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131.
132.
Archis A. Yawalkar Albertus B. M. Heesink Geert F. Versteeg Vishwas G. Pangarkar 《加拿大化工杂志》2002,80(5):791-799
Gas hold‐up (?G) in air‐aqueous electrolyte solutions in stirred tank reactors (STR) is correlated using a relative gas dispersion parameter, N/Ncd and a surface tension factor (STF), (c/z)(dδ/dc)2. For electrolyte concentration below transition concentration (ct) a single correlation in the form of ?G = f(N/Ncd, vvm, STF) shows good agreement with gas hold‐up data over a wide range of system and operating conditions. Above ct no effect of STF on gas hold‐up is observed and the correlation obtained is of the form ?G = f(N/Ncd, vvm). Data available in the literature on large STR show good fit with the proposed correlation. 相似文献
133.
Heat-treated activated carbon has been oxidized to improve the properties related to the use as a support for the preparation
of 5wt% Ru/C catalysts by impregnation. The pore structure, surface oxygen groups of the heat-treated activated carbon before
and after oxidation in the gas and liquid phase, as well as catalytic activities and dispersion of Ru in the catalysts were
investigated systematically. The pore structures of the samples were characterized by N2 physisorption. Temperature-programmed desorption (TPD) was conducted to determine the chemical properties of the samples.
Ru dispersion was measured by CO pulse chemisorption. The effects of oxidation treatments on carbon surface chemistry and
pore structure which are closely related to Ru dispersion and catalytic activity, was examined. Furthermore, the modified
heat-treated activated carbon support obtained by gas phase oxidation in CO2 and liquid phase oxidation in nitric acid was more suitable to prepare Ru-based catalysts for ammonia synthesis than that
without treatment. 相似文献
134.
135.
Eric Jorge Thierry Chartier Phillippe Boch 《Journal of the American Ceramic Society》1990,73(8):2552-2554
Ultrasonication is very effective in dispersing alumina and barium titanate slurries. When optimum conditions are used, very short durations (2 to 3 min) are enough to achieve well-dispersed, stable suspensions. 相似文献
136.
Computational fluid dynamics (CFD) simulations have been carried out to simulate a turbulent, bubble plume in a liquid pool. A two-fluid enhanced k-? model has been used, with the extra source terms introduced to account for the interaction between the bubbles and the liquid and transient calculations have been performed to study the plume growth, the acceleration of the liquid due to viscous drag, and the approach to steady-state conditions. In order to obtain correct spreading of the plume observed experimentally, it was observed that interfacial forces like lift and turbulent dispersion plays important role. The sensitivity analysis for drag coefficient and two different turbulent dispersion forces is presented. The development of the flow variables has been compared with the experimental data. From the CFD predictions obtained in the present work, it can be concluded that a two-dimensional (2D) axisymmetric assumption in this case is justified, with 2D model predictions in good agreement with the experimental data and those of a three-dimensional (3D) model, except for the shear stresses and turbulent kinetic energy. In general, quantitative comparison with the experimental data has revealed that, by applying proper models of inter-phase momentum transfer, and performing simulations based on the two-fluid model, satisfactory predictions of mean flow quantities can be obtained for this application away from the injector. 相似文献
137.
Yinzhong Guo Vijay M. Mannari Pulin Patel John L. Massingill 《Journal of Coatings Technology and Research》2006,3(4):327-331
A series of soybean oil phosphate ester polyols (SOPEP) was prepared by reaction of fully epoxidized soybean oil with phosphoric
acid and simultanoeous hydrolysis in the presence of a polar solvent. The polyols were characterized by determination of acid
value, oxirane number, hydroxyl value, molecular weight (GPC), and FTIR spectra. These polyols with varying amounts of acid
phosphate groups could be self-emulsified to form aqueous dispersions after neutralization with organic base. These aqueous
dispersion showed varying degrees of stability and their appearance ranged from opaque dispersions to translucent to clear
solutions. Waterborne coating compositions were prepared using these aqueous dispersions as principal components and their
thermally cured film properties were studied. it was found that by careful selection and formulation, SOPEPs can be successfully
used for low-VOC waterborne coating formulations. SOPEPs with 3.5% phosphate ester content showed visibly superior corrosion
resistance properties. 相似文献
138.
Reactive mixing in a wavy torus reactor (WTR) has been examined experimentally. Its performances are compared to these of two other reactors: a plane torus reactor (PTR) and a baffled stirred tank reactor (BSTR). hydrodynamics of mixing has been studied using a plug flow model with axial dispersion for the WTR and PTR. The effect of axial dispersion on the kinetic of a chemical reaction was then analysed for the WTR, PTR and BSTR. Mixing times were slightly longer for the WTR due to a weaker axial dispersion. We also noticed an improvement of the convertion rate for low dissipated power. 相似文献
139.
讨论了悬浮聚合反应器的放大问题及计算机控制技术,介绍了具有预分散器的悬浮聚合反应器和连续悬浮聚合反应器。 相似文献
140.
Monolayer vanadium species are mainly in the V(V) valence state, but with XPS a small fraction of V4+ species are identified. Prolonged analysis treatment increases the V4+ concentration. With increasing vanadium concentration, a monolayer coverage corresponding to 1 mg V2O5 per m2 develops, and it contains additional layers with a thickness of about 250 Å at 4 mg V2O5 per m2, covering 3% of its surface area. 相似文献