SO_4~(2-)(S_2O_8~(2-))/Fe_2O_3-SiO_2固体超强酸对乙酸/丁醇酯化反应的催化性能研究

研究了SO2 -4/Fe2 O3 SiO2 固体超强酸对乙酸 /丁醇酯化反应的催化作用 ,得到合适的工艺条件 :复合氧化物中n(Fe)∶n(Si) =1∶2 ,浸渍的H2 SO4浓度 1mol/L ,5 5 0℃预焙烧活化 3h ,催化剂用量 0 .8g ,酯化反应时间 4h ,乙酸的转化率达 96 .3%。在此条件下制得S2 O2 -8/Fe2 O3 SiO2 固体超强酸催化剂 ,并考察了其催化活性 ,实验结果显示该固体超强酸具有更高的催化活性 ,乙酸转化率高达 98.6 %。     

三维地震资料连片的一致性处理技术

三维地震资料连片处理是一套复杂而精细的数字处理工作。根据各区块三维地震资料的频率、相位、时差、信噪比等的特殊性和差异性，采用叠前能量一致性、相位一致性和振幅一致性处理方法，对能量、振幅、相位等有效地进行一致性补偿和校正，使各区块资料在保持原有品质的前提下，既提高了信噪比和分辨率，又保证了资料整体拼接的一致性。应用该方法处理胜利桩海地区23块共1500km^2三维资料，取得了良好的效果。     

聚酯新型催化剂乙二醇锑的工业应用

介绍了国产新型催化剂惭二醇锑在洛阳石油化工总厂聚酯装置上的使用情况，结果表明：乙二醇锑催化剂活性高、易溶解；以乙二醇锑催化剂合成的聚酯产品质量稳定，纺丝时的加工性能明显得到改善。     

己二胺装置第一脱氢塔分离能力不足的原因分析及对策

对新建己二胺装置中第一脱氢塔分离能力不足的原因进行了分析，并采取针对性的措施；从而使己二胺装置整体负荷达到设计能力。     

J2EE项目中数据访问策略的选择

本文介绍了目前J2EE项目数据访问策略的选择，其中重点描述了O／R映射这种数据访问策略的特点及其适用的最佳条件，它可以帮助我们在项目的开发阶段通过清晰的映射方案构造出高效率的DAO层，为项目的成功打下良好的基础，特别是对于项目的式样变更以及后期维护．这种数据访问策略提供了最大程度上的灵活性。     

A simplified cascade current‐source inverter interconnected to a single‐phase three‐wire distribution system and its application to electric energy storage systems with batteries

A novel current source inverter system interconnected to the single‐phase grid is proposed. It has the same construction as the conventional three‐phase current source inverter that is interconnected to the single‐phase three‐wire distribution system. Though the proposed circuit has no output transformer, it can be equivalently performed as the single‐phase double cascade inverter by diverting the pole transformer in the utility system. By controlling the appropriate scheme, the output currents can be obtained as the five‐level waveforms and their distortions can be decreased sufficiently. It is applied to the interactive electric energy storage system with batteries and the basic discharging characteristics are discussed experimentally. © 2004 Wiley Periodicals, Inc. Electr Eng Jpn, 150(2): 50–61, 2005; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.10380     

Enhanced Oil Recovery: The Synthesis of Anthraquinone [1, 2-C] Alkylisoxazole

Anthraquinone [1, 2-C] methylisoxazole is synthesized from 2-ethylanthraquinone through nitration and treating with oleum. The different methods of 2-ethylanthraquinone nitrated were discussed. The optimum conditions were determined. The structure of the product was confirmed by MS and ¹H NMR.     

地震相控非线性随机反演研究与应用

 在地震相模型控制下，通过原始数据将各个单一反演问题转化为一个联合反演问题，可降低反演在描述参数几何形态时的单个反演问题的自由度，从本质上提高地球物理反演的效果。本文在计算过程中采用了非线性随机反演算法，能有效提高地震资料的分辨率，并充分考虑地质条件的随机特性，使反演结果更符合实际地质情况。在胜利、中原油田等地区的储层预测中，应用本文方法均取得了良好的效果，为岩性油气藏勘探提供了可靠基础数据。     

Long-term stability of an Au/Al2O3 catalyst prepared by incipient wetness in continuous-flow glucose oxidation

A 0.3% Au/Al₂O₃ catalyst prepared by the incipient wetness (IW) method was investigated in the continuous-flow liquid-phase glucose oxidation. Therefore, a continuous stirred tank reactor (CSTR) system equipped with an ultrasonic separator was used. The continuous-flow glucose oxidation was carried out at 40 °C, pH 9 and 1 bar oxygen partial pressure. Residence time and glucose concentration were varied. The IW gold catalyst showed very high activity and selectivity to gluconic acid within its 110 days of operation and, thus, an excellent long-term stability. Even after severe microbial contaminations of the catalyst, its activity could be completely restored by in situ regeneration with 2-propanol.