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101.
A series of new alternating aromatic poly(ester‐imide)s were prepared by the polycondensation of the preformed imide ring‐containing diacids, 2,2′‐bis(4‐trimellitimidophenoxy)biphenyl (2a) and 2,2′‐bis(4‐trimellitimidophenoxy)‐1,1′‐binaphthyl (2b) with various aromatic dihydroxy compounds in the presence of pyridine and lithium chloride. A model compound (3) was also prepared by the reaction of 2b with phenol, its synthesis permitting an optimization of polymerization conditions. Poly(ester‐imides) were fully characterized by FTIR, UV‐vis and NMR spectroscopy. Both biphenylene‐ and binaphthylene‐based poly(ester‐imide)s exhibited excellent solubility in common organic solvents such as tetrahydrofuran, m‐cresol, pyridine and dichloromethane. However, binaphthylene‐based poly(ester‐imide)s were more soluble than those of biphenylene‐based polymers in highly polar organic solvents, including N‐methyl‐2‐pyrrolidone, N,N‐dimethylacetamide, N,N‐dimethylformamide and dimethyl sulfoxide. From differential scanning calorimetry thermograms, the polymers showed glass‐transition temperatures between 261 and 315 °C. Thermal behaviour of the polymers obtained was characterized by thermogravimetric analysis, and the 10 % weight loss temperatures of the poly(ester‐imide)s was in the range 449–491 °C in nitrogen. Furthermore, crystallinity of the polymers was estimated by means of wide‐angle X‐ray diffraction. The resultant poly(ester‐imide)s exhibited nearly an amorphous nature, except poly(ester‐imide)s derived from hydroquinone and 4,4′‐dihydroxybiphenyl. In general, polymers containing binaphthyl units showed higher thermal stability but lower crystallinity than polymers containing biphenyl units. Copyright © 2005 Society of Chemical Industry 相似文献
102.
浅谈克东县水土流失的成因及存在的问题 总被引:1,自引:1,他引:0
克东县属丘陵地带,土壤主要是黑土。近年来由于水土流失严重,对农业生产和农民生活带来了极大的不便。虽然采取治理与开发相结合的措施,取得了一定成绩,但目前的任务仍然艰巨。 相似文献
103.
104.
本文对力学室一等质量实验室的26、27、32三个公斤工作基准砝码的稳定性误差分别作了分析。经过对历年的检定记录和中间核查的分析汇总,得出各个公斤工作基准的稳定性误差,采用多个砝码多次全组合测量,利用最小二乘法计算出这三个公斤工作基准砝码之间的质量差值,找出它们的稳定性误差的变化趋势。 相似文献
105.
Starting from plysical laws a four-dimensional nonlinear model for mecano-hydraulic servomechanisms is deduced. The stability of its equilibria is analysed using a theorem of Lyapunov and Malkin to handle the critical case due to the presence of zero in the spectrum of the matrix of the linear part around equilibria. Stability diagrams are drawn and simulation results are presented through phase diagrams. 相似文献
106.
This study is concerned with the stability of a two-dimensional incompressible conducting liquid film surrounded by a passive
conducting medium, when an electric field is applied in a direction parallel to the initially flat bounding fluid interfaces.
Currents generate charges at the bounding interfaces which in turn affect the stress balances there. In the absence of an
electric field, the viscous liquid film is stable (instability can be induced by the inclusion of van der Waals forces for
ultra thin films). A complete model is presented, at arbitrary Reynolds number, which accounts for conductivity and permittivity
contrasts between the fluid and surrounding medium, as well as surface tension. The linear stability of the system is considered
for arbitrary Reynolds numbers and it is shown that the stable film can become unstable if, (i) σ
R
ɛ
p
>1, or (ii) σ
R
ɛ
p
<1 and (σ
R
−1)(1−ɛ
p
)<0, where σ
R
is the ratio of outer to inner conductivity and ε
p
is the ratio of inner to outer permittivity. Instability is possible only if the electric field is non-zero and the scalings
near bifurcation points that can be used to construct nonlinear theories are calculated. Several asymptotic limits are also
considered including zero Reynolds numbers and short or long waves. The instability criteria given above are constructed explicitly
in the case of Stokes flow. 相似文献
107.
108.
通过对比混凝土四面体与特大块石这两种截流材料的抗冲稳定性和施工的方便性,分析了混凝土四面体截流材料在工程应用中存在的问题。指出:①混凝土四面体密度、综合稳定系数、化引球形粒径都偏小,在龙口的抗冲稳定性不如特大块石;②混凝土四面体制作麻烦,成本高,占地面积大,装运困难,抛投强度低,施工不如特大块石方便;③在截流施工中宜优先使用特大块石,慎用混凝土四面体。 相似文献
109.
110.