灰霉病菌(Botrytis cinerea)的抑制作用

本文首次报道胨冻样芽孢杆菌XDB1和D4B1对烟草灰霉病菌(Botrytis cinerea)的抑制作用。实验表明,XDB1和D4B1的发酵原液和无细胞提取物具有相同的抑菌效果,而经121℃处理30分钟后,抑菌活性丧失。D481菌株的抑菌活性高于XDB1,钾长石作为基质时的活性高于土壤矿物。但是,XDB1和D481对立枯丝核病菌(R..solani)、西瓜尖孢镰刀菌(F.oxysporum)、腐霉(Pythium sp)、小麦全蚀病菌(G.graminis)、烟炭疽病菌(C.gloeosporides)、烟草赤星病菌(A.alternata)、烟草黑胫病菌(P.nicotianae、串珠镰刀病菌(F.moniliforme)和水稻稻瘟病菌(P.grisea)无抑制作用。     

以硅氧烷醇锂为催化剂的氟硅生胶的合成

介绍了单体三氟丙基甲基环三硅氧烷通过硅氧烷醇锂催化剂聚合成氟硅生胶,讨论了不同催化剂及其用量,原料中水分含量、不同乙烯基含量对氟硅生胶分子量的影响.     

盐湖沉积储层孔隙结构特征及演化模式--以马王庙油田为例

盐湖沉积条件下的沉积环境及储集层特征等具有与淡水沉积不同的特征,通过对江汉盐湖盆地马王庙地区储层孔隙结构特征的研究,揭示了孔隙结构的宏观及微观特征.该区新沟咀组下段砂岩储层孔隙类型以粒间溶孔为主,喉道主要为片状、弯片状及点状喉道.Ⅱ、Ⅲ油组的物性比Ⅰ油组好,平面上孔隙分布具分区性.孔喉配置主要为大孔中喉,次为大孔粗喉及中孔中喉.孔隙结构受沉积环境及成岩作用的影响.以马36井Ⅱ油组砂岩为例,建立了孔隙演化定量模式.     

Crack length measurements with a potential drop method: A finite element simulation

A potential drop method, as used for estimations of crack lengths during three-point-beind experiments, is studied. The mechanical state is calculated using a finite element method. The deformed body obtained is used for a subsequent calculation of the electrostatic state. Calculations are performed for both two- and three-dimensional models. The material is assumed to be elastic, linearly hardening plastic and electrostatically linear. Large deformations are considered. Further, the non-linearity caused by the load, depending on the contact area between the cylinder on which the load is applied and the specimen, is considered. The increased contact area did not influence the mechanical state very much but had a direct impact on the electrostatic state. The changes in the potential drop recordings due to deformation and electrical current passing through the load cylinder were shown to be considerable. The study explains, at least partly, the experimental observations. A more reliable registration of crack growth initiation is the main outcome of the analysis.     

Optically tuned superconductive-dielectric resonators with whispering-gallery modes

An analytical method is presented for calculating the resonant frequency andQ-factor of a superconducting dielectric disk resonator operating in millimeter-wave regime with whispering-gallery mode. Resonant frequency shift due to the optical generation of quasi-particles in superconducting film is investigated as a function of photon flux. An optically tunable resonant frequency of about 500 MHz is estimated, and good agreement is found between numerical results and experimental ones.