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151.
Polyester‐based polyurethane/nano‐silica composites were obtained via in situ polymerization and investigated by Fourier‐transform infrared spectroscopy (FTIR), or FTIR coupled with attenuated total reflectance (FTIR‐ATR), Transmission electron microscopy (TEM), atomic force microscopy (AFM), an Instron testing machine, dynamic mechanical analysis (DMA) and ultraviolet‐visible spectrophotometry (UV‐vis). FTIR analysis showed that in situ polymerization provoked some chemical reactions between polyester molecules and nano‐silica particles. FTIR‐ATR, TEM and AFM analyses showed that both surface and interface contained nano‐silica particles. Instron testing and DMA data showed that introducing nano‐silica particles into polyurethane enhanced the hardness, glass temperature and adhesion strength of polyurethane to the substrate, but also increased the resin viscosity. UV‐vis spectrophotometry showed that nano‐silica obtained by the fumed method did not shield UV radiation in polyurethane films. Copyright © 2003 Society of Chemical Industry 相似文献
152.
153.
XiaYinshui A.E.A.Almaini WuXunwei 《电子科学学刊(英文版)》2003,20(3):194-201
Using state assignment to minimize power dissipation and area for finite state machines is computationally hard.Most of published results show that the reduction of switching activity often trades with area penalty.In this paper,a new approach is proposed.Experimental results show a significant reduction of switching activity without area penalty compared with previous publications. 相似文献
154.
High-power 1320-nm wafer-bonded VCSELs with tunnel junctions 总被引:8,自引:0,他引:8
V. Jayaraman M. Mehta A.W. Jackson S. Wu Y. Okuno J. Piprek J.E. Bowers 《Photonics Technology Letters, IEEE》2003,15(11):1495-1497
A new long-wavelength vertical-cavity surface-emitting laser structure is described that utilizes AlGaAs-GaAs mirrors bonded to AlInGaAs-InP quantum wells with an intracavity buried tunnel junction. This structure offers complete wavelength flexibility in the 1250-1650 nm fiber communication bands and reduces the high free-carrier losses and bonded junction voltage drops in previous devices. The intracavity contacts electrically bypass the bonded junctions to reduce threshold voltage. N-type current spreading layers and undoped AlGaAs mirrors minimize optical losses. This has enabled 134/spl deg/C maximum continuous-wave lasing temperature, 2-mW room-temperature continuous-wave single-mode power, and 1-mW single-mode power at 80/spl deg/C, in various devices in the 1310-1340 nm wavelength range. 相似文献
155.
156.
Souheng Wu 《Polymer Engineering and Science》1992,32(12):823-830
The characteristic ratio C∞ and the entanglement molecular weight Me are two key molecular parameters that control melt viscoelasticity, solid mechanical (brittle/ductile) behavior, and adhesion of polymers. We show that the characteristic ratio C∞ and the entanglement molecular weight Me can be predicted from chemical structure by group additivity with uncertainties usually less than ~ 7% for C∞ and ~ 15% for Me, comparable with the accuracies of experimental values. 相似文献
157.
P Oroszlan S Wicar G Teshima S L Wu W S Hancock B L Karger 《Analytical chemistry》1992,64(14):1623-1631
This paper examines the retention behavior of recombinant DNA-derived human growth hormone (rhGH) in reversed-phase chromatography and its separation from the closely related N-methionyl variant (Met-hGH). It is first shown that retention for rhGH decreases with increasing column temperature when 1-propanol (1-PrOH) is used as organic modifier. On the other hand, retention increases with temperature when acetonitrile (CH3CN) is employed. The differences in behavior for the two organic modifiers could be related to conformational changes in the protein as determined by solution and adsorption intrinsic fluorescence spectroscopy. Specifically, desorption and elution of rhGH using 1-PrOH could be correlated with a solvent-induced conformational change, with retention decreasing with increasing temperature due to the increasing ease of structural alteration. On the other hand for CH3CN the increase in retention correlated with temperature rise was related to a partial structural change yielding a more hydrophobic species. In this case, a surface-driven process is suggested. The work then turned to the separation of rhGH and Met-hGH where it was found for both organic modifiers optimum separation occurred at 45 degrees C and pH 6.5. Separate studies revealed that during the conformational change Met-hGH appeared more hydrophobic than rhGH since protein-protein aggregation was observed at a lower 1-PrOH concentration. It is suggested that this hydrophobic difference, which was optimized under the conditions cited above, resulted in the separation. The study demonstrates the importance of conformational changes in retention behavior and separation of protein samples. 相似文献
158.
Uncertainty analysis and allocation of joint tolerances in robot manipulators based on interval analysis 总被引:1,自引:0,他引:1
Many uncertain factors influence the accuracy and repeatability of robots. These factors include manufacturing and assembly tolerances and deviations in actuators and controllers. The effects of these uncertain factors must be carefully analyzed to obtain a clear insight into the manipulator performance. In order to ensure the position and orientation accuracy of a robot end effector as well as to reduce the manufacturing cost of the robot, it is necessary to quantify the influence of the uncertain factors and optimally allocate the tolerances. This involves a study of the direct and inverse kinematics of robot end effectors in the presence of uncertain factors. This paper focuses on the optimal allocation of joint tolerances with consideration of the positional and directional errors of the robot end effector and the manufacturing cost. The interval analysis is used for predicting errors in the performance of robot manipulators. The Stanford manipulator is considered for illustration. The unknown joint variables are modeled as interval parameters due to the inherent uncertainty. The cost-tolerance model is assumed to be of an exponential form during optimization. The effects of the upper bounds on the minimum cost and relative deviations of the directional and positional errors of the end effector are also studied. 相似文献
159.
Zheng Jiao Minghong Wu Jianzhong Gu Zheng Qin 《IEEE sensors journal》2003,3(4):435-438
Zinc ferrite is a promising sensor material. In this paper, thin films of nanocrystalline zinc ferrite were deposited on alumina substrates by nebulization of a 0.01-M solution of a mixture of ZnCl/sub 2/ and FeCl/sub 3/ in ethanol (Zn:Fe=1:2) followed by pyrolysis and annealing in flowing air. The resulting films were characterized by X-ray diffraction and scanning electron microscopy, and the gas-sensing properties of as-deposited films were also investigated. 相似文献
160.
Chung-Bin Wu Bin-Da Liu Jar-Ferr Yang 《IEEE transactions on instrumentation and measurement》2003,52(3):780-784
In this paper, a simple fuzzy-based algorithm to remove the impulse noise from images is proposed. To achieve real-time applications, the proposed filter architecture, which combines fuzzy noise detection and noise filtering, is also designed. With low computational complexity, simulation results show that the proposed filters effectively remove the impulse noise. 相似文献