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81.
Mean-square dipole moment values of styrene/4-vinylpyridine (S4VP) copolymers determined at 25–60°C in 1,4-dioxane solutions were related to the microstructure of the chains. Data on the synthesis and dipole moments of S4VP copolymers were used to calculate the distribution of triad fractions and effective dipole moments of styrene, S-centred, and 4-vinylpyridine, V-centred, fractions in the copolymer chains. The relative magnitudes of the effective dipole moment values calculated for each type of triad reflect the effect of dipole–dipole interactions on these values. 相似文献
82.
Ilkay Orhan Murat Kartal Qamar Naz Asma Ejaz Gülderen Yilmaz Yüksel Kan Belma Konuklugil Bilge Şener M. Iqbal Choudhary 《Food chemistry》2007,103(4):1247-1254
Since Salvia species (Lamiaceae) have been recorded to be used against memory loss in European folk medicine, we herein examined in vitro anticholinesterase and antioxidant activities of 56 extracts prepared with petroleum ether, chloroform, ethyl acetate and methanol obtained from 14 Salvia species (Salvia albimaculata Hedge and Hub, Salvia aucheri Bentham var. canescens Boiss and Heldr, Salvia candidissima Vahl. ssp. occidentalis, Salvia ceratophylla L., Salvia cryptantha Montbret and Bentham, Salvia cyanescens Boiss and Bal., Salvia frigida Boiss, Salvia forskahlei L., Salvia halophilaHedge, Salvia migrostegia Boiss and Bal., Salvia multicaulis Vahl., Salvia sclarea L., Salvia syriaca L., Salvia verticillata L. ssp. amasiaca) growing in Turkey. The antioxidant activities were assessed by both chemical and enzymatic methods against 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical-scavenging and xanthine/xanthine oxidase (XO) system generated superoxide anion radical inhibition. Anticholinesterase effect of the extracts was tested against both acetylcholinesterase (AChE) and butyrylcholinesterase (BChE) at concentrations of 0.2 and 1 mg/ml using a microplate-reader assay based on the Ellman method. Most of the extracts did not show any activity against AChE at 0.2 mg/ml, while the chloroform extracts had noticeable inhibition against BChE between 47.7% and 74.7%. The most active extracts at 1 mg/ml for AChE inhibition were observed to be petroleum ether extract of Salvia albimaculata (89.4%) and chloroform extract of Salvia cyanescens (80.2%), whereas ethyl acetate extracts of Salvia frigida and Salvia migrostegia, chloroform extracts of Salvia candidissima ssp. occidentalis and Salvia ceratophylla, as well as petroleum ether extract of Salvia cyanescens were found to inhibit potently BChE (92.2%, 89.6%, 91.1%, 91.3%, and 91.8%, respectively). Particularly, the ethyl acetate and methanol extracts were observed to be highly active against both DPPH and XO. Our data indicates that nonpolar extracts of Salvia species for anticholinesterase activity and the polar extracts for antioxidant activity are worth further phytochemical evaluation for identifying their active components. 相似文献
83.
Yilmaz D Ekinci K Dilmacunal T Erbas S 《Journal of the science of food and agriculture》2011,91(9):1585-1590
BACKGROUND: Mechanization of Rosa damascena flower harvest is limited because of the asynchronous flowering period, the necessity for the harvest operation to take place in the early hour of the morning, and a lack of knowledge regarding the physical–mechanical properties of R. damascena. This study investigated the effect of harvesting hour on some physical–mechanical properties of R. damascena. RESULTS: The terminal velocity of the rose flower ranged from 4.00 to 2.38 m s?1. The highest picking force was found to be 6.29 N for the harvesting hour of 06:00 am. Tear forces of petal changed from 1.54 to 0.97 N for the harvesting hour of 06:00 am and 12:00 pm, respectively. The tension force of pedicel varied between 8.25 and 7.76 N. The weight of the rose flower was measured as an average of 1.61 and 1.50 g at 06:00 am and 12:00 pm, respectively. Horizontal and vertical projection areas of rose flowers were positively correlated with harvesting hour, with an R2 of 0.97 and 0.75, respectively. Results showed that there was a minor loss in colour for both inner and outer surfaces of petals. CONCLUSION: The results of physical–mechanical properties of R. damascena obtained from this study should be considered for the operation of flower harvest mechanization. Copyright © 2011 Society of Chemical Industry 相似文献
84.
M Demircin R Do?an M Güvener M Yilmaz A Celiker I Pa?ao?lu 《Canadian Metallurgical Quarterly》1998,49(11):941-944
Aortic root abscess, aneurysm of sinus Valsalva, severe aortic valve insufficiency, and a fragile aortic wall caused by infective endocarditis were found in a 10-year-old child. Aortic valve replacement was intended as a preoperative strategy, but one of modifications of Cabrol had to be used urgently because of aortic root rupture between right atrial and aortic connection just after pericardiotomy. 相似文献
85.
