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991.
Guoqiang Yi Bingchu Mei Weiwei Li Jinghong Song Zuodong Liu Zhiwei Zhou Liangbi Su 《Journal of the American Ceramic Society》2020,103(1):279-286
Pr3+, Gd3+ co-doped SrF2 transparent ceramic, as the potential material for visible luminescent applications, was prepared by hot-pressing of precursor nanopowders. The microstructure, phase compositions, and in-line transmittance, as well as the photoluminescence properties were investigated systematically. Highly optical quality Pr,Gd:SrF2 transparent ceramic with nearly pore-free microstructure was obtained at 800°C for 1.5 hours. The average in-line transmittance of the x at.% Pr, 6 at.% Gd:SrF2 (x = 0.2, 0.5, 1.0, 2.0) transparent ceramics reached to 87.3 % in the infrared region. The photoluminescence spectra presented intense visible light emissions under the excitation of 444 nm, the main intrinsic emission bands located at 483 and 605 nm, which were attributed to the transitions of Pr3+: 3P0 → 3H4 and 1D2 → 3H4, respectively. With the co-doping of Gd3+ ions, the emission intensity of the Pr:SrF2 transparent ceramic was greatly enhanced. All the emission bands of x at.% Pr, 6 at.% Gd:SrF2 transparent ceramics exhibited the highest luminescence intensity with the 1.0 at.% Pr3+ doping concentrations, whereas the lifetimes decreased dramatically with the Pr3+ doping contents increasing from 0.2 to 2.0 at.% due to its intense concentration quenching effect. The 1 at.% Pr, 6 at.% Gd:SrF2 transparent ceramic is a promising material for visible luminescent device applications. 相似文献
992.
Lei Xing Yuanxiang Xu Željko Penga Qian Xu Huaneng Su Weidong Shi Frano Barbir 《American Institute of Chemical Engineers》2020,66(6):e16957
An easily machined novel flow field with controllable pressure gradient across adjacent channels was designed and a two dimensional, across-the-channel, two-phase model was developed to study the gas transport and water removal of the novel configuration. The effect of channel-rib width ratio, GDL thickness and pressure gradient on the profiles of oxygen concentration and water saturation within the GDL were investigated. Special attention was paid to the mechanisms of the promoted mass transport and water removal rates under a pressure gradient. The model was validated by experiments with various channel-rib ratios and GDL thicknesses at different operating pressure. The results revealed that, oxygen concentration was increased, and the water saturation was reduced under the rib with a pressure gradient generated across the adjacent channels. The optimal pressure gradient is between 0.1 to 0.2 atm for the studied channel geometry and configuration. The mechanisms of the improved cell performance were elucidated. 相似文献
993.
Yiguang Jiang Benxue Jiang Nan Jiang Dapeng Jiang Jiang Li Liangbi Su Long Zhang 《Journal of the American Ceramic Society》2020,103(10):5808-5812
Er3+-doped CaF2 transparent ceramics are promising mid-infrared gain materials because of their utra-low phonon energy as well as excellent physical, chemical, and optical properties. However, existing hot-pressed and hot-formed CaF2 ceramics are very difficult to be used in practical applications due to residual pores and weak polycrystallization, respectively. Here, we developed the high quality Er3+-doped CaF2 transparent polycrystalline ceramic by single crystal ceramization. The sample exhibits obvious polycrystalline structure, good mechanical properties, perfectly transmittance, and excellent mid-infrared performance, which provides significant and wide-ranging opportunities for advanced mid-infrared gain materials. 相似文献
994.
