Synthesis of Organic Dye-Impregnated Silica Shell-Coated Iron Oxide Nanoparticles by a New Method

A new method for preparing magnetic iron oxide nanoparticles coated by organic dye-doped silica shell was developed in this article. Iron oxide nanoparticles were first coated with dye-impregnated silica shell by the hydrolysis of hexadecyltrimethoxysilane (HTMOS) which produced a hydrophobic core for the entrapment of organic dye molecules. Then, the particles were coated with a hydrophilic shell by the hydrolysis of tetraethylorthosilicate (TEOS), which enabled water dispersal of the resulting nanoparticles. The final product was characterized by X-ray diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy, photoluminescence spectroscopy, and vibration sample magnetometer. All the characterization results proved the final samples possessed magnetic and fluorescent properties simultaneously. And this new multifunctional nanomaterial possessed high photostability and minimal dye leakage.     

三坐标测量机测头半径对测量数据的影响及其消除方法

分析了三坐标测量机测头半径对测量数据的影响,对由三坐标测量机在复杂曲面上测得的点,每一截面的测量点用大挠度三次样条连接,而各截面间采用基样条函数连接,组成基样条函数和大挠度三次样条曲线的混合曲面,在此基础上推导出测量点所形成的曲面及其法向等距面的数学模型,从而消除测头半径的影响。     

A debugger for concurrent programs

This paper reports on an experimental debugger for concurrent programs. Design objectives include a showing of greatest usefulness when dealing with multiprocess interactions, creation of a simplified more approachable interface for programmers, allowance for the systematic organization (and limitation) of debugging information by programmers, reflection of a natural view of concurrency, and portability. The design responds to a perceived need for debugging techniques applicable in systems of concurrent, communicating, asynchronous processes. During debugging sessions, a user is able to dynamically explore interprocess synchronization points, parallel actions and deadlock situations. The programmer interface is based on a transparent window multiplexer providing a set of windows for each concurrent process. The window manager interactively maps interesting windows to programmer-specified viewscreen locations, while relegating temporarily uninteresting windows to the background. In implementing a debugger for concurrent programs, a principal concern is the probe effect, or the possibility that the debugger itself masks synchronization errors in the program being debugged. For the examples explored, the probe effect was not observed to limit the localization of implanted synchronization errors.     

Simultaneous estimation of the thermophysical properties of three kinds of fruit juices based on the measured result by a transient heat flow probe method

The thermophysical properties of three kinds of fruit juices (grape juice, orange juice, and pineapple juice) were measured at various temperatures (10–50 °C) and concentrations (10–50%). A new method for the simultaneous determination of thermophysical properties using a modified version of current probe theory method was proposed. The temperature changes of the probe upon insertion in the sample were fitted to an approximate solution of the heat conduction equation, and the values of two parameters in that solution were determined. Using the values of these parameters, the thermal conductivity and thermal diffusivity of each sample were determined. The specific heat of each sample was estimated from the definition of thermal diffusivity. These thermophysical properties were expressed as a function of concentration and temperature.     

Silicon cantilever arrays with by-pass metal through-silicon-via (TSV) tips for micromachined IC testing probe cards

In this paper, an integrated probe card is proposed and developed for wafer-level IC testing. Based on micromachining technology, totally about 26,000 cantilever-tip probes can be formed simultaneously in one 4-in. silicon wafer, with the minimum pitch of 35 μm for adjacent probing tips. The probe card is designed with a novel composite structure that combines both single-crystalline silicon and electroplated metals. In the composite structure, a novel bypass through-silicon-via with a low aspect ratio can be high-yield fabricated for transferring the testing signals from the probing sided (at the wafer bottom side) to the I/O interface (at the front side). The probe card makes full use of the advantages of the single-crystal silicon and the electroplated nickel and copper. Bulk micromachined silicon cantilevers behave uniform probing height and a good elastic deformation property, while the electroplated nickel probing tips promise high hardness and satisfactory electric contact performance with the dies-under-test (DUT). Measurements show that the fabricated cantilever is able to withstand a contact force of 80mN by a tip displacement of 20 μm. The measured contact resistances on metal pads (Al, Cu, and Au) are all below 1 Ω, whereas the maximum current leakage is 64 pA for 3.3 V voltage across two adjacent tips. After a probing reliability test of 100,000 cycles, the cantilever-tip shows no sign of any performance degradation.     

