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21.
《Journal of the European Ceramic Society》2020,40(12):3824-3828
Reactive hot pressing was utilized to synthesize and densify four ZrB2 ceramics with impurity contents low enough to avoid obscuring the effects of dopants on thermal properties. Nominally pure ZrB2 had a thermal conductivity of 141 ± 3 W/m K at 25 °C. Additions of 3 at% of Ti, Y, or Hf decreased the thermal conductivity by 20 %, 30 %, and 40 %, respectively. The thermal conductivity of (Zr,Hf)B2 was similar to ZrB2 synthesized from commercial powders containing the natural abundance of Hf as an impurity. This is the first study to demonstrate that Ti and Y additions decrease the thermal conductivity of ZrB2 ceramics and report intrinsic values for thermal conductivity and electrical resistivity of ZrB2 containing transition metal additions. Previous studies were unable to detect these effects because the natural abundance of Hf present masked the effects of these additions. 相似文献
22.
《Journal of the European Ceramic Society》2020,40(2):203-211
ZrB2-SiC coatings with different ZrB2 contents were prepared by liquid phase sintering. The oxidation processes of coatings were explained according to TG results of ZrB2-SiC coatings and powders tested from 298 K to 1773 K. Results show that, increasing ZrB2 content made the weight of the samples changed from weight-loss of 10.04% to weight-gain of 0.14%, while the fastest weight-loss regions were narrowed, whose inflection points reduced from 1310℃ to 1050℃. Increasing ZrB2 content made the relative oxygen permeability of the ZrB2-SiC/SiC coatings reduced from 40%–60% to -10%-5%. Increasing ZrB2 content enhanced high-temperature stability of coatings, making final weight of samples changed from weight-loss of 0.16% to weight-gain of 0.11% after oxidation at 1773 K for 200 h. The peeling and dispersion of Zr-oxides formed Zr-B-Si-O compound glass layer, presenting enhanced stability, dispersion strengthening and pinning effect of Zr-oxides, which were responsible for the excellent anti-oxidation protective effect of coatings in a broad temperature region. 相似文献
23.
This paper deals with the investigation of the effect of hygrothermal conditions on the bending of nanoplates using Levy type solution model employing the state-space concept. The nanoplates are assumed to be subjected to a hygrothermal environment. The two-unknown function plate theory is used to derive the governing differential equations on the basis of Eringen's nonlocal elasticity theory. The governing equations contain the small scale effect as well as hygrothermal and mechanical effects. These equations are converted into a set of first-order linear ordinary differential equations with constant coefficients. Analytical solution of bending response for nanoplates under combinations of simply supported, clamped and free boundary conditions is obtained. Comparison of the results with those being in the open literature is made. The influences played by small scale parameter, temperature rise, the degree of moisture concentration, boundary conditions, plate aspect ratio and side-to-thickness ratio are studied. 相似文献
24.
Andrea Bedon Jean Paul Viricelle Mathilde Rieu Simone Mascotto Antonella Glisenti 《International Journal of Hydrogen Energy》2021,46(27):14735-14747
In this contribution brownmillerite-based nanocomposite cathode for Single-Chamber Solid Oxide Fuel Cells is developed. These cells can be very attractive especially for small and cheap devices because of the absence of seals. The efficiency of SC-SOFCs is strictly connected to the selectivity of anode and cathode, the bottleneck for this technology. The development of a cathode inert in fuel oxidation is particularly challenging. Our strategy is to start from a catalytically un-active support (CFA = Ca2FeAl0.95Mg0.05O5) and induce the formation of iron oxide based nanoparticles, expected to activate oxygen. Symmetric (CFA + FeOx/CGO/CFA + FeOx) and complete cells (CFA + FeOx/CGO/Ni-CGO) are studied in air and methane/oxygen 2:1 mixture. The Area Specific Resistance of CFA + FeOx is less than 1/3 that of CFA. The high selectivity allows to reach an efficiency of 25%; power still needs to be increased but we demonstrated the possibility to develop selective low cost electrodes. The effect of air, methane/oxygen exposure and the heat treatments were carefully investigated. 相似文献
25.
26.
Mechanical behavior of a two-dimensional elastoplastic solid with rectilinear cracks is investigated. Plastic strip model is used to reduce plasticity problem to the equivalent linear elasticity formulation. Two realizations of the mixed mode plastic strip model are considered: in-line plastic strips as proposed by Becker and Gross [Int. J. Fract. 37 (1988) 163], and inclined plastic strips of Panasyuk and Savruk [Appl. Mech. Rev. 47 (1994) 151]. The effective mechanical response predictions are based on the procedure presented in Kachanov et al., [Appl. Mech. Rev. 47 (1994) 151]. Stress-strain relations are obtained for parallel and randomly oriented non-interacting cracks. Results are compared with known elastic solutions. 相似文献
27.
28.
以硬脂酸与氢氧化钠反应生成的硬脂酸钠用作制备固体酒精的固化剂,研究了固体酒精的制备工艺与性能的关系,通过正交试验对工艺条件进行了优化。用40mL酒精溶解2.0g硬酯酸,50mL酒精溶解0.4g氢氧化钠,在70℃下反应30min,制备的固体酒精综合性能最好。 相似文献
29.
电信宽带LAN接入网建设中的有关问题探讨 总被引:1,自引:0,他引:1
文章介绍了采用以太网技术的宽带接入网,对目前以及网宽带接入网建设中存在的问题如安全、维护、投资和计费等进行了研究,提出了解决上述问题的建议。 相似文献
30.
采用丙二酸作为连接,针9-蒽甲醇连接到硅胶上生成硅胶固载的光敏剂。利用此因相光敏剂分别在乙醇和甲苯溶液中敏化反式维生素D3。实验结果表明,此固相光敏剂能够有效地敏化反式维生素D3为顺式维生素D3的反应,并且非常容易从反应体系中分离出来。 相似文献