Hong Fang Lihai Wang Weijie Kuai Juan Du Guicheng Jiang Xiaoyan Lu Minglei Zhao Chunming Wang Wenbin Su Limei Zheng Chunying Wang Chunlei Wang 《Journal of the American Ceramic Society》2020,103(5):3257-3264
Domain wall motions mainly affect all kinds of properties of ferroelectric materials, such as piezoelectricity, dielectric response, and mechanical loss, and the extrinsic contributions associated with domain wall motions have always been an important issue. In this study, the reversible and irreversible extrinsic contributions to the dielectric properties of [011]C-oriented 0.27Pb(In1/2Nb1/2)O3-0.46Pb(Mg1/3Nb2/3)O3-0.27PbTiO3:Mn single crystals have been extracted by the Rayleigh analysis. We found that in the unpoled samples, the extrinsic contributions of reversible and irreversible domain wall motions to dielectric properties significantly reduced, whereas after poling, only the irreversible extrinsic contribution decreased. The pinning effect in the 2R domain structure is much weaker than that in the 4R domain structure, leading to the low enhancement of Qm and a slight decrease in piezoelectricity caused by acceptor doping in 2R domain structure. This study explores the domain wall dynamics of acceptor-doped single crystals and mainly guides on further performance optimization in PbTiO3-based relaxor single crystals. 相似文献
995.
The carbon fiber/(carbon nanotubes/polyetherimide)/poly ether ether ketone (CF/(CNTs/PEI)/PEEK) laminates are prepared by inserting carbon nanotubes/polyetherimide (CNTs/PEI) interleaves into interlaminar region. The mechanical properties and electrical conductivities of the developed laminates are evaluated. The results indicate that the interlaminar shear strength and flexural strength of CF/(CNTs/PEI)/PEEK laminates are increased by 42.9% and 24.7%, after inserting CNTs2.91/PEI interleaves, respectively. The cross-sectional images of laminates after mechanical tests verify strong fiber-resin adhesion by scanning electron microscope observation. The pertinent mechanism responsible for the improvement of mechanical properties is mechanical interlocking effect of CNTs. After incorporating CNTs/PEI interleaves, the electrical conductivity of laminates is markedly improved due to the formation of conductive pathway. This work suggests that this method is compatible with the preparation process of thermoplastic composites. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 137, 48658. 相似文献
996.
998.
López-Vásquez A. Suárez-Escobar Andrés López-Suárez F. E. 《Topics in Catalysis》2020,63(11-14):1325-1335
Topics in Catalysis - Black sand from coastal deposits composed by a mixture containing oxides (Fe2O3, TiO2, SiO2, ZrO2, MnO, Al2O3, etc.) and metals (V, Cr, Ni, Sr, Ce, etc.). Both this mineral,... 相似文献
999.
Meihua Hu Ning Bi Mingming Liu Shangsheng Li Taichao Su 《International Journal of Applied Ceramic Technology》2020,17(4):1629-1635
TiB2–B4C composites were in situ synthesized and consolidated by high pressure synthesis method from a mixture of TiC and B powders at the pressure and temperature of 5.0 GPa and 1500℃-1900℃. The phase composition, microstructure, density, hardness, thermal conductivity, and electrical resistivity of TiB2–B4C composites were analyzed. As the increase in the synthesis temperature, the products were TiB2 and B4C phases and that crystallinity improved. TiB2–B4C composites were dense without obvious pores. TiB2–B4C composites synthesized at 1800℃ obtained the optimized performance, including the relative density of 98.2%, the Vickers hardness of 31.7 ± 1.2 GPa with the load of 9.8 N, the thermal conductivity of 30.3 ± 0.7 W/(m K), and the electrical resistivity of 3.3 × 10−3 Ω cm, respectively. The grain size of the TiB2–B4C composites changed with the increase in synthesis temperature, leading to the changes in hardness, thermal conductivity, and electrical resistivity. 相似文献
1000.
为高效充分利用山西某斑岩型金矿资源,采用矿物定量分析仪(MLA)、光学显微镜、电子显微镜(电镜)等测试手段进行工艺矿物学特性研究。主要开展原矿矿块和-0.074 mm含量占60%细度浮选给矿的详尽矿物学研究。结果表明,金矿物产出形式主要为含银自然金、银金矿、自然金,主要金属矿物为黄铁矿、闪锌矿、方铅矿和微量黄铜矿,金属矿物总量少,达不到可回收边界工业品位,脉石矿物主要为长石、石英、白云母等硅酸盐矿物。对金的化学物相、金在矿样中的嵌布特征和嵌布粒度的配分测试,并评价重选、浸出、浮选三种选冶方法的可回收性,确定采用浮选的工艺回收效果较佳,金浮选理论回收率约93.78%。 相似文献