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1.
Organosilicone thin films have been deposited by plasma polymerization (pp) in a plasma enhanced chemical vapor deposition (PECVD) system using hexamethyldisilazane (HMDSN:C6H19Si2N) as a monomer precursor, at different biases of the stainless-steel substrate holder. The substrate bias affected film thickness, surface morphology, chemical composition and photoluminescence (PL) emission. For a negatively biased substrate, it is found that the film thickness is the minimum, while the porosity and PL emission are the maximum. For a positively biased substrate, the thickness and the ratio of Si/N are the maximum which correspond to a blue shift of the PL emission in comparison with the case of non-biased grounded substrate. In addition, the characterization of the plasma using a single cylindrical Langmuir probe has been performed to obtain information about both the electron density and the positive ion energy, where it can be concluded that the ion energy plays a major role in determining film thickness. 相似文献
2.
Hydrodynamics and structure of two-phase flow in the bubbling regime in small-diameter tubes 总被引:1,自引:0,他引:1
Experimental data on the true gas void fraction in a vertical tube under the bubbling flow regime are presented. A generalization of these data on the basis of the drift flow model of Zuber with the distribution parameter C 0 = 1.2 and the weighted average gas velocity u 2j = 0.16 m/s is given. The results of assessing the parameters of the downcoming flow of the fluid in the near wall zone are shown. 相似文献
3.
A full-scale ATHLET system model for the Syrian miniature neutron source reactor (MNSR) has been developed. The model represents all reactor components of primary and secondary loops with the corresponding neutronics and thermal hydraulic characteristics. Under the MNSR operation conditions of natural circulation, normal operation, step reactivity transients and reactivity insertion accidents have been simulated. The analyses indicate the capability of ATHLET to simulate MNSR dynamic and thermal hydraulic behaviour and particularly to calculate the core coolant velocity of prevailing natural circulation in presence of the strong negative reactivity feed back of coolant temperature. The predicted time distribution of reactor power, core inlet and outlet coolant temperature follow closely the measured data for the quasi steady and transient states. However, sensitivity analyses indicate the influence of pressure form loss coefficients at core inlet and outlet on the results. The analysis of reactivity accidents represented by the insertion of large reactivity, demonstrates the high inherent safety features of MNSR. Even in case of insertion of total available cold excess reactivity without scram, the high negative reactivity feedback of moderator temperature limits power excursion and avoids consequently the escalation of clad temperature to the level of onset of sub-cooled void formation. The calculated peak power in this case agrees well with the data reported in the safety analysis report. The ATHLET code had not previously been assessed under these conditions. The results of this comprehensive analysis ensure the ability of the code to test some conceptual design modifications of MNSR's cooling system aiming the improvement of core cooling conditions to increase the maximum continuous reactor operation time allowing more effective use of MNSR for irradiation purposes. 相似文献
4.
Influence of cobalt and nickel sorption on the texture of crystalline α-titanium phosphate 总被引:1,自引:0,他引:1
M. Kassem 《Powder Metallurgy and Metal Ceramics》2012,51(1-2):121-127
5.
The dynamic response of an organic bulk heterojunction photodiode to small changes in applied bias or light intensity is investigated as function of the intensity of a constant background illumination by means of photoimpedance and transient photocurrent measurements. For bias voltages close to the open circuit voltage we find that the response timescale with the square root of the light intensity. The results can be quantitatively explained in terms of a space charge limitation on the photocurrent as predicted by Goodman and Rose (J. Appl. Phys. 42, 2823 (1971)). The relaxation time of the diode at open circuit corresponds to the lifetime of the slowest charge carrier in the diode. This relaxation time is determined by the dielectric constant and the smallest of the two carrier mobilities in the bulk heterojunction. This illustrates the importance of balanced carrier mobilities for obtaining diodes with fast response time at low bias for e.g. imaging arrays. 相似文献
6.
