一种高精度磁性参数测试仪设计

设计了一种高精度磁性参数测试仪。该仪器以TMS320F2812为处理器,采用12位串行A/D TLC2588进行数据采集。使用复化Newton-Cotes数字积分算法快速求取磁通值,不仅可以很好地解决模拟积分器带来的零漂问题,而且也提高了积分精度。采用软件实现IIR数字滤波和系统零点的自动修正和补偿。同时通过数字压控恒流源和开关电源技术实现充退磁。与传统的磁性参数测试仪相比,该测试仪具有测试精度高、数据重复性好、性能稳定等特点。     

Superior Magnetic Performance in FePt L10 Nanomaterials

The discovery of the high maximum energy product of 59 MGOe for NdFeB magnets is a breakthrough in the development of permanent magnets with a tremendous impact in many fields of technology. This value is still the world record, for 40 years. This work reports on a reliable and robust route to realize nearly perfectly ordered L1₀‐phase FePt nanoparticles, leading to an unprecedented energy product of 80 MGOe at room temperature. Furthermore, with a 3 nm Au coverage, the magnetic polarization of these nanomagnets can be enhanced by 25% exceeding 1.8 T. This exceptional magnetization and anisotropy is confirmed by using multiple imaging and spectroscopic methods, which reveal highly consistent results. Due to the unprecedented huge energy product, this material can be envisaged as a new advanced basic magnetic component in modern micro and nanosized devices.     

电沉积Co-Pt-W磁性薄膜及其性能的研究

使用电沉积技术制备了磁性能较好的Co-Pt-W薄膜,并研究了pH值对薄膜的成分、结构、表面形貌和磁性能的影响。研究发现:Co-Pt-W薄膜是一种具有fct四方结构的晶态颗粒膜。随着pH值的升高,Co-Pt-W薄膜中Co和W的质量分数下降,而Pt的质量分数增大。pH值过低,析氢作用明显,Co-Pt-W薄膜表面颗粒较大,并且孔隙率高。增大pH值,有利于细化Co-Pt-W薄膜表面颗粒并降低孔隙率,从而提高矫顽力。     

Physical and Magnetic Properties of Calcium-Substituted Li-Zn Ferrite

The effect of Ca-substitution on the physical and magnetic properties of Li_0.3-0.5x Zn_0.4Ca _x Fe_2.3-0.5x O₄ ferrites (x = 0.0, 0.01, 0.02, 0.03, and 0.05), prepared by the standard ceramic method, has been studied. It is found that the saturation magnetization increases up to x = 0.01 and then it decreases. On the other hand, the initial permeability decreased while the Curie temperature remained almost constant with increasing x. The coercivity and remanence ratio increased with increasing x. A. A. Sattar is on leave from Physics Department, Faculty of Science, Ain Shams University, Cairo, Egypt     

Coercivity enhancement of Nd2Fe14B/α-Fe nanocomposite magnets through neodymium diffusion under annealing

The coercivity enhancement of ball-milled Nd2Fe14B/α-Fe nanocomposite magnets was investigated. It was found that the coercivity could be enhanced through mixing a small amount of Nd powder with as-milled Fe-rich Nd-Fe-B powders. The annealed samples were investigated by means of X-ray diffraction, scanning electron microscopy and magnetic measurement systems. Under annealing, some of Nd powders promoted the formation of hard magnetic phase Nd2Fe14B. On the other hand, a few of Nd would diffuse into the interface of Nd2Fe14B/α-Fe nanocomposite to compensate for the loss of the interfacial magnetic anisotropy. These two features are all beneficial to the coercivity.     

WC-Co硬质合金磁性能与晶粒度之间的关系

对硬质合金磁性能与显微结构参数之间的关系模型进行了简短介绍。测量了超细、亚微和中粗晶粒度WC-Co硬质合金的磁性能,并利用扫描电镜或金相显微镜测量对应牌号合金的WC平均晶粒度,建立了一个新的描述WC-Co硬质合金磁性能和平均晶粒度之间的经验关系公式。结果表明,新关系式对于不同合金牌号合金具有较高的准确度和良好的应用效果。     

Sm-Co/α-Fe双层膜和多层膜磁反转的微磁学模拟

采用微磁学模拟软件OOMMF,详细研究了软/硬磁层总厚度不变,结构的变化对Sm-Co/α-Fe薄膜磁性能和磁反转过程的影响。结果显示,从双层膜变化到多层膜的过程中,不同的结构具有不同的磁性能和磁反转过程;当结构优化为Sm-Co(7.5 nm)/α-Fe(2.5 nm)/Sm-Co(5 nm)/α-Fe(2.5 nm)/Sm-Co(7.5 nm)多层膜时,最大磁能积和矫顽力相比Sm-Co(20 nm)/α-Fe(5 nm)双层膜大幅度提高,分别为1015.44 k J/m3和μ0Hc=1.891T。此结论对高性能交换耦合类磁性薄膜的研究具有一定的指导意义。     

高性能各向异性Sm_2Co_(17)纳米永磁材料的制备与表征

利用表面活性剂辅助高能球磨(SA-HEBM)分别制备了高性能的各向异性Sm2Co17纳米永磁粉末材料,然后对球磨产物进行超声波分散清洗。利用高速离心技术进行纳米颗粒分级,获得颗粒尺寸分布狭窄的纳米永磁颗粒,对所得粉末进行适当的快速热处理。分别采用扫描电镜、X射线衍射和振动样品磁强计分析、测试样品的显微形貌、相结构和室温磁性能。结果表明,粉末的厚度在80 nm左右,长度为亚微米级,具有高比表面积、强形状各向异性与磁各向异性;经过磁场取向后,Sm2Co17的易磁化轴和难磁化轴方向的室温矫顽力分别达到612.9 k A/m(7.7 k Oe)和278.6 k A/m(3.5 k Oe);表面活性剂在球磨过程中起到了重要作用。     

B掺杂FePt基纳米复合膜的制备与磁学性能研究

利用磁控溅射法将厚度可控的B掺杂到FePt多层膜中,构成FePtB多层膜体系。多层膜结构采用中间层掺杂和底层掺杂等方式组合,由此研究热处理温度与B掺杂对FePtB多层膜体系磁学性能的影响,分析成相过程。另一方面,B层作为中间层掺杂到FePt多层膜样品中构成不同B掺杂浓度的多层膜体系,通过X射线衍射等表征手段研究不同的掺杂浓度对FePt多层膜样品成相及退火温度的影响。实验结果表明,B掺杂的FePt多层膜样品的矫顽力大幅度提高,出现垂直择优取向;随着B层厚度的增加,FePtB多层膜体系的磁有序相比例增加,当B层为14nm时,FePtB多层膜体系展现良好的垂直取向特性。此外,B掺杂降低了FePt多层膜样品的退火温度。     

添加Bi_2O_3对锶铁氧体微观形貌及内禀矫顽力的影响

采用传统的高温固相合成方法制备了添加Bi2O3的锶铁氧体粘结磁粉,研究了不同焙烧温度和时间下Bi2O3对锶铁氧体相组成、微结构以及内禀矫顽力的影响。结果表明,添加1wt%Bi2O3的试样中,由于含Bi液相的生成,在1050℃的较低温度下促进了铁氧体化反应和晶粒生长,从而显著提高SrM的内禀矫顽力。在添加1wt%Bi2O3的情况下,获得的锶铁氧体颗粒尺寸在1.2μm附近,球形度较佳,同时具有超过300kA/m的内禀矫顽力,可应用于制备高填充型粘结铁氧体磁体。