镁合金与钛合金的瞬间液相扩散焊

为实现镁合金AZ31B与钛合金Ti6A14V的可靠连接，研究了两者以Al为中间层的瞬间液相扩散焊接头的微观结构与连接强度。研究结果表明：当焊接时间为180min时，焊接温度是影响界面反应热力学与动力学的主要参数，其对接头的微观组织、接头界面新生相构成与连接强度有重要影响。保温温度低于450℃时，AZ3IB／AI界面无液相产生，无法实现AZ31B与Ti6A14V的可靠连接；保温温度在450℃～480℃变化时，温度对AZ31B／Al／Ti6A14V界面反应的动力学因素有明显影响，且直接决定了焊后接头新生相的构成与分布。470℃保温180min的接头剪切强度较高（72．4MPa），达到AZ31B母材（86MPa）的84．2％。     

镁合金焊接接头的力学性能

随着镬合金应用的日益广泛，其焊接接头的力学性能也受到人们的重视。介绍和分析了采用不同焊接方法时焊接接头的力学性能。并提出一些看法，对镬合金焊接接头力学性能的研究有一定促进作用。     

快速凝固Mg94.6Zn4.8Y0.6镁合金薄带的组织与性能

采用单辊快速凝固技术制备了Mg94.6Zn4.8Y0.6合金薄带,研究了薄带的组织及性能特征。结果表明:Mg94.6Zn4.8Y0.6镁合金快速凝固薄带组织由过饱和的单相-αMg固溶体组成,沿厚度方向分为两个晶区:近辊面粗大等轴晶区和自由面细小等轴晶区。Mg94.6Zn4.8Y0.6合金快速凝固薄带的显微硬度为85.95HV,在250℃左右保温2 h的显微硬度最高,超过该温度(250~300℃)显微硬度显著下降。     

Effect of temperature on mechanical behavior of AZ31 magnesium alloy

Strain rate sensitivity and tension/compression asymmetry of AZ31 magnesium alloy at different temperatures and strainrates were investigated.Both of mechanical behaviors are temperature dependent.Strain rate sensitivity increases with increasingtemperature.Thermally activated slip is the source of strain rate sensitivity.At the temperature below or near 373 K,strain ratesensitivity is very little.Tension/compression asymmetry in yielding decreases with increasing temperature.Twinning is the reasonof tension/compression asymmetry.At the temperature above or near 573 K,the material shows little tension/compressionasymmetry of the flow stress.     

Thermodynamic database of the phase diagrams in the Mg-Al-Zn-Y-Ce system

The Mg-Al-Zn-Y-Ce system is one of the key systems for designing high-strength Mg alloys. The purpose of the present article is to develop a thermodynamic database for the Mg-Al-Zn-Y-Ce multicomponent system to design Mg alloys using the calculation of phase diagrams （CALPHAD） method, where the Gibbs energies of solution phases such as liquid, fcc, bcc, and hcp phases were described by the subregular solution model, whereas those of all the compounds were described by the sublattice model. The thermodynamic parameters describing Gibbs energies of the different phases in this database were evaluated by fitting the experimental data for phase equilibria and thermodynamic properties. On the basis of this database, a lot of information concerning stable and metastable phase equilibria of isothermal and vertical sections, molar fractions of constituent phases, the liquidus projection, etc., can be predicted. This database is expected to play an important role in the design of Mg alloys.     

Wear resistance of ceramic coating on AZ91 magnesium alloy by micro-arc oxidation

The ceramic coating formed on AZ91 magnesium alloy by micro-arc oxidation （MAO） was characterized. The results show that the ceramic coating （3.4-23 μm in thickness）on the surface ofAZ91 alloy was attained under different micro-arc oxidation treatment conditions, which consist mainly of MgO, Mg2SiO4 and MgSiO3 phases. Nano-hardness in a cross-sectional specimen was determined by nano-indentation experiment. The MAO coatings exhibit higher hardness than the substrate. Dry sliding wear tests for the MAO coatings and AZ91 alloy were also carded out using an oscillating friction and wear tester in a ball-on-disc contact configuration. The wear resistance of the MAO coatings is improved respectively under different treatment time as a result of different structures of ceramic coatings formed on AZ91 alloy.     

定向凝固AZ31镁合金晶粒取向及力学性能研究

采用自行设计的定向凝固装置制备了AZ31镁合金铸件,通过金相观察、XRD分析和室温压缩试验,研究定向凝固工艺对AZ31镁合金晶粒取向和常温力学性能的影响。结果表明:定向凝固制备的AZ31镁合金铸件具有柱状晶组织,第二相呈球状弥散分布于晶粒内部。由于温度梯度的影响,晶体规律性地定向生长,呈现较明显的[1010]择优取向。该铸件在常温力学性能和塑性成形性能上表现出各向异性的特点。     

粉末冶金法制备SiC晶须增强MB15镁基复合材料

采用粉末冶金法制备了SiC晶须增强镁基复合材料(SiCW／MB15)试样。通过检测基体显微硬度探讨了SiCW对镁合金时效规律的影响，并借助扫描电镜(SEM)、透射电镜(TEM)和拉伸试验，研究了混粉方式对复合材料室温力学性能、SiCW分布及显微结构的影响。结果表明，MB15及其复合材料的时效硬化曲线上均存在双峰现象；SiCW的加入既提高了MB5的硬度，又加快了其时效速度：混粉方式对晶须分布及SiCW／MB15复合材料的室温力学性能影响很大。     

镁合金焊丝挤压成形过程挤压力的研究

本文探索出一种镁合金焊丝挤压成形新工艺 ,简要阐述了该种工艺挤压成形的基本试验过程、试验装置。通过试验发现 ,挤压力是镁合金焊丝制备工艺过程的关键 ,探讨了影响挤压力的各种因素 ,如 :坯料温度、变形速度、变形程度、润滑条件及挤压模形状与尺寸。同时 ,以挤压1 2mm镁合金焊丝为例 ,运用主应力法计算得到了焊丝挤压过程中稳定变形阶段模具出口部分、锥形部分、挤压筒部分的单位挤压力 ,以及挤压机上的单位挤压力 ,试验发现计算所得的挤压机上的单位挤压力与实测值基本接近 ,并且可通过取定补偿系数的方法修正 ,利用该计算值 ,通过控制挤压力 ,首次成功制备出1 2mm镁合金焊丝。在此基础上运用该种计算方法分别计算出挤压1 6mm、2 0mm、2 4mm、3 0mm镁合金焊丝所需的单位挤压力 ,并在试验中成功制备出上述焊丝。     

薄带连铸技术的发展现状与思考

综述了钢的薄带连铸及铝合金的薄带铸轧发展现状,简要介绍了在高速钢、硅钢和镁合金的薄带连铸实验研究方面取得的进展.认为钢的薄带连铸技术近年取得了重要突破,未来10年薄带连铸技术可能快速发展;发展特殊性能或难加工合金的薄带连铸可充分发挥快速凝固的优势;采用立式双辊法可望进一步提高铝合金的浇铸速度,特别是高牌号铝合金的浇铸速度;应积极发展镁合金的薄带连铸技术,以改善镁合金板材的塑性加工及耐腐蚀问题.