熔炼铝青铜吹氩工艺试验

介绍了熔炼铝青铜吹氩工艺。该工艺不仅能解决铸件夹杂、气孔缺陷，而且可使用１００％回炉料进行熔炼。     

冷变形管材残余应力测试与分析

用电阻应变片法测试了变形锡黄铜ＨＳｎ７０－１管材表面的残余应力，分析了拉拔管材变形参数对管材表面残余应力及其他性能指标的影响规律，结果表明，增大管材的减壁变形，可以显著地减小管材表面的拉伸残余应力，当减壁比ｔ０／ｔ１大于１．２时，拉拔管材的残余应力较小，经成品退火后管材晶粒组织细小，采用不同型变形方法生产的管材，其表面残余应力也遵循这一规律，２辊冷轧管材有很大的减壁变形，其表面产生了很大的压应力，     

新型模具铝青铜合金材料的研制

进行了新型模具铝青铜合金材料的试制研究。结果表明，高铝（13％－15％Al)青铜合金中加入Fe、Mn、Ni、Co等多元合金，通过850－880℃油淬固溶＋580－600℃空冷时效处理，可以获得高强韧性β相中弥散分布有（α γ2）沉淀相＋k相的组织。其性能优于国家最高牌号QA110－3－1．5，是替代铁基合金材料制作拉伸、挤压模具的理想材料。     

稀土铈对锡黄铜罐耳件性能的影响

矿井提升罐笼罐耳,由于磨损严重,增加了采煤成本。为了解决罐耳磨损严重问题,研究稀土铈的加入量对罐耳组织和力学性能的影响。通过实验数据的分析,结果表明:适量的稀土铈使锡黄铜组织细化,可以较好的提高锡黄铜的耐磨性。     

Fabrication and structure characterization of ITO transparent conducting film by sol-gel technique

Using In（NO3）3·5H2O and acetylacetone as raw materials and anhydrous SnCl4 as dopant, the transparent conducting indium tin oxide（ITO） films were prepared by sol-gel and dip-coating technique. The phase transformation, structure properties and physical properties （sheet resistance and transmittance） of the films were investigated by DTA-TG, XRD, SEM, four-probe method and UV-Vis spectrometry. The results indicate that it is feasible to fabricate 1TO films on the quartz substrates by sol-gel technique, and the ITO films are formed by accumulating of particles with the size of several decades of nanometers. The prepared ITO film has cubic bixbyite structure, and （111） is its preferred plane. After five-times dip-coating, the 1TO film has a thickness less than 150 nm, a sheet resistance of 110Ω/□, a resistivity of 1.65×10^-3Ω· cm and a transparency of 90% .     

新型铸造铝青铜的润滑摩擦性能

对新型高强度、高耐磨铝青铜合金(代号HSWAB)在润滑条件下的摩擦性能进行了分析.结果表明,HSWAB合金的高耐磨性主要取决于其显微组织,在润滑条件下磨损失效形式主要为磨粒磨损与粘着磨损.由于HSWAB合金基体强度高,强化相呈弥散分布,在润滑摩擦过程中形成高强度的骨架和光滑的支撑面,磨粒细小、圆整、数量少;在润滑及骨架与光滑面的支撑作用下,粘着磨损不能进一步发展,并且合金在摩擦过程中无氧化与裂纹现象产生.     

Wear failure of a leaded bronze bearing: Correlation between plant experience and laboratory wear test data

This paper describes an investigation on the failure of a large leaded bronze bearing that supports a nine-ton roller of a plastic calendering machine. At the end of the normal service life of a good bearing, which lasted for seven years, a new bearing was installed. However the new one failed catastrophically within a few days, generating a huge amount of metallic wear debris and causing pitting on the surface of the cast iron roller. Following the failure, samples were collected from both good and failed bearings. The samples were analyzed chemically and their microstructures examined. Both samples were subjected to accelerated wear tests in a laboratory type pin-on-disk apparatus. During the tests, the bearing materials acted as pins, which were pressed against a rotating cast iron disk. The wear behaviors of both bearing materials were studied using weight loss measurement. The worn surfaces of samples and the wear debris were examined by light optical microscope, scanning electron microscope, and energy-dispersive x-ray microanalyzer. It was found that the laboratory pin-on-disk wear data correlated well with the plant experience. It is suggested that the higher lead content (∼18%) of the good bearing compared with 7% lead of the failed bearing helped to establish a protective transfer layer on the worn surface. This transfer layer reduced metal-to-metal contact between the bearing and the roller and resulted in a lower wear rate. The lower lead content of the failed bearing does not allow the establishment of a well-protected transfer layer and leads to rapid wear.     

铜金粉的颜色及其影响因素

利用分光光度计对国内外铜金粉的颜色进行了测试，研究了铜金粉的成分、微观状态对颜色的影响。结果表明：铜金粉颜色可以用色彩三要素进行描述，其中铜金粉的色相只与合金成分有关，而与铜金粉片的大小、形状及粒度分布无关；明度和纯度与铜金粉片在油墨层中定向排列状态、片的大小、形状及粒度分布有关，而与成分无关；合金成分的微小波动不会引起铜金粉色相的明显改变。     

铍青铜倾角传感器及其线性度补偿

用弹性较好的铍青铜材料作为振动元件,设计制作了“三明治”式差动电容检测结构的倾角传感器、给出敏感头结构尺寸,利用弹性力学分析了传感器的力学特性,推导出被测倾角和铍青铜元件偏角的关系。使用单片机,通过软件线性度补偿,提高了倾角传感器的输出线性度。该传感器结构简单,成本低,稳定性好,使用方便,并经过在全量程范围内测试,最大误差为6°。     

基于氧化石墨烯/聚吡咯-铟锡氧化物微电极的细胞阻抗生物传感器构建及细胞粘附增殖行为检测

构建一种基于氧化石墨烯/聚吡咯-铟锡氧化物GO/PPy-ITO（Graphene Oxide/Polypyrrole-Indium Tin Oxide）微电极的细胞阻抗生物传感器并用于细胞粘附增殖行为学检测。ITO微电极采用光刻技术对感光干膜绝缘层蚀刻而成,通过一步法电聚合技术在ITO微电极表面沉积GO/PPy纳米复合膜制备GO/PPy-ITO微电极;形状测量激光显微镜和扫描电子显微镜分别对GO/PPy表面粗糙度和拓扑形貌进行表征;电化学循环伏安法及阻抗谱表征GO/PPy-ITO微电极的电化学性质;人肺癌细胞株A549粘附、铺展和增殖实验考察GO/PPy界面的生物相容性;以GO/PPy-ITO微电极作为传感电极,利用电化学阻抗谱技术对A549细胞的粘附增殖行为进行检测。结果显示,ITO微电极表面上电沉积的GO/PPy纳米复合物表面平整,分布大量的微孔结构;电化————————————学实验结果显示GO/PPy-ITO微电极比裸ITO微电极具有更低的阻抗特征和更高的电化学活性;GO/PPy比纯PPy膜更能促进A549细胞粘附、铺展和增殖;GO/PPy-ITO微电极表面A549细胞的粘附增殖行为改变电极系统的阻抗谱特征,通过对阻抗谱数据进行等效电路拟合分析获得细胞粘附增殖行为学信息。本文发展的GO/PPy-ITO微电极兼具优良的电化学性质和细胞生物相容性,基于该电极系统构建的细胞阻抗生物传感器可用于细胞病理生理学行为、药物筛选等研究领域。