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81.
《Sensors and actuators. A, Physical》2006,125(2):223-233
To characterize the thickness of a corrosive fluid system's coated facilities, such as pipes, tubes, tanks, and structural members, a complex ultrasonic transducer capable of measuring multilayered parts was fabricated and the time and frequency responses were evaluated. The target transducer was constructed with two active dual elements made from tape-cast PbNb2O6 sheets and an additional thin-film active element made from sol–gel spin-coated Pb(Zr0.52Ti0.48)O3 films. After adjusting the properties of each active element, a complex transducer was assembled after matching the impedance of each element and considering the minimal interference between the active layers. The impulse response of the assembled complex transducer shows excellent characteristics. Moreover, the assembled transducer's capability of accurately measuring the thickness assures that it can be directly applied to related industries. 相似文献
82.
《International Dairy Journal》2006,16(3):268-273
Buffalo milk proteins (casein, co-precipitate or whey protein concentrate) were phosphorylated with phosphorus oxychloride (POCl3) at three different pH values (5.0, 7.0 and 9.0). The solubilities of phosphorylated milk proteins were examined over the pH range 3.0–9.0 in water and ionic (0.1 m NaCl or 10–70 mm Ca2+) systems. The solubilities of buffalo milk proteins decreased at pH 3.0, while there was an increase in the solubilities of casein and co-precipitate near their isoelectric points upon phosphorylation. Solubilities of these phosphorylated milk proteins were pH dependent in 0.1 m NaCl but there was a decrease in their solubilities with increase in calcium ion concentration. This alteration could be due to the shifting of isoionic points of phosphorylated buffalo milk proteins towards acidic pH. 相似文献
83.
《Computers & Geosciences》2006,32(8):1221-1227
The multiple inverse method is a numerical technique designed to separate stresses from heterogeneous fault–slip data. The method is one of the resampling methods based on the pattern recognition. Plotting solutions determined from k-fault subset into the parameter space, we have clusters representing significant stresses for the dataset. This paper presents a technique to improve the resolution of stress for the method. The regularity/singularity test of the subsets taken from the fault–slip data is the key for this purpose. The resolution and accuracy of the method are improved by eliminating erroneous stresses or artifacts that were yielded by the method. The performances of the method are demonstrated with a variety of artificial datasets. 相似文献
84.
合成并表征了N-十六烷基丙烯酰胺(HDA)和对叔丁基苯酚甲基丙烯酸酯(BPhMA)的共聚物p(HDA-BPhMA)s。当HDA含量较高时,共聚物可在气,液界面上形成稳定,排列紧密的单分子薄膜,并可以Y型膜的方式沉积在各种固体基片上,形成多层均匀的Langrnuir-Blodgett(LB)膜。这种LB膜被成功地应用于光刻,获得了分辨率为0.5μm的LB膜图形。以该图形为抗蚀层,可将图形进一步转移至金属薄膜上,得到分辨率较高的金属图形,在图形转移的过程中,这种LB膜显示出较高的抗蚀性,有望作为纳米抗蚀薄膜材料在亚微米刻蚀领域得到应用。 相似文献
85.
《Journal of the European Ceramic Society》2005,25(9):1681-1688
The effect of simultaneous addition of CaO and SiO2 on the microstructure and magnetic properties of sintered SrO-excess Sr-hexaferrites was studied. Both additives markedly affect the grain growth behavior and the magnetic properties. CaO-additions promote densification, which results in increased remanence, but due to simultaneuous grain growth the coercivity drops to <100 kA/m. SiO2 additions are known to suppress grain growth. Simultaneous addition of CaO and SiO2 is shown to be very beneficial in tailoring a dense microstructure with relatively small grains. The ratio of CaO/SiO2 was found to be optimum at about 1, and magnets with a remanence of 430 mT and a coercivity of 300 kA/m were obtained. Transmission electron microscopy (TEM) studies and investigations by energy-dispersive analysis of X-rays (EDX) in the scanning TEM (STEM) mode show that both CaO and SiO2 are concentrated at grain boundaries and grain junctions forming an amorphous secondary phase. 相似文献
86.
《Journal of the European Ceramic Society》2005,25(2-3):129-135
A poly(aminoborazine), precursor for hexagonal boron nitride (h-BN) obtained by reaction of borazine B3N3H6 with ammonia, and its pyrolysis derivatives have been extensively characterised by 15N and 11B MAS NMR. The various B and N sites have been identified according to their first neighbouring atoms, as well as to the second ones in the case of 15N, and have also been quantified. This study demonstrates that a suitable choice of NMR techniques together with the use of isotopic enrichment can lead to a large improvement in spectral resolution, which allows a better understanding of such complex BN preceramic polymer structures and permits to follow the polymer-to-ceramic transformation. 相似文献
87.
88.
用天然甘油磷脂胆碱开环丙交酯,以获得具有仿生功能的生物降解聚乳酸.采用1H-NMR、FT-IR确证在聚合物结构中引入了生物功能基团磷脂胆碱.通过1H-NMR和GPC测定分子量及其分布,研究了反应时间和温度对聚合物分子量扣产率的影响,聚合物产率达80%以上.将磷脂引入聚乳酸链段中得到可全降解的、生物相容性好的磷脂高分子.这一新的思路可以用于合成一系列新型的药物载体和组织工程支架材料. 相似文献
89.
90.
《Materials Letters》2007,61(8-9):1881-1884
Organic ultraviolet (UV) ray absorbents, cinnamic acid (CA) and p-methoxycinnamic acid (PMOCA) were intercalated into Zn2Al layered double hydroxides (Zn2Al-LDHs) by co-precipitation reaction. The organic–inorganic nanocomposites, Zn2Al-LDH/CA and Zn2Al-LDH/PMOCA were obtained. The samples showed excellent UV ray absorption ability and their catalytic activity for the air oxidation of castor oil greatly decreased when the organic UV ray absorbents were intercalated in the layers of the Zn2Al-LDHs. The studies suggested that Zn2Al-LDH/organic UV absorbent nanocomposites might be used as safe sunscreen materials. 相似文献