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研究了微波制样,用ICP-AES法同时测定珍珠白样品中Mg、Al、Fe、Pb、Cr、Ni、Mn、As八种微量元素的新方法。方法的检出限为0.002~0.036μg/mL,回收率为92.8%~107.6%.RSD小于3.19%。该法准确、快速、简便,应用于花岗石的测定,结果满意。 相似文献
73.
《Measurement》2014
In this study, a digital CMOS camera was calibrated for use as a non-contact colorimeter for measuring the color of granite artworks. The low chroma values of the granite, which yield similar stimulation of the three color channels of the camera, proved to be the most challenging aspect of the task. The appropriate parameters for converting the device-dependent RGB color space into a device-independent color space were established. For this purpose, the color of a large number of Munsell samples (corresponding to the previously defined color gamut of granite) was measured with a digital camera and with a spectrophotometer (reference instrument). The color data were then compared using the CIELAB color formulae. The best correlations between measurements were obtained when the camera works to 10-bits and the spectrophotometric measures in SCI mode. Finally, the calibrated instrument was used successfully to measure the color of six commercial varieties of Spanish granite. 相似文献
74.
以凝灰岩为主要原料,加入发泡剂、助溶剂等形成发泡保温层(上层),以微晶玻璃颗粒为釉面层(下层),在1050~1100℃发泡、熔融,一次烧结形成仿花岗岩、大理石釉面泡沫陶瓷保温、装饰材料,具有保温装饰双重功能。发泡保温层密度为300~500㎏/m3、导热系数为0.7~0.12W/m·K、抗压强度为5~10MPa,釉面层装饰效果独特,可与花岗岩、大理石相媲美。可用于建筑物内外墙、公园建筑小品等的保温与装饰,为凝灰岩资源的合理开发利用开辟了新途径。 相似文献
75.
It is widely acknowledged that residual and sedimentary soils differ considerably because of how they formed. However, despite extensive advances regarding sedimentary soil, little is known about the small-strain stiffness of residual soil. This paper concerns granite residual soil from Xiamen in China, for which a typical profile is established by in situ investigations. How the stiffness varies with the soil current state, including effective mean stress, void ratio and strain, is established via systematic resonant-column tests on high-quality undisturbed and remolded specimens. Highlighted are the unique properties of the studied soil and how they affect the soil stiffness. It is found that cementation among soil particles plays a critical role in the soil stiffness. Although some existing methods can confirm the existence of cementation in the studied soil, they cannot quantify it. Therefore, a new parameter Rn is proposed to quantify the degree of cementation, with lower Rn corresponding to a more cemented structure. According to the proposed Rn, the studied residual soil in Xiamen has a different degree of cementation from that of some well-studied weathered materials, thereby necessitating separate characterization of this soil. This study improves the understanding of residual soil stiffness at small strain, especially the key effect of cementation in natural soil. 相似文献
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The mechanical behaviors and energy dissipation characteristics of heat-treated granite were investigated under repeated impact loading. The granite samples were firstly heat-treated at the temperature of 20°C, 200°C, 400°C, and 600°C, respectively. The thermal damage characteristics of these samples were then observed and measured before impact tests. Dynamic impact compression tests finally were carried out using a modified split-Hopkinson pressure bar under three impact velocities of 12 m/s, 15 m/s, and 18 m/s. These test results show that the mineral composition and the main oxides of the granite do not change with these treatment temperatures. The number of microcracks and microvoids decreases in the sample after 200°C treatment. The mechanical properties of a sample after 600°C treatment were rapidly deteriorated under the same impact velocity. The average of peak stress is much smaller than those after 20°C, 200°C and 400°C treatments. The heat-treated samples have an energy threshold each. When the dissipated energy of a sample under a single impact is less than this threshold, the repeated impacts hardly lead to further damage accumulation even if its total breakage energy dissipation (BED) density is large. Under the same number of repeated impacts, the cumulative BED density of a sample after 600°C treatment is the largest and its damage evolves most quickly. The total BED density of the sample after 200°C treatment is the highest, which implies that this sample has better resistance to repeated impact, thus having less crack initiation and growth. 相似文献
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