LL Hansen M Yilmaz J Overgaard J Andersen TA Kruse 《Canadian Metallurgical Quarterly》1998,58(10):2166-2169
Allelic loss, detected as a loss of heterozygosity (LOH) on the long arm of chromosome 16, is an early and frequent event in breast cancer. Despite this, the clinical significance of LOH on 16q has been very poorly studied. In this study, corresponding blood and tumor samples from 199 clinically well-characterized primary breast cancer patients were analyzed for LOH with the highly polymorphic microsatellite marker D16S511, located at 16q23.2-24.2. 61% of 168 informative tumors showed LOH. Univariate and multivariate analysis found a highly significant association between LOH at 16q23.2-24.2 and freedom from distant metastases, disease-free survival, and overall survival, respectively. No association was found with other clinical parameters such as menopausal status, tumor size, lymph node status, histopathology, and lymph node capsule invasion. This makes allelic loss of 16q23.2-24.2 an independent marker of good prognosis for primary breast cancer. 相似文献
86.
87.
Tülay Özcan Yilsay Lütfiye Yilmaz Arzu Akpinar Bayizit 《European Food Research and Technology》2006,222(1-2):171-175
The purpose of this research was to evaluate the texture of regular (12%), low fat (6%), and fat-free vanilla (0.5%) ice creams by sensory and instrumental analyses. The low fat and fat free ice cream were prepared using a whey protein based fat replacer (Simplesse ® 100) as the fat replacement ingredient. Two processing trials with continuous commercial-like process conditions were undertaken. Sensory analyses disclosed that ice creams containing 6% of fat replacer in place of or with milk fat had no demonstrable effect on vanillin flavour. While the sensory attributes of the low fat samples were comparable to the regular vanilla ice cream, the trained sensory panel rated the fat free ice cream to have lower viscosity, smoothness and mouth coating properties. Instrumentally determined apparent viscosity data supported the sensory data. Compared with the fat replacer, milk fat significantly increased the fresh milk and cream flavours of the ice cream. Results emphasized the importance of fat as a flavour modifier and the improvement of texture by addition of Simplesse ® 100. 相似文献
88.
Daubechies I. Yilmaz O. 《IEEE transactions on information theory / Professional Technical Group on Information Theory》2006,52(8):3533-3545
Beta-encoders with error correction were introduced by Daubechies, DeVore, Guumlntuumlrk and Vaishampayan as an alternative to pulse-code modulation (PCM) for analog-to-digital conversion. An N-bit beta-encoder quantizes a real number by computing one of its N-bit truncated beta-expansions where betaisin(1,2) determines the base of expansion. These encoders have (almost) optimal rate-distortion properties like PCM; furthermore, they exploit the redundancy of beta-expansions and thus they are robust with respect to quantizer imperfections. However, these encoders have the shortcoming that the decoder needs to know the value of the base of expansion beta, a gain factor in the circuit used by the encoder, which is an impractical constraint. We present a method to implement beta-encoders so that they are also robust with respect to uncertainties of the value of beta. The method relies upon embedding the value of beta in the encoded bitstream. We show that this can be done without a priori knowledge of beta by the transmitting party. Moreover the algorithm still works if the value of beta changes (slowly) during the implementation 相似文献
89.
Crystallization kinetics of basalt glass 总被引:2,自引:0,他引:2
The crystallization behaviour of basalt glass at elevated temperatures was studied using glass samples prepared by melting the natural basalt rock from the Thrace region of Türkiye. DTA and XRD analysis revealed the crystallization of augite [(Ca Fe Mg) SiO3 at 800 °C. The kinetics of crystallization of augite were studied by applying the DTA measurements carried out at different heating rates and the activation energies of crystallization and viscous flow were measured as 238 kJ mol−1 and 413 kJ mol−1, respectively. The resultant basalt glass-ceramic revealed very fine and homogeneous microstructure. 相似文献
90.
Yilmaz Tokad 《Dynamics and Control》1992,2(1):59-82
In the formulation of equations of motion of three-dimensional mechanical systems, the techniques utilized and developed to analyze the electrical networks based on linear graph theory can conveniently be used. The success of this approach, however, relies on the availability of a complete and adequate mathematical model of the rigid body valid in the three-dimensional motion. This article is devoted to the derivation of such a mathematical model for the rigid body as a (k + 1)-port component. In this derivation, the dynamic properties of the rigid body are automatically included as a consequence of the analytical procedures used in the article. In this model, a general form of the terminal equations is given. In many applications, however, its special form, also given in this article, is used. 相似文献