鱼类耳石扫描电镜样品制备与观察

本文介绍了一种鱼类耳石样品的扫描电镜制样方法，通过对草鱼耳石进行包埋，抛磨，并用合适的腐蚀剂处理，用ＳＥＭ成功地观察了耳石的日轮及超微结构，该方法简便易行，保证所观察耳石样品的微观结构完整与清晰。     

高水固结尾砂充填采矿充填体合理配比的研究

高水固结尾砂充填采矿是一种新型充填采矿法。试验测定了高水固结尾矿充填体的强度和变形特征；研究分析了影响充填体强度的主要因素、高水充填工艺的特殊要求，以及上向，下向进路开采对充填体强度和稳定性的要求，提出了满足支护强度，工艺及经济需求的充填材料的合理配比范围。     

Off-Optimum Cure of Aerospace Epoxy Adhesives

Four epoxy film adhesives used in aircraft manufacture and repair have been examined to establish the effect of deviation from the cure cycle specified by the manufacturer. In addition to the variation of the cure cycle, two surface preparations of the aluminium adherends (chromic acid etch or grit blast followed by silane treatment) were evaluated. Thermal analysis was used to examine the cure envelope of the adhesive, and its extent of cure and glass transition temperature. The adhesive properties were assessed by shear strength (in both single lap joints and in Iosipescu configuration), durability (Boeing wedge test) and chemical resistance to selected aggressive fluids. The sensitivity of the performance of a particular adhesive to offoptimum cure conditions depends on its composition and needs to be determined, not predicted.     

Asymmetric alumina membranes electrochemically formed in oxalic acid solution

Alumina membranes were fabricated by anodizing aluminium metal in 0.15 M oxalic acid. The growth kinetics of the porous layer were investigated in the temperature range –1 to 16 °C using linear potential scans up to 70 V. The faradaic efficiencies of metal oxidation and of porous layer formation, determined by applying Faraday's law, were found to be independent of both temperature and electrical charge. SEM analysis of the metal-side and solution-side surfaces revealed different morphologies. After dissolution of the barrier layer in phosphoric acid, the metal-side surface showed circular pores whose size of about 90 nm was found to be uniform and independent of temperature. The pore population was also practically independent of temperature and a value of about 4 × 10¹³ pores m^–2 was determined. On the solution-side surface the presence of a deposit partially occluding the mouths of pores was observed. This coating could be removed by chemical etching in NaOH or thermal treatment at 870 °C, where decomposition of oxalate occurs. This supports the hypothesis that the deposit consists of an aluminium salt containing oxalate anions precipitated from the solution. The results show that it is possible to control the morphological characteristics of the anodic alumina membranes by careful choice of experimental conditions.     

超高纯铜的制备方法和应用

简要介绍了超高纯铜(UHPC)的几种精炼方法，以及它在工业方面的应用。并对超高纯铜的研究开发趋势及应用前景进行了展望。     

喷气纺的条子制备

新纺纱系统的研制开发与传统纺纱工艺的进一步发展都需要对技术要求和经济效果进行反复准确的分析。由于喷气纺的推广，尤其是在美国的推广使用，Rieter公司对此工艺的原材料的最佳准备状态进行了研究。本文即为Rieter公司纺织技术专家所完成的这方面大量研究工作的一个概述。     

阳离子型聚丙烯酰胺絮凝剂的开发与应用

阳离子型聚丙烯酰胺具有许多优点，极具开发研究价值，是重要的高分子絮凝剂。介绍了阳离子型聚丙烯酰胺絮凝剂的制备方法，应用及其絮凝作用机理，并分析了其发展方向。     

石英玻璃基复合材料的研究进展

石英玻璃基复合材料属于重要国防材料，在导弹通讯、制导和防热上具有不可取代的地位。本工作介绍了几种形式的石英玻璃基复合材料的组织结构、性能和制备工艺的研究与应用情况。同时提出了石英玻璃基复合材料研究中存在的问题。     

胶体五氧化二锑研究现状及发展方向

对胶体五乳化二锑的研究现状进行了回顾，详细概述了胶体五乳化二锑的各种制备方法及其特点和适用范围，讨论了两种成胶理论。针对目前存在的问题，对胶体五乳化二锑的研究方向及研究重点提出了几点建议。     

吉利河水库大坝安全运行与管理综述

本文介绍了吉利河水库管理处加强水库安全运行管理的实践和经验，尤其是在洪水调度和险情处置方面积累的经验。