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21.
高温预析出对Al-Zn-Mg系铝合金时效硬化和应力腐蚀的影响 总被引:1,自引:0,他引:1
研究了高温固溶后降温处理工艺对中强可使预析出LC52和7039铝合金的组织、时效硬化和应力腐蚀的影响。金相观察发现,高温预析出可优先在晶界处产生,并提高随后时效状态下晶界析出相的不连续分布程度,温度降低到一定程度晶内和晶界产生大量析出。合金拉伸性能和应力腐蚀结果表明,预析出在保持强度和塑性的同时,可提高抗应力腐蚀性能。而预析出温度降低,合金强度呈下降趋势。 相似文献
22.
Fabrication of Fe-, Ni- and FeNi-coated Al2O3 core-shell microspheres by heterogeneous precipitation 总被引:1,自引:0,他引:1
The precursors with NiCO3·2Ni(OH)2·2H2O-, Fe2O3·nH2O-, or both of NiCO3·2Ni(OH)2·2H2O- and Fe2O3·nH2O-coated alumina microspheres were prepared, respectively, by the aqueous heterogeneous precipitation using metal salts, ammonium hydro-carbonate and -Al2O3 micropowders as the starting materials. Subsequently, magnetic metallic Ni-, -Fe- and γ-FeNi-coated alumina core-shell structural microspheres were successfully obtained by thermal reduction of the as-prepared precursors at 700 °C for 2 h, respectively. Optimized precipitation processing parameters of the concentration of alumina micropowders (15 g/L), the rate of adding reactants (5 mL/min) and pH value were determined by a trial and error method. Powders of the precursors and the resultant metal (Ni, -Fe, γ-FeNi alloy)-coated alumina micropowders were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The experimental results show that it is possible to adjust metal coating thicknesses and fabricate multilayer structured metal/ceramics core-shell microspherical powder materials and these materials may be applied for high performance of functional materials and devices. 相似文献
23.
Tomi Gominek Andrej Lubej Ciril Pohar 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(8):939-947
Precipitation of calcium sulfate dihydrate, gypsum, from (i) a pure sulfuric acid/lime suspension and (ii) a waste sulfuric acid/lime suspension in a continuous pilot plant in the temperature range from 40 °C to 80 °C was studied. It was observed that in the case of waste sulfuric acid with a high content of Mg2+ and Fe2+ ions, several hours after the beginning of the precipitation, partial dissolution of the product and modification of the crystals from needle‐ and plate‐like to agglomerated structures occurred. It is suggested that the secondary changes occur due to the increased concentration of Mg2+ and Fe2+ ions in the reactor. Below 60 °C, and above 70 °C plate‐like and needle‐like single crystals respectively were formed. The mean size (d50) of the crystals was found to increase with increasing temperature and decrease with the initial concentration of lime. Gypsum produced between 70 °C and 80 °C is suitable for further processing for construction plaster. In a precipitation process with pure sulfuric acid only single perfect needle‐like crystals occurred. Copyright © 2005 Society of Chemical Industry 相似文献
24.
Atmospheric corrosion of reference metals in Antarctic sites 总被引:1,自引:0,他引:1
Manuel Morcillo Beln Chico Daniel de la Fuente Elisabete Almeida Günter Joseph Susana Rivero Blanca Rosales 《Cold Regions Science and Technology》2004,40(3):165-178
This paper presents the results obtained at three Antarctic test sites participating in the “Ibero-American Map of Atmospheric Corrosiveness” (MICAT), a project on atmospheric corrosion carried out during the period 1988–1994 at some 70 sites distributed across 12 countries of the Latin-American region, Spain and Portugal. The three Antarctic sites are located near the coastline.The singular climatic characteristics of Antarctic regions are related with the purity of the air, the absence of rainfall and the formation of ice on the metallic surface during an important part of the exposure time. However, electrochemical activity is possible below ice layers. This situation affects the structure and morphology of corrosion product films and the resulting corrosion rates of metallic surfaces. 相似文献
25.
G. N. Churilov R. B. Weisman N. V. Bulina N. G. Vnukova A. P. Puzir L. A. Solovyov S. M. Bachilo D. A. Tsyboulski G. A. Glushenko 《Fullerenes, Nanotubes and Carbon Nanostructures》2003,11(4):371-382
The addition of metallic Ir and Pt to a fullerene-forming, atmospheric-pressure plasma reactor was found to influence the generation of carbonaceous products. It was observed that the added metals were efficiently dispersed into the plasma and that their presence increased the yield of fullerenes. The addition of Ir led to a noticeable shift in the fullerene distribution towards C60, whereas the addition of Pt increased the proportion of C60 oxides and decreased the proportion of higher fullerenes. Addition of Ir also caused a reduction of the soot particle size and the formation of a considerable quantity of carbon nanotubes. 相似文献
26.
A Confocal Scanning Laser Microscope equipped with a gold image furnace was used to directly observe the precipitation of MnS during solidification of high sulphur steels under isothermal conditions in the temperature region 1440 to 1480°C on the free surface of the steel melt. For the case of Al‐killed steels, below 1480°C MnS particles were found to precipitate with Fe forming simultaneously around them. This MnS containing structure continued to grow rapidly (264 μm/s) as a surface film. The film gradually changed, as the level of S in the melt decreased, into a eutectic structure (with lamella spacing of 2 μm) as predicted by thermodynamics. In Si‐ killed steels there was significantly lower tendency to form MnS both in terms of time until precipitation occurred and growth rate. 相似文献
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29.
HUANG Jianfeng CAO Liyun ZHANG Chuanbo WU Jianpeng HE Haiyan 《武汉理工大学学报(材料科学英文版)》2005,20(B12):138-140
Nano-particle hydroxyapatite ( HA ) was prepared with a novel ultrasonic precipitation process and the as-prepared nanopowder was used to produce hydroxyapatite ( HA ) coatings on titanium substrate via plasma spraying. The phase and the microstructare of the coating were characterized by X- ray diffraction (XRD) and scanning electron microscopy (SEM). Results showed that spherical particles could be prepared by ultrasonic precipitation process; and a corresponding dense HA coating with molten surface and low-porosity cross-section structure was acquired. During the plasma spraying process, new phases of Ca3 ( PO4 )2 and Ca2 P2O7 were generated. After heat-treating at 800℃ for 1 h, the contents of Ca3 ( PO4 )2 and Ca2 P2O7 decreased while HA content increased. Tensile adhesion tests showed that the plasma sprayed coating prepared with the spherical nanoparticles exhibited high tensile bond strength. 相似文献
30.
动态波前相位的高分辨率测量 总被引:4,自引:0,他引:4
动态波前相位信息测量是大气光学,气动光学和激光技术等领域的重要实验手段。提出了一种具有高的时间和空间分辨率以及长的测量持续时间的动态波前相位测量方法。应用Hartmann-Shack波前传感器获得高空间分辨率的相位信息,采用高帧频CCD摄象机获得高时间分辨率图象数据。 相似文献