新疆西伯利亚白刺果中红色素的提取工艺

以溶剂浓度、浸提时间、pH值为因素，各设3个水平，按L9（34）正交表设计实验，筛选白刺红色素的最佳提取工艺。结果得出采用pH1的20％乙醇，提取4次，每次0．5h效果较佳。本方法工艺简便、合理可行，适于工业化生产。     

Chemical compositional characterization of eight pear cultivars grown in China

The sugar, organic acid, amino acid and fatty acid compounds of eight commercial pear cultivars were identified and quantified using high-performance liquid chromatography (HPLC) equipped with RI and UV detectors and gas-chromatography (GC) equipped with FID detector. The mineral composition was determined by inductively coupled plasma-mass spectrometry (ICP-MS). The results showed great quantitative differences in the composition of the pear cultivars. Fructose was the dominant sugar in the eight pear varieties, followed by glucose and sucrose, while malic acid was the principal organic acid. The C16:0, C18:0, C18:1, C18:2 and C18:3 fatty acids were clearly the most abundant fatty acids, and the C18 family comprised more than 70% of the total fatty acids content. Asparagine and serine were the principal amino acids. Potassium is the most abundant mineral, followed by magnesium and calcium. The results provide important information on how to make the best use of pear cultivars investigated for different uses, which is of significance for both technological research and processing practice.     

超声法提取中药制剂中醇溶性成分的研究

以超声时间、提取温度、乙醇浓度和固液比为因素,每因素进行3水平的正交实验,用紫外分光光度法测定中药制剂——促生长散中厚朴酚的含量和以其作为综合评价指标。结果发现提取实验中影响因素最大的是乙醇浓度,最佳提取条件为:超声时间60(20,20,20)min,超声温度35℃,乙醇浓度65%,固液比1:10。     

棉油皂脚中植物甾醇的提取工艺研究

为了探索从棉油皂脚中提取植物甾醇的工艺条件。以皂脚为原料,通过单因素和正交实验优化最佳工艺条件,并对粗品进行纯化,以高效液相色谱法测定的甾醇含量为考察指标。植物甾醇提取的最佳工艺为:皂化料液比1∶3,90℃下皂化3 h,用乙酸乙酯进行萃取,料液比为1∶20,粗甾醇的提取率为75.6%,其中提取得到的β-谷甾醇和菜油甾醇的纯度分别为(66.5±0.47)%、(5.67±0.08)%,其经无水乙醇重结晶两次后,纯度可达91.8%。结果表明最佳提取工艺重现性较好;HPLC法测定甾醇含量结果准确可靠。     

CO余热锅炉装置关键部件的设计及流场模拟

CO余热锅炉是催化裂化装置的关键部件,影响整套装置的安全经济运行。针对高温烟气热能浪费、环境污染等问题,设计了一种高温烟气回收装置,并对关键结构气风混合室进行三维实体建模,通过CFD前处理软件Gambit进行网格划分,最后导入Fluent软件对该结构进行数值流场模拟,结果表明该装置能够有效回收高温烟气、减少热量损耗、降低生产成本,具有很好的经济与社会效益。     

食品中辣椒红色素含量测量不确定度的评定

本文对高效液相色谱法测定食品中辣椒红色素含量的测定不确定度进行了评定,按照JJF1059-1999方法建立了数学模型,通过实验过程中取样器具、对照品的纯度,标准曲线拟合等不确定因素的分析,确定不确定度分量,合成不确定度.本评定方法客观、准确,在实际工作中有较强的实用性.     

北疆部分地区食源性大肠杆菌血清型、毒力基因及耐药基因的研究

目的研究北疆部分地区食源性大肠杆菌的优势血清型、毒力基因和耐药基因的相关性。方法采用玻片凝集法测定了大肠杆菌血清型分布,PCR方法调查11种耐药基因和9种毒力基因。结果血清试验,定型菌株26株,分别属于17种血清型,其中O1、O115为优势血清型;PCR结果表明,不含有所检测耐药基因的分离株占12.50%,至少含有2种以及以上的分离株占50.00%,分离株对blaOXA基因携带率高达57.14%;检出率较高的毒力基因为fimC(64.29%)和fimA(25.00%)。结论 O1、O115为主要的血清型,2种血清型菌株拥有的耐药基因谱和毒力基因谱不相同。     

Line and point cluster models for spatial health data

Spatial cluster modelling of small area disease incidence and mortality has previously focused on clusters where excess risk is distributed around fixed points, and the aim is the reconstruction of these points (cluster centers). Often there is a need to assess clusters of a different form, such as around roads or river systems. These clusters are often linear or can be approximated by combinations of several linear segments. In this paper the recovery of point and line clusters is considered jointly. An example application is given where both linear or point clustering could be present.     

Implementing automated diagnostic systems for breast cancer detection

This paper intends to an integrated view of implementing automated diagnostic systems for breast cancer detection. The major objective of the paper is to be a guide for the readers, who want to develop an automated decision support system for detection of breast cancer. Because of the importance of making the right decision, better classification procedures for breast cancer have been searched. The classification accuracies of different classifiers, namely multilayer perceptron neural network (MLPNN), combined neural network (CNN), probabilistic neural network (PNN), recurrent neural network (RNN) and support vector machine (SVM), which were trained on the attributes of each record in the Wisconsin breast cancer database, were compared. The purpose was to determine an optimum classification scheme with high diagnostic accuracy for this problem. This research demonstrated that the SVM achieved diagnostic accuracies which were higher than that of the other automated diagnostic systems.     

新疆天然骨料粉煤灰混凝土抗渗性研究

新疆混凝土工程天然骨料料源丰富,水工混凝土骨料几乎全部采用天然骨料,针对这一特点,结合当地原材料情况,通过实验探讨了影响新疆天然骨料粉煤灰混凝土抗渗性的主要因素,提出了天然骨料粉煤灰混凝土提高抗渗性的最大水胶比和粉煤灰掺量上限值等指标。