热场致发射电子源曝光系统的技术现状和应用前景

高亮度、长寿命的热场致发射(Thermal field emitter)阴极自七十年代中期已受到人们的关注和重视,历经十多年在理论分析、工艺制备和实验研究上做了大量工作之后,于1988年在电子束曝光机上的应用中取得了突破性进展。用晶向为(100)的钨和具有低逸出功的锆制成的(Zr/O/W)热场致发射阴极在四千小时的使用寿命下亮度值超过六硼化镧阴极一个数量级以上,最近的实验结果表明:在工件台上小束斑下能得到接近两千安培每平方厘米的束流密度,而且四十小时内束流稳定度接近千分之一。显然,这几个表征曝光系统综合技术性能的重要指标,说明多年困扰于各种电子束曝光系统(特别是高斯圆斑电子束系统)在高分辨率情况下生产率较低的技术难题已经得到了比较圆满的解决。 八十年代末期,当热场致发射电子源曝光系统的技术关键解决后,这项技术就成为技术发达国家,特别是美国和日本,在电子束曝光领域进行技术竞争的热点;九一年五月底在美国召开的国际三束会议上有关场致发射阴极和MEBES—4型机已经采用TFE的最新报道充分证实了这项技术在电子束曝光技术应用中的重要地位和发展潜力。     

Interaction between bubbles and fibre optic probes in a bubble column

Spherical bulb fibre optic probes, developed and applied for bubble characterization in a bubble column and a slurry bubble column at high temperature, were investigated. The principle of operation of these new optical fibre probes is based on the difference in refractive indices between the gas and the liquid phases. The interaction between the gas bubbles and the fibre optic probes in a bubble column was studied using photographic techniques. The first objective of these experiments was to study the response of the sensors upon contact with gas bubbles of various sizes. The second objective of this study was to establish, under controlled situations, the optical probe bubble detection performance and ability for local quantitative measurements of the bubble rise velocity and the gas hold-up.     

铝合金电磁铸造工艺参数的研究

通过近似计算和试验确定了工程规模的铝合金电磁铸造（ＥＭＣ）基本工艺参数如感应器电流、电压、频率、功能消耗等一液柱高度及稳定性的关系，设计制造了ＥＭＣ装置，成功地铸造了截面直径为０．１８ｍ，０．１１×０．０５ｍ，０．５２×０．１３ｍ的铝及铝合金锭和扁锭。     

Kinetics of oxygen absorption in aqueous sodium dithionite solutions

The absorption and reaction of oxygen in aqueous alkaline solutions of sodium dithionite has been experimentally investigated in a novel gas-liquid contactor. The novel gas-lift bubble column contactor was used to study the kinetics over wide ranges of reactant concentrations, temperature, and pH. The oxygen-sodium dithionite reaction was found to be first-order with respect to dithionite in the range of dithionite concentration < 0.1 M, and second-order in the range of dithionite concentration > 0.1 M. The reaction with respect to oxygen was found to be zero-order for all dithionite concentrations. These results and experimental investigations of the effect of solution alkalinity and temperature on the reaction rate are consistent with previous findings obtained in different gas-liquid contactors. The results thus confirm the feasibility of using the gas-lift bubble column for the kinetics of gas-liquid reactions.     

异丁醛氧化制丙酮热导气相色谱分析

本工作用２米４０１有机担体填充柱，在带四臂热导检测器的国产１０３型气相色谱仪上，仅８分钟将原料异丁醛、产物丙酮及水进行良好分离，并采用内标法定量，其最大平均偏差在±２％以内。方法简单、快速、准确     

Erosion-corrosion of a stainless steel distillation column in food industry

Unusual extended corrosion phenomena were detected in a distillation column made in AISI type 316 stainless steel (UNS S31600) of a plant for natural pectins extraction from citrus. The column was the first of a series of two distillation columns representing the unit core. Corrosion problems were observed only in that column and mainly along the surface of the trays located in the lower section of the column. The phenomenon was observed subsequently to a modification of the original plant layout that caused an increase of the operating temperatures and turbulence of the process stream inside the column.     

应用列对象的Tag属性实现多表数据动态查询

探讨在PB开发的应用程序中利用数据窗口列对象的Tag属性,结合自行设计的一个更改SELECT语句中的Where子句的全局函数,实现应用程序多表数据的动态查询。该种方法是PB开发的应用程序中实现数据查询的一种高效、简洁且行之有效的方法。     

基于湿润锋前进法的不同应力状态砂质黄土土柱渗流试验

由于试验装置的局限性,非饱和土渗透特性的研究大多未考虑应力对渗透系数的影响。为探讨水-力耦合作用下砂质黄土的渗透特性,自主研制了一套水-力耦合试验装置。采用湿润锋前进法探究了不同初始干密度和轴向力对非饱和渗透系数的影响,得到水-力耦合作用下非饱和黄土渗透性和轴向位移的演化规律。结果表明:(1)砂质黄土的渗透系数随基质吸力的增大而减小,在不同测试截面处渗透函数曲线出现分层现象;(2)土体的渗透系数随初始干密度和轴向力增大而减小;(3)随轴向力增大,不同初始干密度土柱的稳定渗透系数趋向一致;(4)砂质黄土具有较大的水敏性,在水-力耦合作用下土体结构破坏,导致湿化前后轴向位移差异较大。     

堆石混凝土单轴受压应力-应变全曲线试验方法研究

为了研究堆石混凝土应力-应变全曲线,采用碟形弹簧与钢柱组合成附加刚性元件增强压力机的刚性,研究了碟形弹簧并联与串联联结装置的变形量和刚度以及实现单轴受压端部减摩措施,提出了一种堆石混凝土单轴受压应力-应变全曲线的试验方法。在混凝土压力试验机上进行了堆石混凝土立方体试件单轴受压试验,测得了堆石混凝土受压应力-应变全曲线。试件破坏形态表明,采用的端部减摩措施有效,测得的应力-应变曲线下降段验证了碟形弹簧与钢柱组合装置能够吸收试件破坏时混凝土压力试验机存储的变形能。研究结果为在混凝土压力试验机上进行堆石混凝土单轴受压应力-应变全曲线提供了可行、简便、经济的测试方法。     

多目标优化策略在精馏过程中的应用研究

针对精馏塔自由度多,能耗大,扰动复杂多变,控制和优化要求高等特点,提出了一种基于动态矩阵控制(DMC)的二层多目标优化控制策略。在实现精馏过程控制目标的前提下,设计了二层优化指标,可在有多余自由度的情况下,进行二层控制和优化,实现精馏过程质量控制目标和经济运行优化。通过对Shell多侧线精馏过程的仿真研究,验证了二层多目标优化控制策略的有效性。与DMC控制相比,二层多目标优化控制策略可以明显改善精馏塔运行的经济性,实现增加收益的目标。