三峡永久船闸导垂孔施工用电镀金刚石钻头的研制

为了满足导垂孔施工孔径大、垂直精度高（扎斜允许偏差在1‰以内）的要求，本文采用复合电镀技术研制出大口径会刚石钻头，所用胎体材料为镍钴合金，钻进金刚石的品级为MBD8、MBD10，其中MBD10占总量的60％，金刚石粒度分别为40／45、45／50、50／60、60／70，各种粒度的比例（质量比）分别为20％、30％、35％、15％。电镀金刚石钻头在室温下进行，pH值在3～5之间，电流密度在0．5—0．9A／dm^2范围内。文章还提出了基体设计和强化方案，分析了钢体、金刚石参数、胎体对钻进过程的影响，采用混目金刚石扩大了钻头的适用范嗣，提高了钻头的自锐性。使用结果表明：胎体配方、工艺流程、电镀参数和钢体强化没汁是合理的，研制的电镀金刚石钻头在二峡永久船闸倒垂孔钻进中，其平均使用寿命达到16米，钻进时效为0．3～0．5m．     

(TiB_2+Al_3Ti)/ZL101原位复合材料的强化机理

采用透射电镜对(TiB2+Al3Ti)/ZL101原位复合材料中增强相组织、结构和分布进行了研究,测试了(TiB2+Al3Ti)/ZL101原位复合材料的力学性能。结果表明,原位复合材料经热处理后,其抗拉强度、硬度及伸长率都比ZL101基体材料高,分别提高了23.3%、23.5%、14.6%;增强相TiB2和Al3Ti颗粒均匀分布于-αAl基体中,对基体具有显著的晶粒细化效果;(TiB2+Al3Ti)/ZL101原位复合材料主要强化机制为细晶强化、固溶强化、弥散强化和位错强化。     

复合材料微波快速抢修技术在某重型 战机抢修中的应用

我国空军多架现役重型战斗机的结构损伤（裂纹）经用复合材料微波快速抢修技术修复。本文以此为例，详细推介了这一我国独创的快速抢修技术。     

Cu/Al2O3(Cr2O3)复合材料的耐磨损性能

研究了不同工艺制备的Cu/Al2O3(Cr2O3)复合材料的耐磨损性能,结果表明:Cu/Al2O3(Cr2O3)复合材料的磨损机制以磨粒磨损为主.Cu/Al2O3复合材料的耐磨损性能要优于同样条件下制备的Cu/Cr2O3复合材料.当Al或Cr与Cu形成预合金后而进行原位氧化合成的Cu/Al2O3(Cr2O3)复合材料的耐磨性优于当未形成预合金粉末原位氧化合成的Cu/Al2O3(Cr2O3)复合材料的耐磨性.     

WC颗粒/高铬铸铁表面复合材料的应用研究

利用涂覆铸造技术，在灰铸铁表面以WC颗粒增强相／高铬铸铁复合制成耐磨衬板，与球墨铸铁、中锰耐磨铸铁对比试验和装机运行表明，复合材料的耐磨性有较大幅度的提高。在复杂的服役条件下，复合材料衬板的耐磨性具有良好的组织基础，制作工艺简单，有实际应用价值。     

Contact fatigue behavior of nano-ZrO2/Ni coating prepared by electro-brush plating

Nano-ZrO₂/Ni composite coatings were prepared through co-depositing nano-ZrO₂ particles and pure nickel by electro-brush plating (EBP). By analyzing the effects of microstructure, annealing and load on contact fatigue life, the contact fatigue behavior of the nano-ZrO₂/Ni EBP coating was investigated. Furthermore, the contact fatigue behaviors of the nano-ZrO₂/Ni EBP coating and the nickel EBP coating were compared. The results show that the nano-ZrO₂ particles in the as-deposited nano-ZrO₂/Ni EBP coating were partially conglomerated, and the microstructure of the annealed nano-ZrO₂/Ni EBP coating was finer. Under the as-deposited condition, the contact fatigue life of the nano-ZrO₂/Ni EBP coating was much lower than that of the nickel EBP coating. After the annealing process, the contact fatigue life of the nano-ZrO₂/Ni EBP coating was greatly increased and much higher than that of the nickel EBP coating. The scanning electron microscope (SEM) images of the fatigue fracture zones and the transmission electron microscope (TEM) images of microstructure of the deformation layer show that the annealing could improve the ductility of the nano-ZrO₂/Ni EBP coating, and the nano-ZrO₂ particles could restrain the propagation of the fatigue cracks, which contributed to the enhancement of the contact fatigue properties of the nano-ZrO₂/Ni EBP coating.     

