Amorphous diffusion bonding of steel pipe and its impact toughness

An iron-based amorphous foil (FeNiCrSiB) was used as an interlayer for the amorphous diffusion bonding of low carbon steel pipes under argon flux. The microstructure and mechanical properties of the joint were analyzed using an electron probe micro-analyzer (EPMA), tensile test, bending test and impact test. The results show that the joint microstructure resembles that of the base metal and no precipitates form at the joint. Melting point depressants (B, Si) diffuse far away from the joint and the base metal element is homogenous across the joint. The joint impact toughness is greater than the base metal toughness and the mechanical properties of the joint are similar around the pipe.     

Structural properties of phosphorous-doped polycrystalline silicon

The structural properties and hydrogen bonding of undoped and phosphorous doped polycrystalline silicon produced by step-by-step laser dehydrogenation and crystallization technique were investigated using Raman spectroscopy and hydrogen effusion measurements. At low laser fluences, E_L, a two-layer system is created. This is accompanied by the change in hydrogen bonding. The intensity of the Si–H vibration mode at 2000 decreases faster than the one at 2100 cm⁻¹. This is even more pronounced in phosphorous-doped specimens. The laser crystallization results in an increase of the hydrogen binding energy by approximately 0.2–0.3 eV compared to the amorphous starting materials.     

API长圆螺纹套管抗粘结性能的试验研究

通过对国内外大量石油套管螺纹参数的测量和全尺寸的模拟试验，以及对测量和试验数据的理论分析，找出了影响国产套管发生粘扣的原因，并在实际生产中实施验证。采取相应的措施改善了套管的抗粘结性能，同时套管的密封和抗滑脱性能并未下降。     

Improved direct bonding method of Nd:YVO4 and YVO4 laser crystals

We succeeded in the fabrication of bonded laser crystals composed of a neodymium-doped YVO₄ laser crystal (Nd:YVO₄) and its host crystals YVO₄ by a newly developed dry etching technique using an argon ion beam. The optical distortion caused by the bonded interface of size 5 mm × 6 mm was estimated to be 0.05λ at 633 nm. From the comparison of laser performance pumped by a laser diode, the bonded crystals could increase the laser output power by nearly twice that of the non-bonded crystals with the same degree of polarization of 99.2%. To analyze the mechanism of the enhanced reduction of the thermal load in the bonded crystals, numerical simulations with a finite-element method were also performed.     

钢／铝合金液固相复合工艺的研究

通过正交试验研究了各工艺量数以钢／铝合金液固相复合性能的影响，最佳工艺条件为铝合金液体温度７９０℃，钢板表面处理为酸洗＋钢刷＋５％的氟钛酸钾助焊剂，复合压力为３９．２ＭＰａ，组织观察表面界面脆性化合物的形成是导致结合强度降低的一个重要因素。     

织构对铟凸点剪切强度的影响

制作了2种形式的铟凸点：即直接蒸发沉积的铟柱和将铟柱回流得到的铟球。同时对比了铟柱和铟球2种凸点的剪切强度，测试结果表明铟球剪切强度为5.6MPa，铟柱的剪切强度为1.9MPa，前者约为后者的2.9倍。对铟凸点微观结构的X光衍射分析发现：铟柱剪切强度低是织构弱化所致；铟球剪切强度高是由于回流破坏了铟柱的理想（101）丝织构模式，从而提高了铟球的剪切强度。     

Al-Cu双金属复合结构的扩散连接试验研究

应用扩散连方法进行了Al-Cu双金属复合结构的试验研究，比较了不同的焊接工艺，材料组合以及母材状态情况Al合金与Cu的连接性，观察了接头区域的微观组织结构，研究表明，固相扩散连接是一种适用于异种材料连接的有效方法，通过在连接区域形成Al-Cu金属间化合物，达到Al和Cu的有效连接，材料组合，母材原始状态以及连接工艺参数对Al合金与Cu的扩散连接存在着明显的影响。表面镀Ni工艺不但能够有效阻止Al和Cu之间形成脆性相，而且Al和Ni之间形成了良好的扩散连接，改善了接头性能。     

金属－橡胶硫化粘接过程中分子取向行为的间接证据

对金属－橡胶热硫化粘接复合体的剥离行为进行了研究，同一粘接试样的双向１８０°剥离试验显示出了巨大的差异。本文分析了弹性材料在硫化过程中的分子行为，并提出了相应的新假设，认为这是由于金属－橡胶在硫化粘接过程中分子取向交联行为所致。这种双向１８０°剥离破坏现象可被看作是金属－橡胶硫化粘接过程中分子取向行为的间接证据。