纳米复合永磁材料的研究进展

纳米复合永磁材料兼具硬磁性相的高矫顽力和软磁性相的高饱和磁化强度,磁性能优异。本文综述了纳米复合永磁材料的磁性相晶粒间的交换耦合作用、矫顽力机制、微磁学模拟等理论方面的研究进展,同时论述了成分、添加元素、制备工艺对材料微观结构和磁性能的影响,着重介绍了最有应用价值的快淬法磁粉制备工艺。     

区外销售企业青年员工队伍建设探讨

文章从青年的重要性和特点入手,结合所在单位青年员工结构特点,对区外销售企业当前在青年员工队伍建设上存在的问题进行了总结,并从社会和企业层面对产生这些问题的原因进行了深入分析,最后提出了区外销售企业青年员工队伍建设在思想教育和引导、满足利益诉求两大方面应采取的七项具体措施。     

Effects of nano-Ag on the combustion process of Al–CuO metastable intermolecular composite

Effects of nano-Ag with high thermal conductivity on the combustion wave behavior of Al–CuO MIC (metastable intermolecular composite) are studied in this paper by incorporating Al–CuO MIC with nano-Ag particles in different weight proportions. The physical and chemical characteristics of Al–CuO MIC are determined using scanning electron microscope (SEM), X-ray diffraction (XRD) and differential scanning calorimeter (DSC). The combustion wave behavior is identified by high-speed video recording (HSVR). The experimental observations confirm that the presence of nano-Ag particles improves the heat transfer efficiency. With nano-Ag increasing from 1 wt% to 10 wt%, the first exothermic peak temperature decreases from 607.8 °C to 567.6 °C, and average combustion speed (ACS) increases at first and then reduces. The most suitable amount of nano-Ag is 2 wt% with the ACS and instantaneous combustion velocity on the order of 954.0 m/s, 1562.5 m/s. Moreover, heat transfer mechanisms in the combustion process of Al–CuO MIC are better understood, especially by distinguishing conduction from convection during the combustion propagation. Furthermore, three stages (ignition, acceleration and steady combustion) of reactive propagation are observed in the combustion process. And the corresponding dominative heat transfer mechanisms in the three stages are conduction, conduction to convection transition, and convection, respectively.     

The hydrogen flow characteristics of the multistage hydrogen Knudsen compressor based on the thermal transpiration effect

Multistage hydrogen Knudsen compressor based on the thermal transpiration effect has very exciting prospect for the hydrogen transmission in the micro devices. Understanding of the hydrogen flow characteristic is the key issue for the designs and applications of the hydrogen energy systems. Firstly, the numerical models of the multistage hydrogen Knudsen compressor are established. The distributions of the rarefaction, velocity and temperature at different stages of the hydrogen flow are calculated and presented. Moreover, the dimensional pressure increases of the hydrogen gas flow are analyzed, and the flow behaviors in the microchannel and the connection channel are discussed. Secondly, the numerical simulation at different connection channel height is implemented, and the hydrogen gas flow characteristics in the connection are analyzed. Especially, the performances of the pressure drop in the connection channel under different channel heights are studied, and the hydrogen gas compression characteristics of different cases are compared and discussed. Also, the effect of the connection channel height on the hydrogen gas pressure increase in the microchannel is investigated. The studies presented in this paper could be greatly beneficial for the hydrogen detection and transmission.     

Facile and eco-friendly synthesis of porous carbon nanosheets as ideal platform for stabilizing rhodium nanoparticles in efficient hydrolysis of ammonia borane

Carbon materials have been demonstrated as excellent carriers for preparing supported metal nanocatalysts in catalytic applications. However, numerous chemical activators including strong acids and bases were applied, leading to the entire process dangerous and hazardous. Eco-friendly, economic, and convenient synthesis of carbon materials with desired properties as supports for metal nanoparticle (NP) stabilization to boost performance is important but remains challenging. Here, we developed a facile and eco-friendly strategy to synthesize porous carbon nanosheets (PCNs) with ultrahigh specific surface area (2575.1 m²/g) via pyrolysis the mixture of potassium oxalate and glucose. The resultant PCNs can be used as ideal platform for in-situ distribution of small Rh NPs (Rh/PCNs) as efficient catalysts in hydrogen production from ammonia borane (AB) under ambient conditions. Specifically, Rh/PCNs displayed high activity for AB hydrolysis, with a turnover frequency (TOF) of 513.2 min⁻¹. Small and well-distributed Rh NPs on PCNs with large catalytically active surface atoms are contributed to the high catalytic property of Rh/PCNs for the reaction. Present study has demonstrated that the PCNs is a superior catalyst support for preparing a series of metal NPs in other catalytic applications beyond hydrolysis reaction.     

