Characterization method of thermomechanical parameters for microelectronic materials

Reliability of thermomechanical simulations is critically linked to the accuracy of the mechanical properties that govern the behaviour of structure, like Young's modulus (E) and coefficient of thermal expansion (CTE). For many cases, the values found in literatures are dealing with bulk properties without detailed information on temperature effects. To address such issues, it is necessary to measure the materials parameters as a function of temperature. The measurement of CTE is usually accomplished by evaluating the thermal deflections of a subjected material layer deposited on a substrate, providing that E is known at a specific temperature of experiment. A bilayer method, based on theory of elasticity, is proposed to determine both E and CTE for a given temperature with a good resolution. This paper presents the theoretical analysis, the design and process of the microsystem test structures, and the main calculation results.     

Vicarious calibration experiment in support of the Multi-angle Imaging SpectroRadiometer

On June 11, 2000, the first vicarious calibration experiment in support of the Multi-angle Imaging SpectroRadiometer (MISR) was conducted. The purpose of this experiment was to acquire in situ measurements of surface and atmospheric conditions over a bright, uniform area. These data were then used to compute top-of-atmosphere (TOA) radiances, which were correlated with the camera digital number output, to determine the in-flight radiometric response of the on-orbit sensor. The Lunar Lake Playa, Nevada, was the primary target instrumented by the Jet Propulsion Laboratory for this experiment. The airborne MISR simulator (AirMISR) on board a NASA ER-2 acquired simultaneous observations over Lunar Lake. The in situ estimations of top-of-atmosphere radiances and AirMISR measurements at a 20-km altitude were in good agreement with each other and differed by 9% from MISR measurements. The difference has been corrected by adjusting the gain coefficients used in MISR standard product generation. Data acquired simultaneously by other sensors, such as Landsat, the Terra Moderate-Resolution Imaging SpectroRadiometer (MODIS), and the Airborne Visible and Infrared Imaging Spectrometer (AVIRIS), were used to validate this correction. Because of this experiment, MISR radiances are 9% higher than the values based on the on-board calibration. Semiannual field campaigns are planned for the future in order to detect any systematic trends in sensor calibration.     

Dynamic and equilibrium swelling of DVB-crosslinked polystyrene particles

The dynamic and equilibrium swelling behavior of polystyrene microparticles crosslinked with divinyl benzene was investigated in methyl ethyl ketone and cyclohexane. The dynamic studies gave new information about the mechanism of penetrant transport in this polymer. The equilibrium studies were used to determine important parameters of the crosslinked structure of these systems, including the average molecular weight between crosslinks, M?_c     

Dynamic mechanical properties of some polyurethane-acrylic copolymer interpenetrating polymer networks

Dynamic mechanical properties have been investigated for interpenetrating-network systems based on polyol-cured polyurethanes (PU) and 2 to 1 n-butyl acrylate-n-butyl methacrylate (Ac) networks. The systems were formed simultaneously (SIN) from all of the precursors and reactants for both networks in the same vessel, and sequentially (SIPN) by swelling a precured PU with the reactants that will form the Ac network. If the Ac network is formed after gelation of the PU, the IPNs are transparent and appear to have single T (tan δ_max) between those of the homonetworks; visible-phase separation occurs if the Ac is intentionally polymerized prior to PU gelation. Damping curves were lower and broader and the T (tan δ_max) and rubber moduli were higher for the SIN than for the SIPN systems. Up to 65 percent Ac, the T (tan δ_max) data for both SIN and SIPN fit the Gordon-Taylor equation if a T (tan δ_max) for the Ac homonetwork 7°C higher than observed is used, suggesting a higher crosslink density for the Ac network under these conditions. The differences in properties of the SIN and SIPN are assumed to be dependent on sample homogeneity and upon the presence of a tin catalyst in the SIN preparation. This can result in limited Ac-network formation and consequent phase separation before PU gelation has occurred, and the catalyst may also increase the extent of interaction, such as grafting or hydrogen-bond formation between the networks.     

Neutron-activation determination of elements with overlapping resonances in neutron-absorption cross sections

Translated from Atomnaya Énergiya, Vol. 66, No. 6, pp. 423–424, June, 1989.     

Use of166mHo for calibration of gamma-ray spectrometers with semiconductor detectors

Translated from Atomnaya Énergiya, Vol. 67, No. 3, pp. 215–216, September, 1989.