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Three-dimensional braided carbon fiber-reinforced ZrC matrix composite, 3-D Cf/ZrC, were prepared by liquid metal infiltration process at 1200 °C using a Zr2Cu intermetallic compound as infiltrator. The microstructure and properties of the composites were investigated. The results indicated that ZrC with a yield of 35.2 ± 1.8 vol.% was certified as the major phase of the composites. The formation of ZrC was controlled by a solution-precipitation mechanism. The obtained composites exhibited good mechanical properties, with a flexural strength of 293.0 ± 12.1 MPa, a flexural modulus of 82.7 ± 6.4 GPa and a fracture toughness of 9.8 ± 0.9 MPa m1/2. The mass and linear ablation rates of the composites exposed to oxyacetylene torch were 0.0013 ± 0.0005 g s−1 and −0.0009 ± 0.0003 mm s−1, respectively. The formation of a dense ZrO2 protective layer and the evaporation of residual Cu contributed mainly to the excellent ablation resistance. 相似文献
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Yong Zhang Hongbo Ren Yutie Bi Xianpan Shi Bin Wang Lin Zhang 《Journal of Porous Materials》2017,24(5):1303-1307
A new hybrid aerogel with low volume shrinkage and high toughness was prepared by aqueous condensation of melamine, starch and formaldehyde and extracting the solvent from the wet gel with carbon dioxide under the supercritical condition. The sizes of the wet gel and aerogel were measured by vernier calipers and the volume shrinkage of the aerogel was as low as 1.8%. The results from BET and SEM indicated that the hybrid aerogel belonged to the mesoporous material, which showed a typical three-dimensional porous structure with a specific surface area about 366.2 m2/g and pore diameter about 12.9 nm. To study the mechanical properties of the hybrid aerogel, we measured the compressive stress as a function of strain and the hybrid aerogel demonstrated excellent elasticity and mechanical durability. 相似文献
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DDoS攻击的研究是网络安全研究领域的一个研究热点。预测DDoS攻击发生的概率,对于早期防御和响应DDoS攻击具有重要意义。提出了一种基于概率有限状态自动机的DDoS攻击预警模型,给出了一种计算攻击成功概率和攻击期望威胁度的方法。实验表明,方法能有效地计算出DDoS攻击成功概率和期望威胁度,实现早期防御。 相似文献
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《Ceramics International》2020,46(4):4587-4594
Carbon fiber reinforced boron carbide (Cf/B4C) composites were fabricated with different Cfs contents by spark plasma sintering (SPS). The interfacial residual thermal stress (RTS) distribution in the Cf/B4C composites and its effects on the fracture behavior of the composites was investigated based on Raman spectroscopy and finite-element (FE) calculation. The results show that the maximum RTS of Cf in as-produced composites were obtained at the edge of fibers. The B4C matrix among fibers suffered a high compressive and tensile RTS simultaneously in radial and tangential directions, which caused the formation of micro-cracks and became the origin of fracture failure of the Cf/B4C composites. The maximum relative density 98.7% and bending strength of 391.41 MPa were obtained when the Cf content was 2.5% while the maximum fracture toughness of 5.46 MPa·m1/2 at 5% Cf content of Cf/B4C sample. The sharp decreases of bending strength when increasing content of Cf cloth was mainly caused by high RTS in the composites. 相似文献
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