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1.
Feng Wenran Li Zhen Chen Yingying Chen Jinyang Lang Haoze Wan Jianghong Gao Yan Dong Haitao 《Journal of Materials Science》2022,57(3):1881-1889
Journal of Materials Science - Although chalcogenide materials continue to generate considerable interest due to great potentials for various optoelectronic devices, annealing for a long time in... 相似文献
2.
To reduce the energy consumption of the shrimp blanching process and improve the economic value of the blanched product, a transcritical CO2 heat pump blanching system (THPB system) was designed in this paper. The trends of astaxanthin were investigated at atmospheric pressure near boiling temperature, combined with the color and structural properties of shrimp samples, and the optimal blanching times of 270 s and 240 s were obtained at 90°C and 95°C, respectively. In contrast to the fuel blanching system (FB system) at 100°C, the annual standard coal consumption of the THPB system with 90°C blanching is decreased by 79%, and the annual operating cost can be saved by CNY 63,800, with a payback period of about 3.13 years.Industrial relevanceBlanching is one of the effective ways to prolong the shelf life of shrimp. However, the research on the blanching time and temperature of shrimp is not comprehensive. In addition, the traditional fuel blanching process has high energy consumption and pollution, and can no longer meet the quality requirements of the modern food processing industry. Heat pump has been shown to have better performance in food drying, but it is less used in blanching. The information presented in this study may provide other insights into food processing. 相似文献
3.
Forecasting the volatility and correlation among different kinds of assets has important applications in areas such as risk management, options pricing, and asset allocation. This paper mainly uses a novel multivariate Generalized Autoregressive Score (GAS) model to analyze and forecast volatilities and correlations between Brent, WTI and gold prices. The time-varying parameters of multivariate GAS model for a given distribution of crude oil and gold prices is observed which is supported by Doornik-Hansen test. The testing results of time-varying parameters based on LRT statistics reveal that the dependent structure between Brent and gold prices is more complex than those of WTI and gold. The estimation results show that the multivariate GAS method well captures the volatility persistence and nonlinear interaction effects between the crude oil and gold markets. In addition, we compare the forecasting performance of the GAS with the classical Dynamic Conditional Correlation Generalized Auto-Regressive Conditional Heteroskedasticity (DCC-GARCH) model, and find that the forecasting power of volatility and correlation in multivariate GAS model is better than the DCC-GARCH model. 相似文献
4.
采用共沉淀法制备了系列Ca-Mg-Al复合氧化物催化剂,通过对沉淀剂配比、沉淀液pH值及焙烧温度等制备条件的考察,得到以Na2CO3为沉淀剂、pH=9.5、850℃下焙烧4h制备的Ca-Mg-Al催化活性最高。在 n(PG)∶n(urea)=1.5∶1、反应温度为145℃、绝压20kPa、反应时间4h、催化剂用量为尿素质量的5%时,碳酸丙烯酯收率达到84.6%。采用XRF、XRD、NH3-TPD、SEM及BET对催化剂的组成、晶型及酸性进行了表征,发现随着沉淀剂中Na2CO3的含量增加,催化剂中CaO∶MgO的比例增大,碳酸丙烯酯的收率亦升高;经850℃焙烧后,催化剂中存在CaO和MgO两种活性中心,起协同催化作用;随着焙烧温度由700℃升高到850℃,NH3-TPD脱附曲线向低温方向偏移,且强酸中心NH3脱附峰面积比由81.14%明显下降为0,中强酸中心NH3脱附峰面积比由0增加到78.07%,而碳酸丙烯酯收率由68%增加到84.6%,这表明催化剂强酸性位的减少是催化活性增加的主要原因。 相似文献
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采用搅拌摩擦焊方法对3 mm厚7050-T7451铝合金进行焊接,为改善接头应力腐蚀敏感性,焊后进行121 ℃ × 5 h + 163 ℃ × 27 h双级时效处理. 通过对微观组织、显微硬度以及应力腐蚀敏感性的分析,研究双级时效对焊接接头性能的影响. 结果表明,双级时效后晶粒发生粗化,晶界内析出相和周边无沉淀析出带(PFZ)变宽,导致在热影响区和热力影响区出现大量不连续晶界;接头热影响区的显微硬度有所下降,但范围明显变窄,接头组织的均一性得到改善;时效处理后的接头在进行应力腐蚀试验 60天后仍未发生断裂,而未经时效处理的接头在1天内全部发生断裂,说明双级时效有效降低了焊接接头的应力腐蚀敏感性. 相似文献
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Xiaoqin Zhang Shugang Ma Ang Shen Jin Zhu Zhisen Shen Jinggang Wang Xiaoqing Liu 《应用聚合物科学杂志》2020,137(44):49365
Poly(butylene terephthalate-co-butylene 2,5-furandicarboxylate) copolyesters (PBTFs) were synthesized from 1,4-butanediol, dimethyl terephthalate (DMT), and 2,5-furandicarboxylic acid (FDCA) by a two-step polymerization method. Their chemical structures were confirmed by Fourier-transform infrared spectroscopy, proton nuclear magnetic resonance spectroscopy, and carbon nuclear magnetic resonance before thermal properties were explored with differential scanning calorimeter and thermogravimetric analyzer. Results showed that PBTFs changed from semi-crystalline to completely amorphous when the content of FDCA unit was increased to 45 mol% at first, and then became crystallographic again with the further increment of FDCA unit to 75 mol%. For their mechanical properties, the tensile modulus and strength showed the similar trend, decreasing firstly and then increasing later. Their barrier to carbon dioxide and oxygen became better with the increasing of furan content due to the rigidity and higher polarity of furan ring. The performance of PBTFs copolyesters was investigated clearly, and the relative content of FDCA and DMT can be adjusted to satisfy different performance requirements. 相似文献
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10.
Liu Chuanfa Zhou Zhiwei Qin Juan Xia Guangbo Liu Yangyang He Binbin Li Fanqing Sun Peiyong Wu Wenliang 《Journal of Porous Materials》2021,28(4):1215-1225
Journal of Porous Materials - New Sn-Ti microspheres were first successfully synthesized by a PVP-assisted sol-gel method in this paper, and their performance in the B–V oxidation of... 相似文献