晶圆测试探针新的测试价值

晶圆测试探针曾被认为是节约废芯片封装成本的一种方法,现今它却成为工艺控制、成品率管理、产品质量以及总测试成本的一个关键因素。此外,随着组装相关的故障测试之后,封装水准晶圆分选的完全测试不久将会来临。     

基于探针的固网漏话通知业务的实觋

随着本地呼叫移动趋势的不断加大,各大运营商之间的竞争更加激烈,面对市场的竞争压力,如何通过业务创新提升用户的ARPU值,保持客户忠诚度,成为运营商关注的重点。漏话通知业务是为了解决固定电话的不足而推出的新业务,是一种基于语音的增值服务,它可以及时地通知被叫错失的来电,并提高现有客户的ARPU值。论文基于探针侦听信令方式实现的漏话语音增值业务平台,在未来语音增值业务市场中将会起到非常重要的作用。     

自振荡电子镇流器的设计方法

该文提出并分析了利用自振荡指令电路的电子镇流器的设计方法.作为继电控制系统的自振荡电子镇流器,为确定其参数,应用了(等效频率传输的)描述函数及扩展的Nyquist稳定性判据.提供了40 W荧光灯用电子镇流器的模拟与试验结果,以证实该设计方法的可行性和有效性.     

可检测Fe~(3+)的萘酰亚胺席夫碱荧光探针的合成及性质研究

通过醛胺缩合反应,合成了一种萘酰亚胺席夫碱荧光探针(L)。探针L的分子结构通过1H NMR进行了鉴定。紫外-可见吸收光谱和荧光发射光谱测试结果表明探针L可选择性识别Fe~(3+)离子,并且具有可视化识别特点。     

Green synthesis of yellow emitting PMMA–CdSe/ZnS quantum dots nanophosphors

We herein report the fabrication of highly fluorescent yellow emitting nanophosphors using CdSe/ZnS quantum dots (QDs) dispersed in polymethyl methacrylate (PMMA). The QDs were synthesised via a simple, non-phosphine and one pot synthetic method in the absence of an inert atmosphere. The as-prepared nanocrystallites were characterised by Fourier transform infrared spectroscopy (FTIR), ultraviolet–visible (UV–vis) and photoluminescence spectroscopy, energy-dispersive spectroscopy (EDS), Raman spectroscopy, transmission electron microscopy (TEM) and high resolution TEM (HRTEM) microscopy. Optical analysis confirmed that the as-synthesised CdSe/ZnS QDs were of high quality with sharp absorption peaks, bright luminescence, narrow emission width and high PL quantum yield (up to 74%). The electron microscope images showed that the QDs are small and spherical in shape with narrow size distributions while the HRTEM micrograph confirmed the high crystallinity of the material. The Raman analysis of the QDs revealed the formation of core–shell structure and the energy dispersive spectroscopy confirmed the presence of the corresponding elements (i.e., Cd, Se, Zn and S). The dispersion of the core–shell QDs in PMMA matrix led to the red-shifting of the emission position from 393 nm in the neat PMMA to 592 nm in the nanocomposite. The fabricated highly fluorescent yellow emitting PMMA–CdSe/ZnS core–shell QDs polymer nanocomposite film display excellent optical properties without loss of luminescence. Furthermore, the as-synthesised organic soluble CdSe/ZnS QDs were successfully converted into highly water soluble QDs after ligand exchange with mercaptoundecanoic acid (MUA) without the loss of their emission properties. The simplicity of the method and the quality of the as-synthesised nanocomposite make it a promising material for the large scale fabrication of diverse optical devices.