Measurement of longitudinal distribution of solids holdup in a three-phase fluidized bed by ultrasonic technique

A method of measurement of solids holdup in a three-phase reactor by analyzing the shape and the phase lag or lead of an ultrasonic wave has been proposed. The solids holdup in a solids-dilute three-phase fluidized bed could be measured without being affected by the presence of gas bubbles. The experimental values of solids axial dispersivity measured by the ultrasonic technique are in reasonable agreement with an empirical correlation of previous data obtained by other methods. The possibility of the application of the ultrasonic technique to the measurement of solids holdup in a three-phase fluidized bed has been suggested.     

Variability of light absorption properties in optically complex inland waters of Lake Chaohu,China

Absorption coefficients of phytoplankton, colored detrital matter (CDM), non-algal particles (NAP), colored dissolved organic matter (CDOM), and their relative contributions to total non-water absorption (a_t ? w) are essential variables for bio-optical and radiative transfer models. Light absorption properties showed large range and variability sampled at 194 stations throughout Lake Chaohu between May 2013 and April 2015. The a_t ? w was dominated by phytoplankton absorption (a_ph) and NAP absorption (a_d). The contribution of CDOM absorption to a_t ? w was lower than 30%. Phytoplankton and NAP were the primary sources of spatial and vertical variability in absorption properties. Light absorption by CDOM, though significant in magnitude, was relatively constant. CDM absorption (a_dg) was dominated by NAP. The spatial variation of the absorption coefficients from each of the optically active constituents were driven by several main inflow rivers in the western and middle part of Lake Chaohu. Algal blooms and bottom resuspension contributed to vertical variability as observed by phytoplankton and NAP profiles. Specific absorption of phytoplankton had significant spatial and seasonal variations without vertical variation. The spectral slope of absorption showed no significant spatial variability (p > 0.05). Variations of absorption affected different ranges of remote sensing reflectance (R_rs) spectrum, thereby increasing the difficulty of applying the remote sensing algorithm in optically complex waters. Parameters and relationships presented in this study provide useful information for bio-optical models and remote sensing of lakes similar to Lake Chaohu in terms of optical properties.     

基于总体最小二乘法的系统响应修正方法

为了提高实时洪水预报的预报精度,提出了基于总体最小二乘平差理论的系统响应方法。传统的系统响应方法基于最小二乘法,只能考虑观测值的误差,因而传统的系统响应方法不能考虑动态系统响应矩阵存在的误差。对传统方法进行了分析并引入了总体最小二乘平差理论,改进方法同时考虑了动态系统响应矩阵和观测值的误差。针对动态系统响应矩阵的病态情形,通过总体最小二乘的岭估计解法给出稳定解。通过改进方法对新安江模型中的土壤含水量进行修正,应用于七里街流域,并与传统的系统响应方法进行比较。结果表明,两种方法都能提高模拟精度,改进方法相比于传统方法精度明显提升;改进方法的修正效果要优于传统方法,更加稳定。     

中国部分河口及其近海水域缺氧现象研究

对长江、珠江等河口及其近海水域缺氧现象与影响因素进行研究,结果表明,主要分布于长江与珠江河口及其邻近海域的缺氧现象,夏季(6—8月)达到最盛,秋冬季消失;长江口的缺氧区域主要位于30.75°N~32°N,122.5°E~123.25°E附近海域,具有南北2个缺氧中心;珠江口缺氧程度相对较轻,缺氧区域主要在广州黄埔区河段至虎门水域和伶仃洋;辽河、钱塘江、海河等河口区域也时而出现零星的缺氧现象;水体缺氧受控于多项环境要素,物理层化作用是缺氧产生的最初诱因之一,陆源污染物的分解则是重要的耗氧负荷;各河口区特征各异,潮汐、洋流、营养盐、叶绿素a等要素对缺氧区的范围、程度和持续时间影响程度不一。     

城市径流总量控制指标分解及实现路径探索与实践

针对海绵城市径流总量控制目标,提出一种在城市规划体系中控制性详细规划和修建性详细规划阶段分解落实年径流总量控制率的方法。在控制性详细规划阶段分解径流总量控制指标时,分步骤先后确定各项低影响开发措施的面积率和下沉深度;在修建性详细规划阶段,配合径流总量控制指标分解结果,给出适宜的各项低影响开发措施的技术实施导则,以保证各单项指标的正确实施,并以某项目为例介绍了技术实施导则的构建方法。     

Particle velocity and solids circulation rate in a jet-spouted bed

Radial distribution of particle velocities, solids circulation rate and radial variation in bed voidage in a jet-spouted bed were investigated in a 0.2 m diameter conical-cylindrical column. The upward particle velocity is strongly dependent on gas velocity and its radial profile is the Gaussian. The solids circulation rates are of the same order of magnitude as those in a conventional spouted bed and are proportional to the gas velocity. Estimation of the variation in bed voidage in the radial direction revealed that the annulus voidage of about 0.90 was greater than the spout voidage of around 0.70. This tendency is contrary to that in a conventional spouted bed.     

双颗粒提升管中细颗粒的混合行为研究(Ⅱ)──弥散颗粒的轴径向混合行为

利用磷光颗粒示踪技术，使用点源示踪的方法在不同的径向位置测得反映颗粒径向扩散行为的停留时间分布曲线，并对弥散细颗粒的径向混合行为进行了分析．提出二维扩散模型描述所测量的停留时间分布曲线特征．实验发现弥散细颗粒的径向扩散Peclet数随粗颗粒加入量的增加而增加，随细颗粒浓度的增大而增大，而几乎不随气速变化．给出了一个与实验数据吻合较好并可适用于单颗粒提升管的关联式．     

虎杖中抗氧化成分的提取分离及其活性研究

提取了虎杖中具有抗氧化活性的总蒽醌(TA),并从总蒽醌中依次分离出强酸成分(SAP)、中酸成分(MAP)和弱酸成分(WAP)。然后采用二苯代苦味酰自由基(DPPH)法对不同质量浓度的TA、SAP、MAP和WAP进行了抗氧化活性测定。TA、SAP、MAP和WAP质量浓度分别为0.2 g/L、0.5 g/L、0.8 g/L、1.2 g/L时,对自由基的最大清除率依次分别为:29.5%、67.1%、85.7%、87.5%;34.0%、74.2%、86.5%、95.4%;9.8%、24.0%、35.2%、47.3%;6.5%、11.1%、19.6%、19.9%。TA、SAP、MAP和WAP对自由基均有程度不同的清除作用,其中SAP的效果最佳,当其质量浓度为1.2 g/L时,最大清除率可高达95.4%。     

蛋壳中钙镁含量的测定

分别采用酸碱滴定法、配位滴定法和氧化还原滴定法测定了普通鸡蛋壳的钙镁总量，并对上述三种方法进行了比较，从中选择出较适合教学的方法为配合滴定法。采用配位滴定法分别测定了普通鸡蛋壳、山鸡蛋壳和乌鸡蛋壳的钙镁总量分别为95．34％、97．03％、83．28％，从中选择出较适合教学的鸡蛋壳为普通鸡蛋壳。     

涂料剖析

简要分析了不同涂料体系分析程序,说明了每种涂料剖析体系中应该注意的事项。