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171.
172.
173.
柯家骏 《稀有金属(英文版)》1992,(3)
Scandium was recovered from dilute chloride solutions with potassium salt of saturated C_8~C_(12)fattyacids as surfactant by Ion flotation.The optimum comprehensive results of physical properties,stability andscandium concentration of the foam formed with potassium caprate CH_3(CH_2)_8 COOK can be obtained.Re-covery of scandium in the foam was 98% at pH 3.8~5.0 and 25~55℃.The experimental results of 0.3 L/minairflow rate was satisfactory for flotation column.It is of a great potential for using ion flotation technique toconcentrate scandium from dilute solutions. 相似文献
174.
Characteristics of graphite felt electrode electrochemically oxidized for vanadium redox battery application 总被引:2,自引:0,他引:2
The graphite felt was oxidized at a positive electrode potential in sulfuric acid solution.The electrochemical performance of the treated graphite felt served as electrode for vanadium redox battery was investigated with FT-IR,SEM,XPS,BET,cyclic voltammetry and testing VRB system,respectively.The results show that the molar ratio of O to C increases from 0.085 to 0.15 due to the increase of—COOH functional groups during electrochemical oxidation treatment,and the GF surface is eroded by electrochemical oxidation,resulting in the surface area increase from 0.33 m2/g to 0.49 m 2/g.The VRB with modified GF electrode exhibits excellent performance under a current density of 30 mA/cm 2 .The average current efficiency reaches 94%and average voltage efficiency reaches 85%.The improvement of electrochemical activity for the electrode is ascribed to the increase of the number of—COOH group and the special surface of GF. 相似文献
175.
Wei-Chao Gu 《Surface & coatings technology》2007,201(15):6619-6622
Plasma electrolytic oxidation (PEO), also called micro-arc oxidation (MAO) or anode spark deposition (ASD), is a novel technique to produce hard ceramic coatings on metals, such as aluminum, titanium, magnesium (called valve metals) and their alloys. Up to now, many researchers focused on the PEO process for workpieces of regular shapes such as cube, cake or stick samples, etc. But no one paid attention to the irregular samples such as tubular materials. This research emphasized the PEO process of long tubes, especially the way to obtain uniform thickness of ceramic coatings on inner surface of tubes. Furthermore, the PEO kinetic behaviors of aluminum tubes were also investigated. The potential difference between the electrodes indicated a linear relationship with the coating thickness. A central accessory electrode was axially used to eliminate the shielding effect of electric field and was effective to obtain axially uniform coating on the inner surface of the tubes. The combination of hot-dipping aluminum and PEO process to obtain ceramic coating on 45# steel tubes was also performed in this work. 相似文献
176.
QINHongwei HUJifan YANGFuming 《稀有金属(英文版)》2004,23(3):231-234
The amorphization and magnetic properties of Fe62Nb38 mechanically alloyed powders were investigated. In the initial mechanical alloying processes, the lattice structure of pure Fe is destroyed due to the cold-welding and fracturing, accompanying the reduction of ferromagnetic properties. The Ms value of Fe62Nb38 powders with ball-milling time t=6 h is only 48.1 A.m^2/kg. With prolongating of mechanical alloying processes, a solid state amorphization reaction (SSAR) takes place and the Fe-Nb ferromagnetic amorphous phase is formed. With the milling time increasing from 6 to 18 h, the saturation magnetization of Fe62Nb38 powders increases with enhancement of the proportion of ferromagnetic amorphous phase in milled powders. The Ms value of the Fe62Nb38 amorphous powders is 98 A.m^2/kg, which is very close to the value estimated from dilute model. However, the Curie temperature of the Fe62Nb38 amorphous phase is only 206℃, which is much smaller than that of the pure Fe. This implies that the exchange interaction between Fe atoms in amorphous alloyed Fe62Nb38 becomes weak due to the Nb dilution. Investigation shows that the variation of magnetic properties of milled powders is one of important tools for describing the amorphization by mechanical alloying. 相似文献
177.
178.
采用含乙烯基聚硅氮烷为原料,利用先驱体转化法与有机泡沫浸渍法相结合制备SiCN泡沫陶瓷。通过聚氨酯泡沫及聚硅氮烷的热分析制定温度曲线,研究了裂解温度、浸渍/裂解增强处理次数等工艺参数对泡沫陶瓷抗压强度的影响,采用XRD、SEM及EDS对SiCN泡沫陶瓷进行了物相、微观结构及成分分析。结果表明,在1000~1400℃温度范围内,随着温度的升高,泡沫陶瓷的抗压强度先升高后降低,增强处理对提高抗压强度有明显效果,当裂解温度为1300℃,经二次增强处理后,试样的抗压强度达11.5MPa。XRD研究表明,随着温度的逐步升高,聚硅氮烷的裂解产物发生了由非晶态向晶态的转变。微观结构分析显示,SiCN泡沫陶瓷呈三维网状结构,具有良好的贯通性,开孔气孔率达到85%。 相似文献
179.
层流等离子体材料表面改性工艺研究 总被引:2,自引:0,他引:2
针对热物理性能明显不同的3种金属,研究层流等离子体技术在材料表面改性工程应用的可行性.结果表明,重熔工艺适用于热导率适中和微结构稀疏的铸铁类材料;熔覆工艺则适用于低热导率的不锈钢.两种处理工艺均可以明显改变热影响区的材料微结构并提高材料表面硬度.研究表明改性层微结构的改善与材料热物理性能和凝固过程瞬态特性密切相关. 相似文献
180.
Y.G. Xiao Q. Huang Z.W. Ouyang J.W. Lynn J.K. Liang G.H. Rao 《Journal of Alloys and Compounds》2006,420(1-2):29-33
The crystal and magnetic structures of the Laves phase compound NdCo2 in the temperature range from 9 to 300 K are determined by Rietveld refinement technique, using high-resolution neutron powder diffraction data. The compound crystallizes in space group above the magnetic ordering temperature TC (≈100 K), in space group I41/amd below TC and in space group Imma below the tetragonal–orthorhombic structural/magnetic transitions at TM ≈ 42 K. The assignment of the space groups to the crystal structures of NdCo2 in different temperature ranges complies with the reported Mössbauer studies. Detailed information of the crystal and magnetic structures of NdCo2 at different temperatures are reported. 相似文献