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91.
92.
Toughening modification of poly(l -lactide) (PLLA) with rubber particles is often realized at the cost of transparency, mechanical strength, and modulus because high rubber loadings are generally required for toughening. In this work, a promising strategy to simultaneously improve the transparency and stiffness–toughness performance of poly(butyl acrylate)-poly(methyl methacrylate) (BAMMA) core-shell rubber nanoparticles toughened PLLA blends by utilizing the stereocomplex (SC) crystallization between PLLA and poly(d -lactide) (PDLA) is devised. The results reveal that the construction of SC crystallites in PLLA matrix via melt-mixing PLLA/BAMMA blends with PDLA can prevent BAMMA nanoparticles from aggregation and promote them to form network-like structure at lower contents. As a result, not only higher toughening efficiency with less rubber contents but also superior transparency is achieved in the PLLA/PDLA/BAMMA blends as compared with the PLLA/BAMMA ones where large aggregated BAMMA clusters are formed. Moreover, the outstanding reinforcement of SC crystallites network for PLLA can impart an enhanced tensile strength and modulus to PLLA/PDLA/BAMMA blends, thus improving the stiffness–toughness performance of PLLA/PDLA/BAMMA blends to a higher degree. This work demonstrates that SC crystallization is a promising solution to solve the contradiction between transparency and mechanical properties and then obtain superior comprehensive performances in rubber toughened PLLA blends. 相似文献
93.
94.
The mechanical properties and post-thermal aging properties of natural rubber (NR) and polybutadiene rubber (BR) blends at
different blending ratios are investigated herein. The experimental results show that both tensile and tear strengths of NR/BR
blends increase with increasing NR content. BR has a higher compression stiffness than NR. The deformation of BR is less than
that of NR under the same load conditions. With regard to aging properties, both tensile stress and strain of NR/BR blends
decrease after prolonged aging. In addition, the stress loss of BR is lower than that of NR, meaning that the aging resistance
property of BR is superior to that of NR. Furthermore, accumulated thermal history has shifted the glass transition temperature
(T
g) of NR/BR blends toward lower temperatures while the loss tangent (tan δ) value increases with prolonged thermal aging. 相似文献
95.
“金属布”硬质复合涂层的微观组织及性能 总被引:1,自引:0,他引:1
用X射线衍射仪、扫描电镜、摩擦磨损试验等,研究了粉末冶金“金属布”及其钢表面改性技术在钢表面制备的WC-Ni系合金复合涂层的微观组织和性能。结果表明:该合金涂层中硬质相的体积含量可大于60%;涂层的微观组织有两类:一种是在粘结相中均匀分布的碳化物与弥散分布的球状粘结相富集区构成的非均匀结构;另一种是碳化物和粘结相都均匀分布的均匀结构。碳化物分布区的硬度大于Hv1076,粘结相富集区的硬度在Hv967~Hv458之间。涂层与钢基体之间有几~几十微米的界面过渡区,形成剪切结合强度大于400MPa的冶金结合。复合涂层的耐磨性明显优于调质T8工具钢。 相似文献
96.
97.
橡胶密炼机混炼工艺瞬时功率控制法 总被引:2,自引:0,他引:2
橡胶密炼机混炼工艺瞬时功率控制法的理论由3部分组成:橡胶混炼过程的机理、密炼机流理论和混炼过程功率曲线与能量控制法不同,瞬时功率控制法实质上是控制混炼过程中胶料的粘度,确保混炼工艺过程保持最佳状态。因而瞬时功能控制法可监控生产过程,为密炼机混炼工艺的智能控制奠定了基础。 相似文献
98.
Polynitroalcohols (PNA) were obtained by AN‐reaction of nitro oligomers from ground waste rubbers (NO‐GWR) with C1‐C2‐aldehydes in presence of organic bases triethanolamine, triethylamine and cyclopropylamine. The AN‐reaction was studied at temperatures from 30 to 50°C, time 4 h, and NO‐GWR : aldehyde = 1 : 0.5/2.0 mass ratios in the solution. PNA were characterized by elemental analyses, such as 1H NMR spectra, IR spectroscopy—baseline method with internal standard and thermal analyses. The quantitative functional composition of PNA (%NO2, %C?O, and %OH groups) was proved to be similar to the composition of PNA obtained from model butadiene–styrene nitro oligomer (BSNO). It was concluded that NO‐GWR could replace NO based on elastomers in nitro aldol reaction with formaldehyde and acetaldehyde. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 3241–3250, 2006 相似文献
99.
CR/MMA乳液接枝共聚物的研制 总被引:1,自引:0,他引:1
用乳液接枝共聚法制备CR/MMA共聚物,讨论CR乳液、引发剂、接枝温度、MMA用量对接枝共聚转化率,接枝MMA含量、MMA接枝效率和粘接性能的影响,用红外光谱对接枝共聚物进行表征,该共聚物具有较好的粘接性能。 相似文献
100.