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排序方式: 共有10000条查询结果,搜索用时 187 毫秒
991.
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T. Gallina Toschi M. F. Caboni G. Penazzi G. Lercker P. Capella 《Journal of the American Oil Chemists' Society》1993,70(10):1017-1020
Eight samples of cashew nut oil were assayed, and the component triacylglycerols, fatty acids and several unsaponifiable compounds
were analyzed by gas chromatography (GC) and high-performance liquid chromatography (HPLC). Total lipid amount, unsaponifiable
percentage, fatty acids, sterols, triterpene alcohols and tocopherols are reported here. The combination of GC and HPLC enhanced
the resolution of compound classes. 相似文献
994.
通过熔体插层法以及常压硫化法制备了橡胶/黏土纳米复合材料,并与模压硫化法制备的复合材料进行了对比,研究了硫化方法对橡胶/黏土纳米复合材料微观分散状态的影响。结果表明:采用熔体插层法制备的橡胶/黏土混合物,其受限状态的橡胶大分子链在高温、高压条件下,在黏土片层之间处于一种热力学不稳定状态;模压处理会对橡胶/黏土混合物的分散状态产生不利影响。透射电子显微镜和X光衍射分析表明,采用模压硫化、常压硫化得到的丁基橡胶或丁苯橡胶/黏土纳米复合材料中黏土片层的微观分散状态不同;排除压力的影响,常压硫化有利于提高橡胶/黏土纳米复合材料中黏土片层的分散程度。 相似文献
995.
996.
997.
Phase transitions of canola oil sediment 总被引:3,自引:0,他引:3
H. Liu C. G. Biliaderis R. Przybylski N. A. M. Eskin 《Journal of the American Oil Chemists' Society》1993,70(5):441-448
Canola sediment was obtained from an industrial filter cake by solvent extraction. When heated in the differential scanning
calorimeter (DSC) (5–100°C), the sediment exhibited a single narrow melting peak at around 74.8°C. No solid-state polymorphic
transformation of the material could be detected over this temperature range. The X-ray powder diffraction pattern of canola
sediment resembled waxes from other sources with an orthorhombic unit cell. The phase transition behavior of canola sediment
in oil was studied by both DSC and polarizing microscopy. With increasing ratio of oil/sediment, a reduction in both melting
temperature and transition enthalpy was observed. The shape of the supercooling curve resembled that of the melting curve.
The induction time was determined by spectrophotometry and was used to calculate the interfacial free energyσ between sediment and oil; σ=4.71 erg/cm2. The effect of temperature and sediment concentration on the clouding time of canola oil was studied; the clouding time was
the shortest at 5°C. 相似文献
998.
EPDM foam was prepared by dynamically vulcanizing EPDM compound in a HAAKE rheometer firstly, then mixing the partially precured EPDM compound with a blowing agent and a sulfur vulcanizing system on a two roll mill. The compound was extruded through a cold feed extruder, and the extrudate was foamed in a circulating hot air oven. EPDM compound was vulcanized partly in the HAAKE rheometer, the final torque increases with increasing sulfur content. Rheological measurement shows the dynamic storage modulus, the loss modulus, and the complex viscosity of precured EPDM compound increase with increasing sulfur content. Then the partially precured EPDM compound was compounded with a blowing agent and a sulfur vulcanizing systems, Rheometric measurement shows that the rate of vulcanization of partially precured EPDM compound is not affected by the precure. The blowing results show that the foam processibility could be improved and the expansion ratio increases in the same processing condition for optimum partially precured EPDM compound, which indicates the optimum crosslink density for EPDM could enhance the efficiency of blowing agent AC. SEM shows that the foam articles have a closed‐cell structure with few open cells, and the large cells inlay among the small cells. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 3387–3394, 2006 相似文献
999.
1000.