Polyaniline-multiwalled carbon nanotube composites: Characterization by WAXS and TGA

Polyaniline/carboxylated multi-walled carbon nanotube (PAni/c-MWNT) nanocomposites have been synthesized by micellar aided emulsion polymerization with various c-MWNTs compositions, viz., 0.5, 1, 5, and 10 wt %. The microcrystalline parameters such as the nanocrystal size (〈N〉), lattice strain (g), interplanar distance (d_hkl), width of the crystallite size distribution, surface weighted crystal size (D_s), and volume of the ordered regions were calculated from the X-ray data by using two mathematical models, namely the Exponential distribution and Reinhold distribution methods. The effects of heat ageing on the microcrystalline parameters of the PAni/c-MWNT nanocomposites were also studied and the results are correlated. The thermal stability and electrical resistivity of the PAni/c-MWNT nanocomposites were examined with thermogravimetric analysis (TGA) and a conventional two-probe method. The TGA data indicate that the thermal stability of the nanocomposites improved after the incorporation of c-MWNTs. The influence of temperature on the resistivity of the nanocomposites was also measured. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci 2008     

基于基尼系数的Web社区稳定性度量

Web社区是互联网中自组织程度较高的部分,它不是一个孤立系统,而是一个耗散系统,很多时候涨落无法耗散摔,导致社区运行不稳定.基尼系数可以用来衡量Web社区稳定性,通过基尼系数的简易计算公式计算社区内部成员积分或者其它参数,可以得出Web社区稳定性的度量.该度量对于研究和利用Web社区具有重要参考意义.     

凸轮逆序测量方法

目前各杂志所发表的关于凸轮测量的文章，所讨论的均是凸轮的顺序测量方法，有关凸轮的逆序测量(反求工程)方法，尚未见于文字。本文将对凸轮的逆序测量方法进行探讨。     

西气东输工程用X70热轧板卷屈服强度检测值波动大的探讨

对西气东输工程用X70热轧板卷检验过程中出的屈服强度σ0.5波动大的情况进行了分析，认为拉伸试样弯曲是主要原因。这一问题可通过反复压平试样，确保试样的平直度以及适当提高钢的强度的方法加以解决。     

用穿透法测量声速时初始点的选择问题

用穿透方法测量岩心或固体的声速时，从测量波形中确定纵波（或横波）的到达时刻（或称初始点）比较困难，当声波的频率比较低时，其误差对测量结果影响比较大。本文用相位分析的方法研究了初始点的选择问题。首先，用各向同性较强、均匀的汉白玉制作标准件，测量其不同传播距离的波形，再用相位补偿的方法得到其传播速度；其次，利用传播速度，可从不同距离的测量波形中确定初始点及其对应的测量系统的时间延迟常数；最后，确定波形的其他位置为初始点时对应的时间延迟常数，因此，我们可以根据实际测量波形的特点选择最佳的初始点，利用其对应的时间延迟常数得到比较精确的声速。模型测量结果表明，初始点位置不同，其对应的测量系统的时间延迟常数也不同，也即测量系统的时间延迟常数是与初始点的选择相对应的。     

Investigation of the Correlation between Texture and Microstructure on a Submicrometer Scale in the TEM

In recent years the investigation of local texture and microstructure by analysis of electron backscatter diffraction patterns (EBSP) in the SEM has become a very powerful and popular method. With the introduction of SEM with field emission guns (FEG) the spatial resolution of EBSP measurements could be enhanced from 500 nm with a tungsten emitter to better than 50 nm. This evolution of SEM techniques raises the question whether transmission electron microscopy (TEM) still has fields of application in texture research. The present article answers this question with a clear “yes” and presents three examples of investigations where TEM is indispensable. The three examples comprise the investigation of the correlation between dislocation structure and deformation texture, a study on nucleation mechanisms of recrystallization in highly deformed metals and the investigation of microtexture and microstructure in nanocrystalline materials. Together with the presentation of these cases some of the necessary measurement techniques are described briefly. It is shown that TEM has to be applied when highest spatial resolution of orientation determination and imaging and high accuracy of orientation determination are to be reached, when the three‐dimensional and quantitative characterization of lattice defects is required or when materials with a high density of lattice defects are to be investigated.     

Techniques and Apparatus for Measuring Rotational Core Losses of Soft Magnetic Materials

In many situations such as the cores of a rotating electrical machine and the T joints of a multiphase transformer, the local flux density varies with time in terms of both magnitude and direction, i.e. the flux density vector is rotating. Therefore, the magnetic properties of the core materials under the rotating flux density vector excitation should be properly measured, modeled and applied in the design and analysis of these electromagnetic devices. This paper presents an extensive review on the development of techniques and apparatus for measuring the rotational core losses of soft magnetic materials based on the experiences of various researchers in the last hundred years.     

Quantitative measurement of gas hold-up distribution in a stirred chemical reactor using X-ray cone-beam computed tomography

Cone-beam type X-ray computed tomography (CBCT) is a potential method to measure three-dimensional phase distributions in vessels. An example for that is the measurement of gas profiles in stirred chemical reactors. Such data are highly valuable for the assessment and evaluation of chemical processes, for optimisation of the reactor and stirrer design, and for evaluation of computational fluid dynamics codes used to model the fluid flow and heat transfer in reactive systems. However, there are considerable difficulties for accurate quantitative measurements due to beam hardening and radiation scattering effects. In a theoretical and experimental work we have investigated the non-linear effects of both physical phenomena and developed a suitable measurement setup as well as calibration and software correction methods to achieve a highly accurate measurement of void fraction profiles with CBCT.     

Facial detection and location based on skin color and eye characteristic

This paper comes true a system of facial detection and location. Firstly, it realizes the facial detection of candidate region used skin color for the given image, and considers the influence of similar skin. Secondly, it realizes the location for eye region used the gray characteristic of eye and correction of central measurement, and makes further selection for facial candidate region. The end, it normalizes the facial image and makes it as front standard image, so realizes the facial characteristic location.     

火焰原子吸收光谱法测量污水中锑量的测量不确定度评定

通过火焰原子吸收光谱法对水中的锑量进行了测定,对影响测量结果的不确定度分量进行了量化的计算,从而得出影响锑量测量不确定的主要因素是测量样品消解液中的锑的质量浓度引起的不确定度.