一个PASCAL结构编辑器的设计与实现

本文对一个新的PASCAL结构编辑编辑器PSE（PASCAL Structured Editor）的系统结构和功能进行了概括的描述。在设计和实现PSE时,作者提出了一种新的程序内部表示法,即所谓“文本-树”表示。与以往的程序内部表示相较,这种表示方法具有占用内存量小,光标控制及编辑操作简便以及无须进行内部语法树与行式文件间的转换等特点。实践证明,基于此种表示的语法制导编辑器是易于实现的,其工作效率是较高的。     

实现铝锭堆垛、称量、打包一体化控制系统

国内大多数铝锭生产企业在铝锭打包过程中。均采用人工作业方式。为此，根据铝锭生产工艺和技术要求以及现代科学生产管理理念。探讨铝锭称量、堆垛、打包一体化控制系统的研究，其主导思想是在原有的铝锭堆垛机控制系统上，实现铝锭自动化流水作业的功能，改变原有的铝锭生产作业方式。     

复杂工作流模式的重构研究*

通过分析在实际工作流中易出现的复杂模式,探究了以往文献中的重构算法不能处理这些模式的原因.通过对算法进行修正,使该算法能够对复杂模式进行有效处理.通过实验证明,改进后的算法仍能保持良好的性能,适用性较强.     

基于Petri网的OLED生产线建模与仿真

介绍了OLED(Organic Light Emitting Diodes)的制造过程及制造系统的PN模型。讨论了Petri网的分析技术。针对OLED制造生产线的复杂性,描述了具体的加工过程。采用结构化方法,综合应用自上而下与自下而上相结合的方法,建立了基于赋时变迁Petri网的OLED制造生产线模型,反映了整个生产线的加工动态特性。利用仿真工具Hpsim,对模型进行了仿真分析,并对其结果进行了定性分析,同时验证了模型的合理性和有效性。     

硝基氯苯的分离

本文叙述了根据硝氯苯的物化性质蒸气压方程，设计了采用高效波纹填料的新流程，并与国内外流程装置作比较，指明了新流程和新装置的优点。．     

顶空-气相色谱法同时测定塑料食品包装袋中11种有机溶剂残留量

采用顶空-气相色谱法对食品塑料包装材料中可能残留的溶剂丙酮、乙醇、乙酸乙酯、丁酮、异丙醇、正丁醇、甲苯、二甲苯等进行了分析。方法采用HP-FFAP色谱柱分离,氢火焰离子化检测器FID检测,11种溶剂能够完全分离,线性较好,样品加标回收率苯系物介于74%～78%,其他溶剂介于86%～95%,最低检出限可达0.002mg/m2。测定了10种不同材质的塑料包装材料中的溶剂残留量和苯系物残留量,方法简便、快速、重现性好,完全能满足塑料包装材料中溶剂残留量的分析。     

三元恒沸精馏生产无水乙醇工艺研究及共轭环的应用

用CHEMCAD软件对乙醇、苯和水三元恒沸体系生产无水乙醇的工艺进行了模拟。根据模拟研究结果设计并建成了年产1 800 t无水乙醇的生产装置。主塔和回收塔中均采用共轭环塔填料。生产实践表明,共轭环塔填料具有传质效率高、单位填料层压降低和操作弹性大的特点;通过对生产工艺的优化,得到无水乙醇产品的苯质量浓度小于0.2 mg/mL,水质量浓度小于0.5 mg/mL。研究结果对设计无水乙醇生产装置有很好的参考价值。     

Continuous production of structured phospholipids in a packed bed reactor with lipase from <Emphasis Type="Italic">Thermomyces lanuginosa</Emphasis>

The possibilities of producing structured phospholipids between soybean phospholipids and caprylic acid by lipase-catalyzed acidolysis were examined in continuous packedbed enzyme reactors. Acidolysis reactions were performed in both a solvent system and a solvent-free system with the commercially immobilized lipase from Thermomyces lanuginosa (Lipozyme TL IM) as catalyst. In the packed bed reactors, different parameters for the lipase-catalyzed acidolysis were elucidated, such as solvent ratio (solvent system), temperature, substrate ratio, residence time, water content, and operation stability. The water content was observed to be very crucial for the acidolysis reaction in packed bed reactors. If no water was added to the substrate during reactions under the solvent-free system, very low incorporation corporation of caprylic acid was observed. In both solvent and solvent-free systems, acyl incorporation was favored by a high substrate ratio between acyl donor and phospholipids, a longer residence time, and a higher reaction temperature. Under certain conditions, the incorporation of around 30% caprylic acid can be obtained in continuous operation with hexane as the solvent. Presented at the 95th American Oil Chemists' Society Annual Meeting and Expo in Cincinnati, Ohio, May 10, 2004.     

Monodisperse‐porous poly(styrene‐co‐divinylbenzene) beads providing high column efficiency in reversed phase HPLC

A multistage polymerization protocol, the so‐called “modified seeded polymerization,” was developed for the production of monodisperse‐porous poly(styrene‐co‐divinylbenzene) providing high column efficiency as a packing material in reversed phase high performance liquid chromatography (RPLC). In the first stage of the multistage production, uniform polystyrene seed particles, produced by dispersion polymerization, were swollen by an organic agent (i.e., the diluent) and then by a monomer mixture containing styrene and divinylbenzene. The final porous particles were obtained in the monodisperse form by the polymerization of monomer mixture in the seed particles. By the use of a small size seed latex with low molecular weight and by the selection of the appropriate diluent, relatively small monodisperse‐porous particles with suitable pore structure could be achieved. In the reversed phase separation of alkylbenzenes, under isocratic conditions, theoretical plate numbers up to 40,000 plates/m were achieved by using 5.2 μm porous particles, obtained by a toluene‐dibutyl phthalate mixture as the diluent. No significant decrease in the resolution power was observed by the fourfold increase in the mobile phase flow rate. The column efficiency and the resolution observed with 5.2 μm monodisperse‐porous particles were significantly higher with respect to the currently available polymer based packing materials used in the reversed phase HPLC. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 95: 1430–1438, 2005     

新型氨氮复合分离流程及装备

开发了全填料结构的吸收，精馏、压缩冷凝新型复合分离流程及装备，用于精细化工氨氮废气（水）的处理，在获得高收率，高纯度的液氨产品同时，基本实现了气、液无污染排放。