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101.
The use of thin film grids coated on surfaces is described in relation to the determination of deformations in doubly curved shells. The technique is called the coating film moiré interference method and employs a laser holographic approach. 相似文献
102.
Fusae Nakanishi 《Polymer International》1992,27(3):237-241
Preparation of photoreactive Langmuir-Blodgett (LB) films was carried out using polymers/oligomers prepared from long-chain dialkyl esters of di-and tetra-olefins and having cyclobutane rings in the main chain. These polymers/oligomers formed stable monolayers on a water surface when mixed with arachidic acid. These monolayers could be deposited onto a substrate successfully forming Y-type films. The oligomer LB films were polymerized on irradiation. The polymer LB films showed a photo-reversible process between polymers and oligomers, depending on wavelength of the irradiating light. On the basis of spectral data and molecular weight change, this behaviour was found to be caused by cleavage and formation of cyclobutane rings. 相似文献
103.
M. Saaoudi E. Chassaing M. Cherkaoui M. Ebntouhami 《Journal of Applied Electrochemistry》2002,32(12):1331-1336
Electroless NiP films, with 12 to 16 wt % P, were deposited from a moderately acid solution. Thermogravimetric analysis indicates the presence of occluded hydrogen in the layers, which desorbs upon heating. The amount of incorporated hydrogen decreases when the pH of the solution or the nickel sulfate concentration is increased; by contrast it increases with hypophosphite concentration. Cyclic voltammetry, using an electrochemical quartz crystal microbalance, confirms the existence of parasitic reactions, namely the reduction of protons of the solvent during the cathodic process and oxidation of hydrogen during the dissolution of the layers. This behaviour is in qualitative agreement with the proposed reaction scheme. 相似文献
104.
GaN buffer and main layers were grown by the conventional hydride vapor phase epitaxy technique using GaCl3 consecutively. The deposited buffer layers were investigated by atomic force microscopy and X-ray analysis. To examine the behavior of the buffer layers at main layer growth temperature, heat treatment was conducted at 900°C. Based on the results of the buffer layer study, GaN thick films were grown at 1050°C. Optimum deposition conditions of buffer layer from the buffer and main layer studies generally coincided. On the φ scanning pattern, the GaN films grown on (0001) Al2 O3 were single-crystalline. Band-edge emission dominated photoluminescence was observed at room temperature. 相似文献
105.
用于液晶光阀空间光调制器的ITO透明导电膜的研制 总被引:1,自引:0,他引:1
本文介绍了ITO(Indium Tin Oxide)透明导电膜的制备工艺,对影响其光学和电学特性的因素作了分析。并讨论了透明导电的机理,在K9玻璃上制备的ITO透明导电膜,在500~600nm波长范围内,典型的峰值透过率为90%,面电阻为40~50Ω/□。用该技术制备的样品作为透明电极,在液晶光阀空间光调制器中得到了应用。 相似文献
106.
107.
The optical and thermal properties of prepared poly(ethylene oxide)/MnCl2 films were studied as a function of MnCl2 concentration at room temperature. The observed optical energy gap (Eopt) and energy gap tail (ΔE) were determined from the measured absorption spectra. It was found that the optical energy gap decreases with MnCl2 concentration, and the absorption coefficient reduces sharply at concentration of 5 wt% MnCl2 compared with the neat PEO. Differential scanning calorimetry (DSC) measurement shows that the heat of fusion increases with the MnCl2 concentration, while the melting point decreases. Correlation between the observed optical energy gap and heat of fusion is presented. 相似文献
108.
Sonny g. Sundaresan William R. Finkenstadt 《International Journal of Refrigeration》1991,14(6):317-320
Earlier studies conducted in the use of sealed tubes with polyalkylene glycol lubricants and polyethylene terephthalete (PET) films revealed that the PET films exhibited embrittlement and (visual) degradation. This led to an investigation of PET embrittlement mechanisms with the new lubricants used with HFC 134a. The lubricants studied were three polypropylene glycols (the monol, the diol and the completely end-capped glycols), pentaerythritol ester and a blend of monol and ester. The effects of moisture content, temperature and lubricant structure were studied. All lubricants in this study were of viscosity grade ISO-32 (150 SUS). The results were compared to PET film embrittlement in the presence of CFC 12 and mineral oil. This study reconfirmed the earlier findings that the PET films must be dried to lower than 0.1 wt.% moisture content for use in hermetic systems. This paper discusses the effect of the moisture content of the lubricant and the effect of the lubricant structure on PET films. The dependence of the various mechanisms on temperature is shown. Esters and end-capped polyalkylene glycols are recommended for use with HFC 134a. 相似文献
109.
Polyurethanes were prepared from pure 4,4′-diphenylmethane diisocyanate (MDI), 1,4-butane diol (BDO) or 1,2-ethane diol (EDO) and α,ω-hydroxyl poly(propylene oxide) (PPO) by reaction injection moulding (RIM). Hard segment (MDI + BDO or EDO) level was 45–50 wt%. The PPO had about 20% ethylene oxide copolymerized in at the chain ends to provide 80% primary OH end groups. Mn was varied from 2000 to 4000. Dibutyl tin dilaurate catalyst and mould temperature were varied. Dynamic mechanical, wide-angle X-ray, differential scanning calorimeter, molecular weight and tensile elongation measurements were made on the RIM polyurethanes. At low reaction rates (low catalyst or temperature) highly crystalline, well phase separated but low molecular weight polymers were produced. At high catalyst or temperature levels more poorly phase separated but high molecular weight, tough polymers resulted. Higher Mn PPO gave better phase separation and EDO gave higher melting temperatures. Preventing hard segment crystallinity by substituting asymmetric MDI or glycols resulted in phase compatibility. 相似文献
110.
超高分子量聚乙烯衬板在煤仓中的应用 总被引:2,自引:0,他引:2
介绍了井底煤仓溜煤斜面采用超高分子量聚乙烯衬板安装及应用情况 ,对井底煤仓棚煤原因及解决办法进行了探讨 相似文献