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71.
72.
Lan Liu 《Chemical engineering science》2006,61(12):4007-4021
A non-intrusive dye tracing technique, laser-induced fluorescence (LIF), has been applied to investigate the co-current flow of two immiscible organic-aqueous liquid flows in a vertical pipe. This technique allowed detailed visualization of the dynamic evolution of the flows. Flow structures in liquid-liquid flows at high dispersed phase fraction were revealed which had not been seen before. In pipe flow, an unstable range was found in the flow pattern map in which oil-in-water (o/w) and water-in-oil (w/o) dispersions could co-exist. Secondary dispersions (o/w/o and w/o/w) were observed for most volume fractions and velocities, especially in the unstable range. It was observed that, when the flow is in the unstable region, both w/o/w and o/w/o secondary dispersions could appear in the same set of experiments. It was found that this unstable range in the pipe flow, in spite of the similar appearance, was different to the ambivalent range seen in agitated systems. The one-dimensional drift flux model of Wallis (1969) for dispersed flow and a laminar model for co-current downward annular flow, were also applied to predict the in situ oil holdup; good agreement was obtained. 相似文献
73.
软段含羧基的水性聚氨酯贮存稳定性研究 总被引:6,自引:0,他引:6
合成了软段含羟基的水性聚氨酯(WPU),对影响其贮存稳定性的各种因素进行了研究,通过显微镜对PU进行了观察。结果表明:以甲苯二异氰酸酯(TDI)合成,在有性溶剂(如丁酮、丙酮)条件下用三乙胺中和,采用较小相地分子质量的聚酯有利于增强WPU的贮存稳定性,以TDI合成的PU-TDI体系的粒径较PU-IPDI体系的小,稳定性高;以丁酮、丙酮为溶剂的PU-IPDI体系相反转完全。 相似文献
74.
Johannes C. Jansen Marialuigia Macchione Raniero Mendichi Enrico Drioli 《Polymer》2005,46(25):11366-11379
Asymmetric gas separation membranes were prepared by the dry-casting technique from PEEKWC, a modified amorphous glassy poly(ether ether ketone). The phase inversion process and membrane performance were correlated to the properties of the polymer and the casting solution (molar mass, polymer concentration, solution rheology and thermodynamics). It was found that a broad molar mass distribution of the polymer in the casting solution is most favourable for the formation of a highly selective membrane with a dense skin and a porous sub-layer. Thus, membranes with an effective skin thickness of less than 1 μm were obtained, exhibiting a maximum O2/N2 selectivity of 7.2 and a CO2/CH4 selectivity of 39, both significantly higher than in a corresponding thick dense PEEKWC membrane and also comparable to or higher than that of the most commonly used polymers for gas separation membranes. The CO2 and O2 permeance were up to 9.5×10−3 and 1.8×10−3 m3/(m2 h bar) (3.5 and 0.67 GPU), respectively. 相似文献
75.
《Computer Speech and Language》2014,28(5):1195-1208
We discuss the use of low-dimensional physical models of the voice source for speech coding and processing applications. A class of waveform-adaptive dynamic glottal models and parameter identification procedures are illustrated. The model and the identification procedures are assessed by addressing signal transformations on recorded speech, achievable by fitting the model to the data, and then acting on the physically oriented parameters of the voice source. The class of models proposed provides in principle a tool for both the estimation of glottal source signals, and the encoding of the speech signal for transformation purposes. The application of this model to time stretching and to fundamental frequency control (pitch shifting) is also illustrated. The experiments show that copy synthesis is perceptually very similar to the target, and that time stretching and “pitch extrapolation” effects can be obtained by simple control strategies. 相似文献
76.
77.
借助电导率仪、光学显微镜和亚微粒子分析仪等测试手段。研究了乳液聚合导致一种新的转相过程,并用于八甲基环四硅氧烷的聚合中。研究表明:体系以 W/O 相态开始,单体由连续相向水相(分散相)内的胶束中扩散并发生聚合反应,形成 O/W/O 复合乳液。反应过程中连续相体积不断减小,分散相(O/W 复相)体积不断增大,当达到某一临界相比时,体系发生转相,转相后乳液为 O/W。对本实验物系,转相点临界相比主要由初始水油比和乳化剂浓度决定。同常规的乳液聚合相比,伴有转相现象的乳液聚合有其自身的特点,转相使得聚合速率、聚合物粒径及分布、乳液稳定性等发生变化。 相似文献
78.
79.
Kiran B. Deshpande 《Chemical engineering science》2003,58(16):3829-3835
As the holdup of dispersed phase in an agitated liquid-liquid dispersion is increased at fixed agitation, a point is reached (called inversion holdup) when the dispersion inverts—the dispersed phase becomes continuous and vice versa. In this work, we present experimental data which suggest that the inversion holdup for sufficiently intense turbulence is independent of all the operational parameters associated with a stirred tank, e.g., stirrer speed, vessel volume, impeller size, and impeller type; it depends only on the properties of the liquid-liquid system. The inversion holdup was verified to remain unchanged even for inversion in turbulent flow field in the annular space between two coaxial cylinders. A hypothesis involving drops in near contact with each other at high holdups is used to explain the experimental data. The new finding may also provide a qualitative basis for selecting a liquid-liquid system with desired extent of mixing in the dispersed phase for carrying out transport and reactions in multiphase systems. 相似文献
80.
This paper presents an integrated approach based on dynamic inversion(DI)and active disturbance rejection control(ADRC)to the entry attitude control of a generic hypersonic vehicle(GHV).DI is frstly used to cancel the nonlinearities of the GHV entry model to construct a basic attitude controller.To enhance the control performance and system robustness to inevitable disturbances,ADRC techniques,including the arranged transient process(ATP),nonlinear feedback(NF),and most importantly the extended state observer(ESO),are integrated with the basic DI controller.As one primary task,the stability and estimation error of the second-order nonlinear ESO are analyzed from a brand new perspective:the nonlinear ESO is treated as a specifc form of forced Li′enard system.Abundant qualitative properties of the Li′enard system are utilized to yield comprehensive theorems on nonlinear ESO solution behaviors,such as the boundedness,convergence,and existence of periodic solutions.Phase portraits of ESO estimation error dynamics are given to validate our analysis.At last,three groups of simulations,including comparative simulations with modeling errors,Monte Carlo runs with parametric uncertainties,and a six degrees-of-freedom reference entry trajectory tracking are executed,which demonstrate the superiority of the proposed integrated controller over the basic DI controller. 相似文献