DS/FH通信系统的跳频同步技术研究

同步是DS/FH混合通信系统的关键技术之一。根据跳频系统中对同步的要求,介绍了一种适用于DS/FH混合扩频通信系统的跳频同步方法,采用同步字头和精准时间相结合的方法实现跳频同步。对同步性能进行了分析,结果表明该跳频同步方法同步时间短,捕获概率高。     

A new efficient method for one‐pot conversions of aryl carboxylic acids into nitriles without solvent

A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry     

11B and 15N solid state NMR investigation of a boron nitride preceramic polymer prepared by ammonolysis of borazine

A poly(aminoborazine), precursor for hexagonal boron nitride (h-BN) obtained by reaction of borazine B₃N₃H₆ with ammonia, and its pyrolysis derivatives have been extensively characterised by ¹⁵N and ¹¹B MAS NMR. The various B and N sites have been identified according to their first neighbouring atoms, as well as to the second ones in the case of ¹⁵N, and have also been quantified. This study demonstrates that a suitable choice of NMR techniques together with the use of isotopic enrichment can lead to a large improvement in spectral resolution, which allows a better understanding of such complex BN preceramic polymer structures and permits to follow the polymer-to-ceramic transformation.     

服装低密度聚乙烯热熔胶化学粉碎的研究

服装粘合衬布的生产需要低密度聚乙烯热熔胶的微细粉末,介绍了对该热熔胶的化学粉碎技术所进行的实验研究,表明采用适当的助剂种类和用量以及适宜的工艺过程,通过化学粉碎可以得到合格的粉末产品。     

超分子主体化合物在分析化学中的应用研究进展

综述了近年来超分子主体化合物在分析化学领域的应用研究与进展。分别以冠醚、环糊精、杯芳烃、卟啉4类超分子为主体功能化合物的研究进行了详细的评述，并对这几类主体化合物在分析化学中的应用研究进行了展望。     

Water reuse in a shrimp processing line: Safety considerations using a HACCP approach

The large consumption of water involved in food manufacturing is prompting food processors to optimise the use. Treating and reusing or recycling water within the food plant results in substantial reduction of water use and wastewater production and discharge. If implemented, water reuse should be integrated into existing HACCP programs, and HACCP plans specifically addressed to the actual reuse should be elaborated. This paper evaluates the microbiological safety issues associated with water recycling during the production of shrimps (Pandalus borealis) in brine, and it indicates how the hazards may be effectively controlled using a HACCP approach. Following these procedures, process water recovered from peeling during shrimp processing and treated by means of reverse osmosis could be recycled within the same food unit operation.     

华北油田鄚东地区深井钻井液技术

鄚东地区钻井过程中经常发生垮塌、卡钻、井漏等复杂事故。该地区深井钻井采用了抑制性及封堵性较强的铵基沥青树脂高密度钻井液体系,并根据地层特点,对不同井段制定了相应的钻井液维护处理措施。结果表明,该钻井液体系抑制性好,抗温、抗污染能力强,性能稳定,成功地控制了复杂事故的发生,满足了该地区深层钻井的要求。     

Stress function with finite magnitude of stress concentration around an interface crack

A new mathematical model for study of an interface crack between two dissimilar elastic half planes is proposed. A process zone is formed along the interface between the physical crack and the continuous part. Both the crack opening (and sliding) displacement with a smooth shape and the finite magnitude of stress concentration appear in this zone. The analytical model is expressed by closed elastic solutions using complex variables, but with no oscillations at the crack tip.     

活化剂在织物漂白中的应用研究

对活化剂TAED和PAG在棉织物常规高温双氧水漂白过程中的应用进行了研究与探讨，并且得出最佳工艺条件，即H2O2 3g／L，渗透剂1g／L，活化剂4g／L，pH为7．