Niobium-containing catalysts—the state of the art

This review article is devoted to the materials containing niobium, which have been discovered or developed in the past few years and exhibit the potential application in heterogeneous catalysis. Niobium oxides and mixed oxides as well as sulfides, nitrides (oxynitrides), carbides (oxycarbides), and phosphates are considered. Among the catalytic processes in which Nb-containing materials were tested, liquid and gas phase oxidation is described in details, and the role of niobium in the prevention of the catalyst from SO₂ poisoning is mentioned.     

磷酸酯类离子液体在燃油深度脱硫中的应用

研究了3种磷酸酯类离子液体,即1,3-二甲基咪唑磷酸二甲酯盐([MM im]DM P)、1-乙基-3-甲基咪唑磷酸二乙酯盐([EM im]DEP)和1-丁基-3-甲基咪唑磷酸二丁酯盐([BM im]DBP)的制备过程,考察了这3种磷酸酯类离子液体对模型油中3-甲基噻吩、苯并噻吩和二苯并噻吩的脱除效果及磷酸酯类离子液体的电化学再生方法。实验结果表明,这3种磷酸酯类离子液体的脱硫能力强弱顺序为:[EM im]DEP>[BM im]DBP[MM im]DM P;且对二苯并噻吩的脱除效果最好,对苯并噻吩的脱除效果次之,对3-甲基噻吩的脱除效果较差。以[EM im]DEP为萃取剂,油剂质量比为1∶1时,经5次萃取后,二苯并噻吩的脱除率可达到99.5%。利用电解法对[EM im]DEP进行了再生,在5~10V电压下电解10h,[EM im]DEP的脱硫率可以达到新鲜[EM im]DEP的90%以上。     

基于MODBUS协议的激光雕刻切割系统HMI人机交互设备

近年来,国内激光雕刻切割控制器技术发展迅速,基于PC的传统控制器已相当成熟.为了显著提高工业生产效率,适应工业生产规模扩张的需要以及工业对系统稳定性要求的提高,目前国内几家专业运动控制器厂家已经实现了激光雕刻切割控制器的完全脱机运行.本文针对脱机控制器的需要设计一款人机交互设备,该设备采用AT89C55WD单片机为主控制器,采用标准的MODBUS协议实现HMI与脱机控制器的可靠通讯.     

脉冲液体射流泵时均值基本方程中的流速系数

运用非恒定的动量方程和时均值计算方法,对脉冲液体射流泵时均值基本方程中的流速系数进行了理论研究,推导出了喉管和喉管进口段流速系数φ2和φ5的计算式。通过与恒定射流的流速系数计算式对比,阐明了脉冲频率是影响φ2和φ5的主要因素,沟通了脉冲射流与恒定射流流速系数之间的关系。     

企业中层管理人员培训的思考

以分析企业中层管理人员培训的现状为突破口,阐述了中层管理人员培训需求分析的思路和方法。在此基础上对培训内容进行整体设计,指出针对此类培训应采用的培训方式和评估方法。以期对企业中层管理人员的培训起到一些启发和借鉴作用。     

浅析FIPS PUB 140-2标准

论文简单分析了FIPSPUB140-2标准及其在密码模块开发过程中的指导意义,可作为密码模块技术开发人员在进行安全性设计时的参考。     

气田集输工艺的选择

近几年我国加快天然气工业的发展，开发了几个大型气田，在与外国石油公司的合作开发中，引进了一些先进的技术及设计理念，集气管道从传统的气液分输工艺发展到气液混输工艺。介绍了气田集输采用的新工艺，分析、总结了各种集输工艺的适用场所。     

Anthocyanin composition of the red wine Babić affected by maceration treatment

Identification of anthocyanins in the wine made of the Croatian autochthonous grape variety of Babić (Vitis vinifera L.) was carried out and their profile was determined by means of high-performance liquid chromatography with diode array and mass spectrometric detection. Dependence of anthocyanins content and profile on maceration treatment conditions was investigated. Statistically significant differences of anthocyanins concentration in wines Babić produced by various maceration treatments were confirmed by the use of multivariate analysis of variances. The investigation results indicated that the maceration temperature exerts higher influence on anthocyanins concentration than the duration of maceration. In addition, on the basis of anthocyanin composition and using different multivariate statistical analyses, differentiation of wines Babić according to maceration treatments was procured.     

Night and Day: Are Siblings as Different in Temperament as Parents Say They Are?

Twin studies suggest that parent ratings of temperament exaggerate differences between twins. The present study examined whether such contrast effects also operate for nontwin siblings. The activity level (AL) and shyness of 95 nontwin sibling pairs (ages 3 to 8 years) were assessed via parent ratings and objective measures (actigraph and observer ratings). Siblings showed no resemblance in either parent-rated AL or shyness; however, sibling resemblance for actigraph AL and observer-rated shyness was substantial. Thus, parents do contrast their nontwin siblings when rating these 2 temperament dimensions. Moreover, the importance of sibling differences in temperament to the sibling relationship and differential maternal treatment varied across the different measures of AL and shyness, suggesting that parent perceptions may play a role in these associations. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

聚合物分散液晶(PMMA:5CB:C60)光折变特性的实验研究

用溶致相分离方法制备了3种不同组分的聚合物分散液晶薄膜(PMMA：5CB：C60)，C60作为敏化剂。利用二波耦合实验测量了不同样品的衍射效率和响应时间等光折变特性，实验发现，液晶含量不同的薄膜光学性质有很大的不同。