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41.
ICP-AES法测定封严涂层中BN含量   总被引:1,自引:0,他引:1  
利用IC-AES法测定了封严涂层的BN,并对样品的溶解方法,仪器工作参数,光谱干扰等进行了研究。方法的相对标准偏差<2%(n=10),加标回收率在95%以上,方法简便,可靠,结果令人满意。  相似文献   
42.
Results are reported of research on intumescent composites based on epoxy resin cross‐linked with polyethylene polyamine and containing ammonium polyphosphate and such modifying additives as calcium borate, manganese dioxide, nickel, and chromium, containing tubulenes as gas‐formers and carbonization stimulators. The changes in composition and physicochemical properties of modified compositions under conditions of heat and fire were investigated by X‐ray photo‐electron spectroscopy, atomic force microscopy, and local force spectroscopy. Ammonium polyphosphate mainly stimulates carbonization processes on the inner surface of a bubble being formed during foam coke formation. The introduction of metal‐containing tubulenes leads to the formation of fire‐retardant and low flammability‐compositions with high coke and carbon structures content. The use of calcium borate in the compositions considerably increases the strength of foam coke being formed. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 1477–1483, 2002  相似文献   
43.
The various parameters related to sol-gel processing are discussed with special reference to those which usually attract less attention but depending on the final product in mind, can play important roles. The versatility of the sol-gel technique in materials preparation is demonstrated by discussing the various products developed at the author’s laboratory by using this processing method.  相似文献   
44.
This study describes the development of multilayer metal-dielectric graded index solar selective coatings in which the metallic volume fraction increases with depth, from top (air–film interface) to bottom (film–substrate interface). The work is based on computer simulation followed by validation through fabrication of the coatings and optical measurements. The influence of the choice of the number of layers present in a graded index composite selective absorber and results obtained for a new destructive interference bilayer (four-layer system) coating, designed using the computer model, were studied. The design and optimization of the composite coating was undertaken using a computer tool developed within this program of research employing Bruggeman and Maxwell–Garnett effective medium formalisms. The design tool enabled all key design parameters, with the exception of particle size and orientation, to be varied systematically to permit the sensitivity of the optical properties of the selective absorber coating to be studied.The model was validated with a supporting program of experimental research in which many different selective absorbers were prepared by co-sputtering of metal and dielectric materials.Although the best compositional gradation can be achieved by increasing the number of layers, the variation in optical performance beyond a certain number of layers is minimal. The destructive interference produced between adjacent layers contributes to the absorptance. The effect of the number of layers (single, four and 10) has been calculated for various materials such as nickel, vanadium, tungsten, cobalt and chromium based coatings. Solar absorptance of 0.98 and 0.96 was achieved by simulation and experimental findings with less than 0.07 thermal emittance at 300 K for 200 nm thick, 4-PGSAC (four-layer system) of V : Al2O3 composites. Other designs showed lower optical performance for all the material combinations regardless of their individual optical properties. Use of such thin film coating on the absorbers of solar thermal appliances can reduce thermal losses significantly, which could be of importance to the relevant industry.  相似文献   
45.
The combination of favorable features of tensile mode dynamic mechanical analysis and torsional braid analysis leads to a useful method for cure monitoring of thermoset coatings. This sensitive technique allows the observation of cure reactions over a wide time and temperature range, thus including gelation and long-term curing in one measurement. Isothermal baking can be simulated realistically, since evaporation of volatile compounds like solvents or blocking agents is not hindered and the sample film is in direct contact with the heating atmosphere. Examples are given showing the cure behavior of automotive clear coats and electro coats depending on parameters like crosslinker type and catalytic agents.  相似文献   
46.
水性木器涂料的研究进展   总被引:6,自引:0,他引:6  
随着环境法规对涂料挥发性有机化合物(VOC)含量的限制,环境友好型水性涂料成为涂料工业的发展趋势。本文综述了水性木器涂料的研究进展。  相似文献   
47.
The determination of the Young’s modulus and damping coefficient Q−1 by means of non-destructive vibrating techniques has been applied to bulk and coated industrial materials. Extensions of a previous analytic model of composite beam allow to determine accurately the macroscopic modulus of each component of multilayered structural materials as coated superalloys or nitride-hardened steels. Furthermore, the study of glasses and polymers has been investigated. An attempt of normalisation of the modulus versus temperature curves allows to establish master curves depending on the specific structure, from metallic glasses to polymeric glasses. Finally a comparison of dynamical modulus and Q−1 values measured between resonant (>1 kHz) and subresonant techniques (10−3 to 10 Hz) in relation to the loading frequencies applied in real conditions has been under folder. For metallic materials such as forged or rolled titanium alloys, the brittle-to-fragile transition occurs abruptly or smoothly with a shift of 300 K following the range of excitation frequencies.  相似文献   
48.
Diamond growth with rates up to 100 to 140 μm/hr was achieved using an oxygen-acetylene combustion spraying technique in an atmospheric environment. Investigations on the processing indicated that the gas flow ratio, substrate position, substrate temperature, temperature distribution, and substrate pretreatment were the most important factors affecting the growth of diamond crystals. Evaluation by means of X-ray diffraction, Raman spectroscopy, scanning electron microscopy, and electron probe microanalysis showed that the synthesized diamond was nearly perfect in morphology, structure, and purity.  相似文献   
49.
The failure of acetabular cups via loosening, migration or fracture is partially related to the stress distribution existing in the acetabular region. The complexity of the investigation of these stresses demands the application of a variety of model testing techniques involving combined embedded strain gauging, finite element analysis, transmission and reflective photoelasticity and crack propagation studies. The application of these procedures are described and the difficulties of obtaining representative loadings and restraints are commented upon.  相似文献   
50.
The thermal decomposition of model extreme-pressure lubricant additives on clean iron was studied in ultrahigh vacuum conditions using molecular beam strategies. Methylene chloride and chloroform react to deposit a solid film consisting of FeCl2 and carbon, and evolve only hydrogen into the gas phase. No gas-phase products and less carbon on the surface are detected in the case of carbon tetrachloride. Dimethyl and diethyl disulfide react on clean iron to deposit a saturated sulfur plus carbon layer at low temperatures (∼600 K) and an iron sulfide film onto a Fe + C underlayer at higher temperatures (∼950 K). Methane is the only gas-phase product when dimethyl disulfide reacts with iron. Ethylene and hydrogen are detected when diethyl disulfide is used.  相似文献   
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