Mechanical alloying in the Al-Bi alloy system

Mechanical alloying (MA) was carried out to investigate the MA behaviour of the immiscible Al-10, 30 at % Bi alloys. After the MA processing, the Al and Bi were finely and homogeneously alloyed. The Bi crystallite size decreased to 25 nm and 30 nm in the Al-10 at % Bi and Al-30 at % Bi alloys, respectively. By increasing the MA time, the hardness increased up to a value of 80 H _v, which is larger than that obtained from the rule of mixtures. The lattice parameter of Bi decreased by about 0.27%, which shows the formation of a non-equilibrium hcp Bi super-saturated solid solution. The extended solubility of Al in Bi was 1.9% in the Al-30 at % Bi alloy. Due to the extended solubility, depression of the melting temperature of hcp Bi was confirmed in the mechanically alloyed Al-Bi alloys. The maximum depression in the temperature was about 10 K. The measured values corresponded well with those estimated from the extrapolation of the solidus line.     

A method for the preparation of PMMA-SiO2 nanocomposites with high homogeneity

It is possible to optimize the performance of the inorganic-organic composites dispersing the inorganic component in the organic matrix on a nanomiter length scale. If dry the inorganic phase cannot be intimately dispersed during the incorporation in the matrix. When the particle surface is organically modified, and the incorporation is made starting from a liquid dispersion (particles in polymer solution), the resulting composites exhibit an excellent homogeneity. Here, monolithic [poly(methyl methacrylate)/monodisperse silica particles] nanocomposites have been prepared and characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), dynamic light scattering (DLS), micro-hardness, and differential scanning calorimetry (DSC).     

A theoretical and photoelastic contact stress analysis relevant to orthopaedic knee prostheses

This study is based on a theoretical and photoelastic static contact stress analysis, relevant to the design of the plastic tibial plateau in an orthopaedic knee prosthesis. It involves the review of existing theoretical analyses concerned with the contact mechanics of layered elastic systems and, where possible, the validation of any relevant findings using two dimensional photoelasticity. Significant findings include the identification of a general minimum recommendable design thickness for the plastic tibial plateau, the endorsement of using the Hertzian contact theory to predict contact stress levels in the tibial plateau of certain knee implants and the slight improvement in contact conditions in the plastic when the plateau is perfectly bonded to its supporting metal tray.     

Single-crystal synthesis of highly thermal conductive 12C-enriched diamond from pyrolytic carbon powder by the high-pressure,high-temperature method

We have examined the possibility of synthesis of ¹²C-enriched diamond single crystal by a conventional temperature gradient method at high pressure and high temperature using a starting material of a carbon powder source prepared via pyrolysis of ¹²C-enriched methane. ¹²C-enriched diamond single crystal (about 3 mm in diameter) was successfully grown at 1430 °C, 6.1 GPa using a ¹²C-enriched pyrolytic carbon source prepared from ¹²C-enriched methane (1 to 5 Torr) at 1800 °C. Thermal conductivity of the ¹²C-enriched diamond single crystal was measured by a modified specimen arrangement of a cut-bar steady-state conduction technique. The result showed that thermal conductivity of the ¹²C-enriched diamond single crystal (99.97% ¹²C) was 29.9 W/cm-K, and it was found to be 32% higher than that of similarly synthesized naturally abundant diamond single crystal (99.0% ¹²C), indicating the isotope effect of diamond.     

Study on the propagation of inlet flow distortion in axial compressor using an integral method

 An integral method is investigated and developed in the current work. The effects of the parameters of inlet distortions on the trend of downstream flow feature in compressor are simulated. Other than the drag-to-lift ratio of the blade and the inlet incidence angle, it is found that the distorted inlet velocity is another essential parameter to control the distortion in propagation. Based on this study, a novel critical distortion line and corresponding critical distortion factor are proposed to express the effect of the two essential inlet parameters on the propagation of distortion, namely, the inlet incidence angle and the distorted inlet velocity. From the viewpoint of compressor efficiency, the propagation of inlet flow distortion is further described by a compressor critical performance and its critical characteristic. The results present a useful physical insight to an axial flow compressor behavior and asymptotic behavior of the propagation of inlet distortion, and confirm the active role of compressor in determining the velocity distribution when compressor responds to an inlet flow distortion. Received: 20 December 2001 / Accepted: 21 August 2002 The authors would like to thank HQ RSAF for permission to publish this work, their financial support and encouragement. The first author wants to acknowledge Prof. Frank Marble of California Institute of Technology, for bringing the problem to the author's attention and for his helpful discussion.     

Computer modeling of the continuous annealing furnace

A computer program to calculate the strip temperature heated in the continuous annealing furnace was developed, using the zone method for radiative heat transfer analysis with the measured gas temperature in the furnace. Using theF _E Operator, the present study considered the effects of soot and transient species, in addition to the H₂O−CO₂ gas mixture on the gas radiative heat transfer. The predicted strip temperature distribution forF _E=1.05 represented well the measured data. The maximum difference in the heat flux transfered to the strip from the combustion gas forF _E=1.0 (without soot and transient species gas radiation) and 1.05 (with soot and transient species gas radiation) was about 15%. The present study also investigated the effects of line speed and thickness variations on the strip temperature, establishing the bases for the on-line computer model.     

Continuous and discontinuous fatigue crack growth of irradiated ultrahigh molecular mass polyethylene in saline solution at 37°C

To provide data for prosthesis design, the fatigue crack growth resistance of irradiated ultrahigh molecular mass polyethylene (UHMMPE) in saline solution at 37°C was determined from tests performed on compact tension specimens, comparable in size to the components in knee prostheses. The specimens were cyclically loaded by using a sinusoidal wave form at 1 Hz with a minimum-to-maximum load ratio of 0.1. Scanning electron microscopic fractography was used to examine the fracture surfaces. At higher stress levels, the Paris's Law was used to analyse the data, and a striation pattern with each striation corresponding to multi-cycles was observed. At lower stress levels, discontinuous fatigue crack growth was found, a phenomenon which dominated the fatigue life of the material and had not been reported previously in this material. A craze zone ahead of the crack tip was observed, which formed the discontinuous crack growth band with a length relevant to the Dugdale plastic zone length.