X70管线钢在模拟土壤介质中裂纹扩展特性研究

试验研究了X70管线钢在模拟土壤介质 0 5mol/LNa2 CO3 + 1mol/LNaHCO3 溶液中和循环载荷下的裂纹扩展特性和宏观规律。结果表明 ,裂纹扩展主要受裂尖应力强度因子幅的控制。不同的应力比下 ,裂纹扩展呈现明显的门槛值特征 ,随着应力比的升高 ,裂纹扩展的门槛值降低。在碱性碳酸盐溶液 (pH =9 3)中 ,加载频率对裂纹扩展速率没有明显的影响 ;在中性碳酸盐溶液 (pH =7 0 )中 ,裂纹扩展速率随加载频率的降低而升高 ,呈现明显的频率效应。中性碳酸盐溶液中的裂纹扩展速率高于碱性碳酸盐溶液的裂纹扩展速率 ,且随加载频率的降低 ,裂纹扩展速率增大     

微机综合自动化在农网建设和改造中的应用

介绍微机综合自动化在农网改造和建设中应用的优点及自动化系统的组成、特点、结构、功能等 ,分析了广西农网改造和建设中选用微机综合自动化系统时应注意的问题。     

提高储层预测精度技术思路与对策

采用地质、地震、测井人员协同一体化作业，对地下地质目标进行综合预测与评价，可提高储层预测精度，降低预测结果的多解性。主要方法是针对不同的区块，采用不同的方法和对策，首先从单井储层划分对比入手，建立储层沉积模式，同时对地震数据目的层段进行精细解释，建立地层构造模式，用沉积、构造等地质规律来指导和约束反演；利用测井资料对地震资料进行精细标定，建立各井的单井波阻抗模型，建立井数据和地震数据沟通的桥梁；在严格的测井约束、地质模型约束、层位控制下进行储层反演；充分利用地质、地震反演结果、地震参数提取及分析结果、测井、测试和分析化验等资料对储层预测结果进行综合分析与评价。该方法应用于长庆、大庆、准噶尔等实际区块，取得了较好的效果。     

一步法合成松香改性酚醛树脂

探讨了一步法合成松香改性酚醛树脂的反应机理，确定了最佳原料组成及合成工艺，由此制备出高溶解粘度和矿油容纳度的松香改性酚醛树脂，是一种性能优异的高级胶印油墨连接料     

Thermoplastic elastomeric composition based on maleic anhydride–grafted ground rubber tire

Ground rubber tire (GRT) powder was maleated in an internal mixer using maleic anhydride and dicumyl peroxide at 160°C. Maleated GRT was characterized by using X‐ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, wettability, and differential scanning calorimetry. The physical properties of the dynamically vulcanized 60 : 40, rubber : plastic composition based on acrylated high‐density polyethylene as the plastic phase and ethylene propylene diene rubber containing maleated GRT as the rubber phase were found to be greater than the corresponding composition containing nonmaleated GRT. The blend was found to be reprocessable, like themoplastic elastomers. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 370–378, 2002; DOI 10.1002/app.10348     

丁腈橡胶/导电粒子复合材料的正温度系数(PTC)特性

将导电粒子碳黑和铜粉分别与丁腈橡胶混合制备导电聚合物复合材料，其中碳黑（Ｎ５５０）／丁腈橡胶复合材料的电阻率随温度的变化呈现较强的正温度系数（ＰＴＣ）效应。讨论了掺入导电粒子浓度、结构和表面性质以及混炼硫化工艺等对该类材料的室温电阻率及ＰＴＣ效应的影响。     

Microstructure-related fracture toughness and fatigue crack growth behaviour in toughened, anhydride-cured epoxy resins

Fracture toughness and fatigue crack propagation (FCP) of plain and modified anhydride-cured epoxy resin (EP) were studied at ambient temperature. Liquid carboxyl-terminated acrylonitrile-butadiene (CTBN) and silicon (SI) rubber dispersions were used as tougheners for the EP. The morphology of the modified EP was characterized by dynamic mechanical analysis (DMA) and by scanning electron microscopy (SEM). The fracture toughness, K_c, of the compositions decreased with increasing deformation rate. K_c of the EP was slightly improved by CTBN addition and practically unaffected by incorporation of the SI dispersion when tests were performed at low cross-head speed, v. Both modifiers improved K_c at high v, and also the resistance to FCP, by shifting the curves to higher stress intensity factor ranges, ΔK, by comparison with the plain EP. It was established that both fracture and fatigue performance rely on the compliance, J_R, at the rubbery plateau, and thus on the apparent molecular mass between crosslinks, M_c. The failure mechanisms were less dependent upon the loading mode (fracture, fatigue), but differed basically for the various modifiers. Rubber-induced cavitation and shear yielding of the EP were dominant for CTBN, whereas crack bifurcation and branching controlled the cracking in SI-modified EP. The simultaneous use of both modifiers resulted in a synergistic effect for both the fracture toughness at high deformation rate and the FCP behavior.     

顺丁橡胶生产过程"门尼升值"的原因研究

研究了顺丁橡胶生产过程中门尼升值的原因。结果表明，顺丁橡胶生产后处理的膨胀干燥过程存在门尼升值现象。不同内在质量的顺丁橡胶门尼升值不同，正常条件下门尼升值发生于门尼粘度的测试过程。     

Y型密封圈橡胶模设计

介绍了Y型橡胶模具的设计 ,重点对模具结构和模腔尺寸进行了分析和阐述 ,经生产验证 ,此模具结构合理 ,定位可靠 ,操作方便 ,从而为同类产品的设计提供了参考。     

Purification and Characterization of an Endoprotease from Melon Fruit

An endoprotease was purified from melon fruit (Cucumis melo L.) by ammonium sulfate precipitation, gel filtration and ion-exchange chromatography using t-butyloxycarbonyl-Ala-Ala-Pro-Leu p-nitroanilide as a substrate. The molecular weight was estimated as 26,000 and isoelectric point pH 9.5. It preferentially hydrolyzed peptide bonds of the carboxyl terminal sides of Leu, Ala, His, Gin, and Am. Activity was strongly inhibited by diisopropyl phosphofluoridate, indicating the serine protease nature of the enzyme. The migration distance on electrophoresis, molecular weight and substrate specificity differed from cucumisin, a known protease from melon. This unusual protease may have potential for special food treatment applications.