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21.
Preparation of polyimide-epoxy composites 总被引:2,自引:0,他引:2
Kevin Gaw Mitsutoshi Kikei Masa-aki Kakimoto Yoshio Imai 《Reactive and Functional Polymers》1996,30(1-3):85-91
The formation of a three dimensional network of crosslinked epoxy leads all unmodified epoxies to have inherent brittleness and relatively low degradation temperatures. Polyimides, on the other hand, are widely used for applications that require high degrees of flexibility and thermal resistance. Here, we have focused on the preparation of epoxy systems cured with polyamic acids instead of traditional amino-group-containing hardening agents. The cure behavior and potential reaction mechanisms of EPON 828 resin and polyamic acid mixtures were evaluated by DSC and TGA. Thermal analysis showed a complex reaction sequence taking place in the mixture and also determined the extent of reaction of the polyamic acid with itself and the competitive reaction of the polyamic acid with the epoxy. The compositions of the mixtures were varied to see the dependence of the cure behavior on component concentrations. Solutions of the two components did not phase separate and also phase separation was not apparent either optically or microscopically in the cured samples. This phase behavior was attributed to a unique in situ reaction. A novel solvent system for the polyamic acid precursor was also used. 相似文献
22.
聚碳硅烷的分子量分布与可纺性研究 总被引:6,自引:1,他引:5
阐述了聚碳烷的合成及其分子量分布,讨论了高低分子含量对聚碳硅烷熔点及可纺性的影响,而且提出了分子量分布的控制标准与方法。 相似文献
23.
The pumping performance of molecular drag pumps (MDP) has been investigated experimentally. The experimented MDPs are a disk-type
drag pump (DTDP), helical-type drag pump (HTDP) and compound drag pump (CDP), respectively. In the case of the DTDP, spiral
channels of a rotor are cut on both upper surface and lower surface of a rotating disk, and the corresponding stator is a
planar disk. In the case of the HTDP, the rotor has six rectangular grooves. The CDP consists with the DTDP, at lower part,
and with the HTDP, at upper part. The experiments are performed in the outlet pressure range of 0.2–533 Pa. The inlet pressure
and compression ratio are measured under the various conditions of outlet pressure and throughputs, and nitrogen is used for
the test gas. At the outlet pressure of 0.2 Pa, the ultimate pressure has been reached to 1.0 × 10−2 Pa for the HTDP, 1.3 × 10−4 Pa for the DTDP, and 3.6 × 10−5 Pa for the CDP. The maximum compression ratio of the CDP is much higher than those of the DTDP or HTDP. Consequently, the
ultimate pressure of the CDP is the lowest one. 相似文献
24.
W. Tang H.Z. Shi G. Xu B.S. Ong Z.D. Popovic J.C. Deng J. Zhao G.H. Rao 《Advanced materials (Deerfield Beach, Fla.)》2005,17(19):2307-2311
25.
G.O. Phillips S. Al-Assaf A. du Plessis 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2007,265(1):390-393
Using a mediating alkyne gas during the radiation treatment prevents the degradation of natural and synthetic polysaccharides and proteins. The product has higher viscosity and is more elastic than the original material and, therefore, gives enhanced functionality. Protein, within demineralised bone, too can be modified to give enhanced osteoinductive capacity after transplantation. Thus new functionalities can be achieved from the new products produced in food and medical products. 相似文献
26.
The distortion structure in nanocrystalline NiAl is studied using molecular dynamics simulation.The rounded grain boundaries in these nanograins are a direct source for the observed lattice distortion.The change of grain size affects directly the volume fraction of the distorted lattice in the nanograin. 相似文献
27.
Yi Kai Zhou Sung Woo Choi Shigeya Kimura Shuichi Emura Shigehiko Hasegawa Hajime Asahi 《Journal of Superconductivity and Novel Magnetism》2007,20(6):429-432
GaGdN layers were grown at temperatures below 300°C by radio-frequency plasma-assisted molecular beam epitaxy on sapphire
substrates. GaGdN samples with high Gd concentration as high as 12.5% were obtained by lowering the growth temperature. X-ray
diffraction results showed no obvious secondary phase, which means that the phase separation can be suppressed by the growth
at low temperatures. All samples, including those grown at room temperature, showed ferromagnetic characteristics. Photoluminescence
emission was observed, though spectra exhibit broad and sharp luminescence bands related to many kinds of defects. It is suggested
that electrons coming from defects, especially, nitrogen vacancy, stabilize ferromagnetism, and that the carrier-induced ferromagnetism
occurs in the low-temperature-growth GaGdN. 相似文献
28.
Nai-Xing Wang 《Fullerenes, Nanotubes and Carbon Nanostructures》2003,11(3):227-235
Thermal decomposition of C60H2 in C6D4Cl2 solution at 236°C for 2 hours was shown to produce hydrogen as a product, the hydrogen production was successfully followed by NMR. In order to further explore the rule of thermal decomposition of C60H2, the dynamics of decomposition reaction was studied and the results showed this decomposition reaction accorded with first order reaction dynamical equation. The experiment temperature was ranged separately in 459K, 455K, 451K, and 446K. 相似文献
29.
Takuma Suzuki Hang-Ju Ko Agus Setiawan Jung-Jin Kim Koh Saitoh Masami Terauchi Takafumi Yao 《Materials Science in Semiconductor Processing》2003,6(5-6):519-521
We report the successful growth of Ga-polar GaN epilayers on O-polar ZnO templates pre-deposited on c-sapphire. Prior to GaN growth, NH3 is exposed onto the ZnO template. The polarity of the GaN layers is confirmed by etching of the surface and by conversion beam electron diffraction (CBED), while the O-polar ZnO is confirmed by CBED. It is suggested that the NH3 pre-exposure helps form a Zn3N2 layer, which possesses inversion symmetry and inverts the crystal from anion polar to cation polar. 相似文献
30.
A centrifugal partition chromatograph (CPC) was used as a liquid-liquid catalytic reactor for the isomerisation of hexen-3-ol into ethylpropylketone with a water soluble rhodium catalyst. Global mass transfer coefficients were measured and shown to depend on both the nature of the solute and the flow rate. Liquid-liquid partition isotherms were also determined with the CPC using elution chromatography. Finally, a reactor model was derived to account for the experimental results obtained both under stationary and transient (pulse) conditions. A parameter sensitivity evaluation is also presented. 相似文献