Pulse-modulation eddy current probes for imaging of external corrosion in nonmagnetic pipes

Since the nonmagnetic pipe is normally utilized in corrosive and hostile environment, it is prone to the external corrosion which occurs on the outer surface of the pipe and severely undermines the structural integrity and safety. Although Pulsed Eddy Current technique (PEC) is currently preferred for detection and evaluation of subsurface defects in tubular conductors, it is subject to technical drawbacks. In light of this, Pulse-modulation Eddy Current technique (PMEC) is intensively investigated in the paper for enhancement of the evaluation sensitivity to external corrosion and accuracy of corrosion imaging. Closed-form expressions of the PMEC response and its sensitivity to external corrosion in tubular conductors are formulated via the Extended Truncated Region Eigenfunction Expansion (ETREE) modeling. Following simulations for analysis and comparison of field signals and evaluation sensitivities of PMEC and PEC, experiments of PMEC for evaluation and imaging of external corrosion are carried out. Through theoretical and experimental investigation, it has been found that regarding the evaluation and imaging of external corrosion in nonmagnetic pipes, the PMEC-based probe have higher sensitivity and imaging accuracy than that based on PEC. The superiority of PMEC to PEC in inspection of tubular conductors is further identified.     

3D ECT reconstruction by an improved Landweber iteration algorithm

Electrical capacitance tomography (ECT) is a relatively mature non-invasive imaging technique that attempts to map dielectric permittivity of materials. Recently, 3D ECT has gained interest because of its potential to generate volumetric images. The study of a fast and accurate image reconstruction algorithm is a challenge task, especially for 3D reconstruction. In this paper, we propose an improved Landweber iteration algorithm. We incorporate an additional acceleration term into the cost function and apply an adaptive threshold operation to the image obtained in each iteration for reducing artefacts. The algorithm proposed is tested by the noise-free and noise-contaminated capacitance data. Sensitivity matrixes and capacitance data of a 3D ECT sensor are obtained by using the finite element (FE) method. Extensive simulations in 3D reconstruction are carried out. The results verify the effectiveness of these improvements. Both the reconstruction time and the artefacts in the reconstructed image are reduced obviously. The experimental results of 3D reconstruction of objects in the shape of letters U and L confirm the effectiveness of the proposed algorithm further.     

Development of microsatellite markers and a preliminary assessment of population structuring in the rice weevil,Sitophilus oryzae (L.)

The rice weevil, Sitophilus oryzae is one of the primary pests of stored grains worldwide. To develop and implement an effective integrated pest management strategy, an understanding of the population structuring of this destructive pest is vital. In this study we used Illumina paired-end sequencing to develop S. oryzae species-specific microsatellite markers, and used these markers to conduct a preliminary assessment of population structuring in four populations of S. oryzae from three countries (Australia, China, and USA). 7,635,996 raw sequencing reads were produced, with 11,794 microsatellites detected and 214,257 primer options designed. 48 microsatellite markers were selected for further validation, with 10 markers amplifying consistently across the four S. oryzae populations. These markers displayed a high level of polymorphism overall (6.67 alleles/locus), though this was slightly lower within populations (3.10–4.88 alleles/locus). We used the markers to conduct a preliminary assessment of genetic structuring among the four S. oryzae populations: three laboratory cultures (New South Wales, Queensland, and Santai) and a field collected population from Kansas. Analyses suggest high levels of genetic differentiation between the sample locations, with a global F_ST of 0.239, and pairwise F_ST values ranging from 0.100 to 0.395. Bayesian clustering analyses suggest these four populations formed four distinct clusters, with a similar pattern identified by Principal Coordinate Analysis. These microsatellite markers, together with our preliminary population genetic analyses, will provide a valuable resource for population genetic research, and contribute to effective integrated pest management strategies in the future.     

Levitation Performance Study of Bulk HTSC over Monopole PMG Consider Different Cross-Section Configuration with 3D-Modeling Numerical Method

Magnetic levitation force of bulk high temperature superconductors (HTSCs) above monopole permanent magnet guideway (PMG) is simulated using finite element method (FEM). The models are formulated by H-formulation and resolving codes is developed using Finite Element Program Generator (FEPG). The E–J power law is used to describe the electrical field vs. current density nonlinear characteristic of HTSC. By the method, the levitation performance is studied consider different cross-section configure of the monopole PMG. The simulation results show that the maximum levitation force (MLF) of the bulk HTSC will increase when the height/width of the PMG rises while fixing the width/height of the monopole PMG cross-section. The increasing trends to slow when the absolute differential value of the height and the width of the PMG cross-section become larger and larger. For a certain cross-section area of the monopole PMG, the economical levitation cost may be achieved while the ratio of height to width of the cross-section changes between 0.475 and 0.525.     

基于USB的TMS320F2803x片内Flash在线编程技术

详细介绍了应用在线编程技术的系统配置,应用程序代码的格式转化的方法步骤.给出应用程序代码的读取存储和在线编程的流程以及程序代码的搬运、烧写、校验的源程序.该技术成功应用于实际工程中,给系统升级维护提供了诸多便利.