晶须转动及其对SiC_W／Al－Ni复合材料高温压缩变形流变应力的影响

本文测定了ＳｉＣＷ／Ａｌ－Ｎｉ复合材料高温压缩变形的应力－应变曲线，讨论了该种复合材料高温压缩变形时所表现出的应变软化现象，利用ＳＥＭ观察了ＳｉＣＷ／Ａｌ－Ｎｉ复合材料在高温压缩变形中晶须的转动，并对晶须长轴的取向分布函数及其与复合材料压缩流变应力之间的关系进行了较为详细的研究．研究结果表明，在压缩变形过程中，ＳｉＣＷ晶须的长轴要发生转动，并趋向垂直于压缩方向分布，晶须取向的重新分布是造成复合材料应变软化的主要原因．     

外场作用下由工业TiOSO4液合成介孔二氧化钛

以工业硫酸氧钛为钛源,采用复合模板合成路线,分别于超声,微波和水热外场作用下合成了介孔二氧化钛前驱体.通过调节反应体系的pH值来控制TiOSO4液的水解和缩聚速率.煅烧脱除模板后得到锐钛型的介孔二氧化钛.产物采用XRD,氮等温吸附脱附,粒度分布,SEM,TEM,SAD和X射线能谱分析(XPS)等技术进行了表征.结果表明具有强极化作用和温和水热环境的外场利于制备结构更佳的介孔二氧化钛;超声振动利于介观结构的形成.在微波辐照下,所制得介孔二氧化钛的比表面积为146.6 m2/g,平均孔径2.57 nm,晶粒尺寸13.65 nm.超声、微波和水热较常规合成方法更利于形成和稳定介孔结构.     

Microstructure and electric properties of Sip/Al composites for electronic packaging applications

Sip/1 199, Sip/4032 and Sip/4019 environment-friendly composites for electronic packaging applications with high volume fraction of Si particles were fabricated by squeeze-casting technology. Effects of microstructure, panicle volume fraction, panicle size, matrix alloy and heat treatment on the electrical properties of composites were discussed, and the electrical conductivity was calculated by theoretical models. It is shown that the Si/Al interfaces are clean and do not have interface reaction products. For the same matrix alloy, the electrical conductivity of composites decreases with increasing the reinforcement volume fraction. As for the same panicle content, the electrical conductivity of composites decreases with increasing the alloying element content of matrix. Panicle size has little effects on the electrical conductivity. Electrical conductivity of composites increases slightly after annealing treatment. The electrical conductivity of composites calculated by P.G model is consistent with the experimental results.     

Al-Zr-O体系反应合成原位复合材料的微结构与磨损特性

运用A359-Zr(CO3)2体系熔体反应法制备了(Al3Zr Al2O3)p/A359复合材料,研究了增强颗粒的含量对(Al3Zr Al2o3)p/A359复合材料干滑动磨损性能的影响.结果表明:Zr(CO3)2与A359熔体反应生成了Al2O3和Al3Zr颗粒;复合材料的磨损量随载荷的增大和时间的延长均远小于基体的,同一条件下复合材料的磨损量随Al3Zr和Al2O3颗粒含量的增加而减少,当载荷为98 N时,12%(Al3Zr Al2O3)p/A359复合材料(体积分数)的耐磨性比基体的提高了2.5倍.磨损表面及亚表面的SEM分析表明,基体A359磨损表面存在撕裂纹并与亚表面连接,表现为粘着磨损和剥层磨损;(Al3Zr Al2O3)p/A359复合材料的磨损表面及亚表面平整光滑,主要表现为磨粒磨损.