Fluorinated amorphous carbon (a-C:F) thin films are deposited on both flat silicon and porous silicon (PS) surfaces via laser ablation of a polished polytetrafluoroethylene (PTFE). Porous silicon (PS) is prepared by anodic etching of p-type silicon wafers in HF based solution. The film deposited on the flat silicon surface exhibits a highly hydrophobic state with water contact angle (WCA) of ~ 146°. In comparison, the surface of film deposited on PS layer shows a roll-off superhydrophobic state, where the water droplet is seen to roll off without wetting its surface with contact angle hysteresis of ~ 4.5°. Micro-Raman results show that the graphite domain of the film deposited on PS has higher disorder level and lower average gain size. The effect of substrate porosity on chemical composition of deposited films has been investigated by using both Fourier transform infrared (FTIR) and X-ray photoelectron spectroscopy (XPS). It is found that the porous substrate improves the incorporation of the fluorine into the film. Atomic force microscopy (AFM) results revealed that the film deposited on PS has higher surface roughness and lower grain size as compared to the film deposited on flat silicon surface. 相似文献
7.
Silicon - This study reports the effect of ageing on plasma polymerized hexamethyldisiloxane (pp-HMDSO) thin films properties during 90 days storage in the atmosphere. The monitoring of... 相似文献
8.
Oxidative solution polymerization of aniline hydrochloride onto electrospun nanofibers mats of polylactic acid: Preparation method and characterization
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Mazen Al‐Jallad Yomen Atassi Eskandar Mounif Matthieu Aressy Abbas Tcharkhtchi 《应用聚合物科学杂志》2015,132(11)
In this work, we present the preparation of polylactic acid (PLLA)/polyaniline (PANI) conductive composite nanofibers mats. They are prepared by bulk oxidative solution polymerization of PANI onto electrospun non‐woven fibers mats of PLLA. The PANI ratio in the composite is about 70%w/w. Scanning electron microscopy (SEM) shows that PLLA nanofibers are randomly oriented, beads free with diameters of 186 ± 85 nm, The PLLA/PANI composite nanofibers diameter values are 518 ± 128 nm with a good adherence between PANI and PLLA nanofibers. DSC and XRD measurements reveal an amorphous structure of the electrospun PLLA fibers due to the rapid evaporization of the solvent. FTIR and UV–vis spectra reflect good mutual interactions between PANI and PLLA chains. The DC‐conductivities ( ) far better than other published ones for similar composites prepared by bulk oxidative solution polymerization of PANI onto other electrospun nanofiber mats or with electrospun nanofibers from a solution mixture of PLLA and PANI. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 41618. 相似文献
9.
Current–voltage characteristics of ZnO/CdS/CuGaSe2 single crystal solar cells measured at room temperature are investigated depending on illumination intensity. The characteristics can be described using the two-diode model, indicating two current transport mechanisms acting in the cells. The first and dominant mechanism is recombination of carriers at the interface between CdS and CuGaSe2. The second one is recombination in the depletion region, which has been found to have a small effect on the solar cell photovoltaic performance. Both the diode ideality factor and the saturation current density of the dominant diode increase under illumination. A model based on interface recombination can explain these results. This model allows the estimation of diffusion voltage, capture cross-section of holes at the interface and mobility of electrons in the CdS layer. 相似文献
10.
S. Alhajali M.H. Kharita B. Naoom S. Yousef M. AlNassar 《Progress in Nuclear Energy》2009,51(2):374-377
Many elements in reactor shielding concrete become radioactive due to interaction with neutrons during the operation of a nuclear reactor. These radioactive elements will build up over the time due to (n,γ) reaction and contribute to the radioactive waste during decommissioning of the reactor, they will increase the dose from the inner part of the biological shielding (concrete) surrounding a nuclear reactor during maintenance works within reactor containment, and their effect should be taken in the calculations of the dose behind the concrete shield.Six mixtures of local ordinary and special shielding concretes have been investigated in this study. Their compositions were determined using X-ray diffraction and neutron activation analysis using the Syrian Miniature Neutron Source Reactor (MNSR) and consequently the dose rates.Based on the results of the analyses and comparing to the published limits in the references, it has been found that 60Co, 152Eu, 154Eu and 134Cs will be the most effective radioactive nuclides existing in the local concrete, but Dolomite aggregates contain the minimum limits of them and it has been found that Fe, Mg, and Ti the major elements existing in the local concrete. 相似文献