异件共型的压铸模设计

阐述了把形状和主要壁厚差别很大的几种零件放在一个压铸模上同时成形的设计方法。     

组织蛋白酶C特异性荧光底物的合成和血清学分析应用

组织蛋白酶C是溶酶体半胱氨酸蛋白酶,源于免疫颗粒细胞.组织蛋白酶C作为近年来的研究热点,在于其为颗粒细胞炎症性丝氨酸蛋白酶的上游活化酶,在生理和病理过程中有着重要作用.通过研究设计并合成基于香豆素的荧光底物(CatC-AFC)来评估血清组织蛋白酶C的活性.结果表明,在特异性底物CatC-AFC与组织蛋白酶C反应后,荧光强度在非常短的时间内显著增加.酶动力学研究显示组织蛋白酶C以稳健的,线性的和时间依赖性的方式水解CatC-AFC.通过梯度稀释方法验证基于血清中组织蛋白酶C的活性测定,并且没有观察到干扰或自发荧光.基于血清中组织蛋白酶C活性的方差系数表明了良好的重现性.     

30%苄氨基嘌呤悬浮剂对芹菜生长和品质的影响

田间条件下研究了不同浓度苄氨基嘌呤悬浮剂对芹菜生长和品质的影响。结果表明,剂量浓度在60~120 mg/kg范围内均可提高芹菜的株高和产量,120 mg/kg剂量浓度处理对亩产量和株高的提高幅度达到了显著水平(P<0.05);药剂对芹菜安全性和品质分析结果表明,试验药剂30%苄氨基嘌呤悬浮剂各剂量浓度对芹菜均没有明显药害,对芹菜的干物质重量、维生素(Vc)和可溶性固形物含量均无显著影响。     

Study on the machinability of resulfurized composite free-cutting steels

The machinability of S, S-Ca, S-RE, and S-RE-Ca system resulfurized composite free-cutting steels were investigated, where RE is rare earths, mostly cerium. The experimental results showed that in the low cutting speed range (≤35 m/min), the S-RE system free-cutting steel had better machinability than the others and that the S-RE-Ca system free-cutting steel exhibited the best machinability at high cutting speeds. A protective layer capable of preventing diffusion wear was formed on the rake face of a P30 tool when S-RE-Ca system free-cutting steel was machined in the cutting speed range of 120 to 160 m/min.     

DIRECT OBSERVATION ON DISLOCATION AND STACKING FAULT CONFIGURATION OF Ni-BASE ALLOY CONTAINING 6.5% A1

对镍铝合金的位错与层错结构及其运动规律,进行了电子衍衬观察.主要结果如下:1.固溶处理不同淬火速度对缺陷组态有重大影响,在大的淬火速度下,观察到空位作三维聚集形成的有特征形貌的宏观孔洞.2.固溶处理加形变,普遍观察到位错塞积现象,存在着一个出现塞积群的临界形变量.提出了一个定义塞积位错列密度的新概念,用它来讨论材料的强度问题较为合理.3.讨论了形变试样的某些位错反应,对扩展位错的运动规律进行了动态观察.     

基于分层维的自由曲面反求建模技术研究

针对CMM测量数据的特点,提出了基于分层维的自由曲面建模技术,以分层维量作为分层依据进行数据分层,利用首尾判断法进行层内数据的排序,建立了大规模数据的拓扑关系.以此为前提, 研究并优化了NURBS求值快速算法,通过符号运算将B样条基函数描述为分段多项式的形式,通过分层维的设定来确定最小初始化数组,利用一个临时多项式存储中间计算结果,最终在大规模计算时进行的是多项式的求值,有效地加快了运算速度.经实例验证,本算法是准确可行的,满足工程实际需求.     

Investigation on gradient material fabrication with electron beam melting based on scanning track control

A new electron beam control system was developed in a general vacuum electron beam machine by assembling with industrial control computer, programmable logic control （PLC）, deflection coil, data acquisition card, power amplifier, etc. In this control system, scanning track and energy distribution of electron beam could be edited off-line, real-time adjusted and controlled on-line. Ti-Mo gradient material （GM） with high temperature resistant was fabricated using the technology of electron beam melting. The melting processes include three steps, such as preheating, melting, and homogenizing. The results show that the GM prepared by melting technology has fine appearance, and it has good integrated interface with the Ti alloy. Mo and Ti elements are gradually distributed in the inter.face of the gradient material. The microstructure close to the Ti alloy base metal is α ＋ β basket-waver grain, and the microstructure close to the GM is a single phase of β solid solution.     

高效液相色谱法测定止痛养胃软胶囊中延胡索乙素的含量

测定止痛胃软胶囊中延索乙素的含量,可用高效液相色谱法。选用甲醇—磷酸缓冲溶液(40∶60)为流动相,测定波长280nm。结果:延胡索乙素浓度在0.02140～1.37mg/mL范围内,与峰面积线性关系良好,y=(8.390×106)x+7.505×103(r=0.9997)。结论:该法操作简便、快捷、特异性强,可用于控制止痛养胃软胶囊的质量。     

TPR处理剂的研究

利用活性单体苯乙烯与氯丁橡胶、高苯乙烯热塑弹性体接枝聚合，所得产物稀释后用于ＴＰＲ（ＴｈｅｒｍａｌＰｌａｓｔｉｃＲｕｂｂｅｒ）粘接前的预处理，可明显提高剥离强度。     

The deposition of coke from methane on a Ni/MgAl2O4 catalyst

Temperature-programmed reaction techniques and Raman spectroscopy were used to characterize coke species deposited on a 5% Ni/MgAl₂O₄ catalyst for dry reforming of methane. The CH₄ temperature-programmed decomposition profiles showed that the ignited decomposition temperatures of CH₄ increased from 273 to 378 °C when MgAl₂O₄ replaced the catalyst support γ-Al₂O₃. The temperature-programmed oxidation, temperature-programmed hydrogenation and temperature-programmed CO₂ reaction profiles showed that there were three carbon species (i.e. C_α, C_β and C_γ) on the catalyst surface. Raman spectroscopy showed that C_γ was graphite-like carbon species, which was responsible for catalyst deactivation. The C_γ species was the most inactive species toward H₂ and O₂, while it was unexpectedly more active toward CO₂. The unique reactivity of CO₂ with different coke specie could be ascribed to the carbonate, bidentate and formate species formation on MgAl₂O₄ surface. These surface species enhanced the oxidation of C_γ species and thus contributed to the high stability of Ni/MgAl₂O₄ catalyst.