Synthesis and characterization of poly (linoleic acid)-g-poly(methyl methacrylate) graft copolymer with applying in Au/PLiMMA/n-Si diode

Poly (linoleic acid)-g-poly(methyl methacrylate) (PLiMMA) graft copolymer was synthesized and characterized. PLiMMA graft copolymer was synthesized from polymeric linoleic acid peroxide (PLina) possessing peroxide groups in the main chain by free radical polymerization of methyl methacrylate. Later, PLiMMA was characterized by proton nuclear magnetic resonance (¹H NMR), gel permeation chromatography (GPC), thermal gravimetric analysis (TGA) and differential scanning calorimetry (DSC) techniques. Furthermore, Au/PLiMMA/n-Si diode was fabricated for the purpose of investigating PLiMMA׳s conformity in diodes. The main electrical characteristics of this diode were investigated using experimental current–voltage (I–V) measurements in dark and at room temperature. Obtained results, such as sufficiently high rectifying ratio of 4.5×10⁴, indicate that PLiMMA is a promising organic material for electronic device applications.     

离子交换法合成三氨基胍叠氮酸盐

三氨基胍叠氮酸（ＴＡＺ）分子中的含氮量高达８５．７％，燃烧分解时不仅－Ｎ３可释放３６７ｋＪ／ｍｏｌ的键能，而且放出大量的氮气，是一个提高比冲，降低燃烧温度的理想的推进剂两组分之一。     

工业CT技术在无损检测炸药部件中的应用综述

综述了美国能源部的有关单位将工业ＣＴ技术用于高能炸药无损检测的研究状况，劳伦斯利弗莫尔国家实验室（ＬＬＮＬ）洛斯阿拉莫斯国家实验室（ＬＡＮＬ）和潘台克斯工厂（ＰａｎｔｅｘＰｌａｎｔ）在这方面做的大量工作，包括ＣＴ机的建造，实验方法的制定和图像的重建等。测试样品有ＰＢＸ－９５０２，ＰＢＸ－９５０１和ＬＸ－１０－２炸药的药饼和半球，对ＣＴ技术在无损检测高能炸药方面的实用性和优越性作了评价。     

Blind estimation of the PN sequence in lower SNR DS-SS signals with residual carrier

This paper presents a method of singular value decomposition (SVD) plus digital phase lock loop (DPLL) to solve the difficult problem of blind pseudo-noise (PN) sequence estimation in low signal to noise ratios (SNR) direct sequence spread spectrum (DS-SS, DS) signals with residual carrier. Of course, the method needs to know the parameters of DS signal, such as the period and code rate of PN sequence. Firstly, the received signal is sampled and divided into non-overlapping signal vectors according to a temporal window, whose duration is two periods of PN sequence. Then, an autocorrelation matrix is computed and accumulated by the signal vectors one by one. The PN sequence with residual carrier can be estimated by the principal eigenvector of this autocorrelation matrix. Furthermore, a DPLL is used to deal with the estimated PN sequence with residual carrier, it estimates and tracks the residual carrier, removes the residual carrier in the end. Theory analysis and computer simulation results show that this method can effectively realize the PN sequence estimation from the input DS signals with residual carrier in lower SNR.     

变形镜交连值的优化分析

关于优化光波控制,自适应光学校正是至关重要的一个环节,可用于改善激光光束质量及校正光束在传输过程中气流引起的波前畸变等。变形镜是其核心器件,而交连值是影响变形镜校正精度的关键因素。针对变形镜实际使用时需要对致动器进行一定的约束,利用带约束的最小二乘法,分析了在一定约束条件下交连值变化对变形镜校正精度及控制稳定性的影响。以Zernike像差和以大气湍流模型构造的像差为校正对象,寻找校正效果最好的交连值。结果表明各阶Zernike像差对应的最优交连值差异较大,最优交连值主要分布在15%～35%之间。从控制误差引起的校正效果变化的方面考虑,对正方形致动器排布的最优交连值位于15%～25%区域。     

激光-电弧复合焊接过程中高频干扰的消除

激光-电弧复合焊接过程中,由于引孤产生的高频干扰了激光器的控制系统,造成了激光和电弧不能实现复合焊接.通过分析研究高频引弧对焊接电源和激光器的干扰途径,采取相应的措施,有效地消除了高频干扰问题,成功实现了激光和电弧之间的复合焊接.     

Growth and characterization of indium doped zinc oxide films sputtered from powder targets

Indium doped Zn O films were grown on quartz glass substrates by radio frequency magnetron sputtering from powder targets. Indium content in the targets varied from 1at% to 9at%. In doping on the structure, optical and electrical properties of Zn O thin films were studied. X-ray diffraction shows that all the films are hexagonal wurtzite with c-axis perpendicular to the substrates. There is a positive strain in the films and it increases with indium content. All the films show a high transmittance of 86% in the visible light region. Undoped Zn O thin film exhibits a high transmittance in the near infrared region. The transmittance of indium doped Zn O thin films decreases sharply in the near infrared region, and a cut-off wavelength can be found. The lowest resistivity of 4.3×10~(-4) Ω·cm and the highest carrier concentration of 1.86×10~(21) cm~(-3) can be obtained from Zn O thin films with an indium content of 5at% in the target.     

OLE DB提供程序的开发

OLE DB提供程序广泛用作Web数据库等应用程序的数据源,分析了OLE DB提供程序的结构,通过具体例子说明OLE DB提供程序的开发方法。     

像增强器高压倍压电路的设计与仿真研究

新一代像增强器正在不断朝着微型化的方向发展,其中一个关键技术是产生高达6000V的高压微型电源模块,而选择合适的电路元件参数使模块微型化和性能提升.根据实际像增强器对电源系统的要求,从理论出发,结合工作实践,应对高压倍压产生电路进行数学建模,通过计算机仿真分析高压倍压电路的暂态工作过程,得出了电路的交流输入信号频率、倍压电容和输出负载等对倍压电路输出特性的影响,为设计高性能微型化像增强器电源提供依据.     

双酚A型聚碳酸酯快速拉伸过程的分子动力学模拟

本文采用用分子动力学方法研究了双酚A型聚碳酸酯的快速拉伸过程.采用COMPASS力场和NPT系综研究了应力应/变关系、能量/应变关系等.应力-应变曲线的研究结果显示,前"屈服点"和后"屈服点"分别为0.14和0.17,应变≤0.05为"弹性区域".0.14<ε_(xx)<1.05的区域为"塑性区域",ε_(xx)>1.05属于"硬化"区.能量-应力关系的研究结果显示,在应力-应变呈线性关系的"弹性区域",体系的总势能及各势能分量随应变增大发生不规则的波动.为了从能量的角度解释PBC-PC在外部拉伸条件下的应变情况,本文还研究了体系总能量与各能量分项,与应变的关系,对链结构与能量分项的关系进行了讨论.