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91.
Synthesis and properties of polystyrene/graphite nanocomposites 总被引:3,自引:0,他引:3
In this paper, graphite/polystyrene nanocomposite is synthesized by in situ polymerization of styrene in a tetrahydrofuran (THF) solution system of potassium (K)-THF-graphite intercalation compound (GIC). K-THF-GIC has proved to initiate polymerization of styrene by the anionic mechanism. Due to the interfacial interaction between the graphite nanolayers and the polymer, the composites exhibit higher glass transition temperature and higher thermal stability when compared to polystyrene. The percolation threshold in the conductivity of the composites is lesser than 8.2 wt% and the dielectric constant can reach as high as 136. 相似文献
92.
Vinh Q. Nguyen Jas S. Sanghera Brian Cole Pablo Pureza Frederic H. Kung Ishwar D. Aggarwal 《Journal of the American Ceramic Society》2002,85(8):2056-2058
Arsenic sulfide glass optical fibers typically possess extrinsic absorption bands in the infrared wavelength region associated with residual hydrogen and oxygen related impurities, despite using purified precursors. We report a purification process based on the addition of tellurium tetrachloride (TeCl4 ) to the glass. During melting, the chlorine from TeCl4 reacts with the hydrogen impurities to produce volatile products (e.g., HCl) that can be removed by subsequent dynamic distillation. The processing conditions have been modified accordingly to produce optical fibers with significantly reduced loss due to hydrogen sulfide impurity content (1.5 dB/m). 相似文献
93.
94.
Jose Ivan Escalante-Garcia Victor M. Palacios-Villanueva Alexander V. Gorokhovsky Guillermo Mendoza-Suárez Antonio F. Fuentes 《Journal of the American Ceramic Society》2002,85(7):1788-1792
Mortars of blast furnace slag blended with a geothermal silica waste at various replacement levels of 0%, 5%, 10%, 15%, and 20% were cured for up to 90 days. The binder was activated by 6 wt% Na2 O equivalent of sodium hydroxide. Lime was added as an activating agent and also to promote pozzolanic reaction with the silica. It was found that the presence of the silica waste increased the reactivity of the cementitious materials, as measured by means of nonevaporable water. The compressive strength was increased in the presence of the silica, except at the highest replacement level of 20%, the optimum silica replacement was that of 5%–10%. The microstructures of blended slag showed less porosity than those of neat slag mortars. The lime was completely consumed after 90 days of hydration. 相似文献
95.
96.
The LiPO3-Y(PO3)3 system has been studied for the first time. Microdifferential thermal analysis (μ-DTA), infrared spectroscopy (IR) and X-ray diffraction were used to investigate the liquidus and solidus relations. The only new compound observed within this system is LiY(PO3)4, melting incongruently at 1104 K. An eutectic appears at 4±1 mol% Y(PO3)3 at 933 K. LiY(PO3)4 crystallizes in the monoclinic system C2/c with a unit cell: a=16.201(4) Å, b=7.013(2) Å, c=9.573(2) Å, β=125.589(9)°, Z=4 and V=884.5 Å3, which is isostructural to LiNd(PO3)4. The infrared absorption spectrum indicates that this salt is a chain polyphosphate. 相似文献
97.
结合化肥厂丁辛醇装置薄管板换热器的设计 ,着重分析薄管板的特点 ,应用合理的计算方法对薄管板进行强度校核 ,验证这一新型换热器的安全性和经济实用性 相似文献
98.
An ab initio study using the local spin density approximation of the electronic and optical properties of materials where Cr transition metal substitutes for N in the GaN host semiconductor with an atomic concentration of 1.56% is presented. This material, characterized by an isolated and partially filled intermediate band, is a candidate for high-efficiency solar cells. The atomic and orbital composition of this band has been analyzed showing that is mainly made up of a t-group orbital of the transition metal. The absorption coefficient theoretical results show a sub-gap absorption with respect to the host semiconductor which could lead to an increase in solar conversion efficiency. 相似文献
99.
Mostafa Moussaid Stphane Caillet Josphine Nketsia‐Tabiri Cheikh Boubekri Monique Lacroix 《Journal of the science of food and agriculture》2004,84(13):1657-1662
The study evaluated the effects of waxing, irradiation dose and post‐irradiation storage time on the essential oils in orange peel. Mature oranges (Maroc late) waxed or unwaxed were treated with 1 or 2 kGy radiation and stored for 9 weeks at 20 °C and 40–50% RH. Essential oils from the peel were extracted and analysed by GC. Results showed that D ‐limonene was significantly lower in waxed oranges; levels in samples treated with 2 kGy were higher than those in non‐irradiated or treated with 1 kGy. Linalool, methyl anthranilate and 3,7‐dimethyl‐2,6‐octadienal decreased as the dose increased. Levels of linalool increased with storage time but D ‐limonene was unaffected. These results may aid in guaranteeing the quality of orange essential oils during storage time. Copyright © 2004 Society of Chemical Industry 相似文献
100.
The growth of Li1+xMn2O4 via detonation reaction was investigated with respect to the presence of an energetic precursor, such as the metallic nitrate and the degree of confinement of the explosive charge. The detonation products were characterized by scanning electron microscopy. Powder X-ray diffraction and transmission electron microscopy were used to characterize the products. Li1+xMn2O4 with 1-2 μm spherical morphology and more uniform secondary particles, but with smaller primary particles of diameters from 20 to 60 nm and a variety of morphologies were found. The oxides produced by this cheap method affirmed the validity of detonation synthesis of nano-size powders. 相似文献