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991.
992.
High temperature, high pressure e.s.r. measurements of the hydrogenation reaction of Taiheiyo coal in the presence of catalysts were carried out to understand the stabilization of thermally and/or catalytically induced free radicals. A decrease in free radical concentration with increasing temperature was observed for ZnCl2 and SnCl2 · 2H2O catalysts at 10MPa under hydrogen gas. High pressure modified single-cell d.t.a. and p.d.a. equipment augmented the uniquely designed high temperature, high pressure e.s.r. cell. The hydrogenation reaction was monitored under the same experimental conditions as for e.s.r. From the results of the combination of high temperature, high pressure e.s.r. with high pressure d.t.a. and p.d.a., it was established that H2 molecules can react efficiently with free radicals from coal molecules created by the presence of ZnCl2 and SnCl2 · 2H2O catalysts. 相似文献
993.
研究了高密度聚乙烯在海南自然曝露和氙灯人工老化后的结构和力学性能变化。结果表明:相比于自然曝露,高密度聚乙烯主要力学性能的氙灯人工老化加速倍率大约为4;老化期间,高密度聚乙烯分子间存在着交联和降解二种竞争反应,老化早期以交联为主,后期以降解为主;氙灯老化试验相比于自然曝露,老化主要集中在材料表层。 相似文献
994.
Effects of N application and water supply on yield, oil content and N accumulation by canola, cultivar Marnoo, grown on a heavy clay soil in the Goulburn Murray Irrigation Region were investigated. Treatments were rainfed (Rf) or watered at a deficit of 50 mm (40–60 mm, I50) beginning in the spring. N treatments were 0, 50, 100 or 200 kg N ha–1 at sowing or as split applications of 20/80, and 50/50 kg N ha–1 at sowing and rosette, respectively.Yield (Yg) ranged from 170 to 520 g m–2. Irrigation and N increased yield in both years. Grain yields were increased by N application on the irrigated treatments when 100 or 200 kg N ha–1 was applied. Oil concentrations ranged from a maximum of 46.4% in treatment N0 to a minimum of 40.6% in treatment N200 and was inversely related to seed N concentration. Although fertilizer N decreased oil concentration, it increased the yield of oil.Nitrogen accumulation (Nb) limited yield of all treatments and was described by the equation, Yg = 806[1-EXP(–0.039*Nb)]. This implied a decrease in yield per unit of Nb at the higher rates of fertilizer addition with consequent increases in grain N concentration.The efficiency of water use in the production of grain (WUEg) and biomass (WUEb) were 7.5 and 23 kg ha–1 mm–1 respectively. Nitrogen additions increased WUEg and WUEb in both seasons. Maximum values of 8.9 (WUEg 1986) and 26.8 (WUEb 1987) were measured from treatment N200. These data suggest that the crops made efficient use of the applied water. 相似文献
995.
开发研制的高压水自动清洗炉门装置可彻底清除焦炉炉门上耐火砖及不锈钢刀边上的焦油及焦炭等结垢,从而保证炉门与焦炉本体的密封性,杜绝焦炉内有害气体及烟尘的外泄,降低了操作工人的劳动强度、改善焦炉现场的工作环境. 相似文献
996.
Four cocatalysts, referred to as ethylaluminoxanes, were synthesized by the reaction between triethylaluminium (AIEt3) and water under various molar ratios of H2O/Al at ?78°C. Aluminoxanes were used as cocatalysts for a MgCl2‐supported Ziegler–Natta catalyst for propylene polymerization at temperatures ranging from 70 to 100°C. When the polymerization was activated by AlEt3, the activity as well as the molecular weight and isotacticity of the resulting polymer gradually dropped as the temperature varied from 70 to 100°C. When ethylaluminoxane was employed as the cocatalyst, good activity and high molecular weight and isotacticity were obtained at 100°C. Furthermore, when the cocatalyst varied from AlEt3 to ethylaluminoxane, the atactic fraction and polymer fraction with moderate isotacticity decreased and the high isotactic fraction slightly increased, which indicated that the variation of the cocatalyst significantly affects the isospecificity of active sites. It was suggested that the reactivity of the Al‐Et group and the size of the cocatalyst were correlated to the performance of the Ziegler–Natta catalyst at different temperatures. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 1978–1982, 2006 相似文献
997.
同步污水处理/发电技术-微生物燃料电池的研究进展 总被引:2,自引:0,他引:2
同步污水处理/发电技术的微生物燃料电池是利用生物催化剂直接把化学能转化为电能,具有能量转化率高、污泥产率低、反应条件温和等优点。本文阐述了微生物燃料电池的工作原理,反应器的类型及结构,综述了其最新的研究进展,并对微生物燃料电池在污水处理领域的发展方向作了展望。 相似文献
998.
Michael?W.?PlesniakEmail author Paul?E.?Sojka Anshul?K.?Singh 《Journal of Coatings Technology and Research》2004,1(2):137-145
Spray transfer efficiency (TE) is defined as the mass fraction of sprayed paint which is deposited on the intended target,
the remainder of the sprayed paint becomes undesirable overspray. The relationship between TE and gun supply pressure (or
paint mass flow rate), gun-to-target distance, gun traverse speed, the angle of the spray gun relative to the target (gun-to-target
angle), plus spray cone angle is reported herein for a typical fan spray system. Experimental results indicate that spray
momentum rate (SMR) and droplet size dictate the TE for the various combinations of parameters considered here. The key finding
is that TE correlates with SMR and spray mean drop size (Sauter mean diameter, or D32) via an expression of the form TE=a+b SMR − c (SMR)2+d D32, where a, b, c, and d are coefficients, determined by fitting the experimental data, and SMR is estimated via SMR=m2/ρA, where the paint mass flow rate m, the paint density is ρ, and the gun exit orifice effective tip cross sectional area
is A. This expression accounts for physical phenomena that govern sprayed droplet deposition characteristics, such as entrainment,
bounce-back, and drop size.
Experimental results also show that, for the range of parameters studied, gun traverse speed has no effect on TE, but increasing
the angle of the spray gun relative to the target (gun-to-target angle), increasing the spray cone angle, or increasing the
gun-to-target distance will decrease TE. 相似文献
999.
从三元共聚合制备高性能聚乙烯(PE)和热塑性弹性体两个领域综述了乙烯三元共聚合机理的研究现状。高性能PE的研究主要集中在聚合过程中的“共单体效应”和“促进效应”;而三元乙丙橡胶的研究重点在对催化剂的研究和二烯烃的选择上。介绍了乙烯三元共聚合的工业化应用情况,总结了目前乙烯三元共聚合研究中存在的问题,并提出今后的研究方向。 相似文献
1000.